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31results about How to "Has semiconducting properties" patented technology

Hydrothermal method for preparing water-soluble graphene quantum dots

ActiveCN102190296BGood size controlAverage distribution size narrowNanotechnologySolubilityWater soluble
The invention discloses a hydrothermal method for preparing water-soluble graphene quantum dots. The invention relates to the preparation method of graphene quantum dots, and especially relates to a hydrothermal method for preparing water-soluble graphene quantum dots. The method provided by the present invention is characterized in that: 0.01 to 1.0M of an aqueous solution of polyhydroxyl carbohydrate is added to a hydrothermal reaction vessel; the aqueous solution is heated for 10 to 600 minutes under a temperature of 120 to 220 DEG C; sugar molecules are polymerized into graphene quantum dots with sizes of 1 to 10nm, such that target products are obtained. The graphene quantum dots prepared with the method provided by the present invention has characteristics of water-solubility, monodispersity and special photoelectrical characteristics. The raw materials are cheap, and the sources of the raw materials are wide. With environmental-protective technology, the method is suitable for volume production.
Owner:KUNMING INST OF PHYSICS

Antistatic polyester film and preparation method thereof

The invention relates to an antistatic polyester film and a preparation method thereof, wherein the antistatic polyester film comprises a polyester film and an antistatic coating layer coated on the surface of the polyester film; the antistatic coating layer is composed of hybrid acrylate resin, an antistatic agent, a curing agent and a solvent; the antistatic coating layer is composed of the components in parts by weight: 30-50 parts of hybrid acrylate resin, 0.5-1 part of a leveling agent, 0.2-2.0 part of the curing agent, and 90-120 parts of the solvent. According to the invention, polythiophene conductive macromolecules are added in the polymerization process, the synergistic effect of polythiophene and modified nano inorganic particles is utilized to improve the antistatic property, and the used modified nano inorganic particles have good rigidity and hardness, are copolymerized with other acrylate monomers after being modified by a silane coupling agent and are uniformly distributed in acrylate resin. According to the hybrid acrylate resin prepared by the preparation method disclosed by the invention, coating is performed after compounding, so that the antistatic coating layer coated on the surface of the polyester film has scratch resistance, meanwhile, the antistatic performance of the film is also improved, and electrostatic adsorption of impurities can be effectivelyprevented.
Owner:HEFEI LUCKY SCI & TECH IND

Method for preparing rapid solidified fine spherical high-silicon high-wear-resistant aluminum-silicon alloy powder

The invention relates to a method for preparing rapid solidified fine spherical high-silicon high-wear-resistant aluminum-silicon alloy powder. The method comprises using high purity aluminum (>99.85 %) ingots and high purity silicon (>99.7%) ingots as raw material ingots, firstly fusing the high purity aluminum and then adding the silicon ingots to obtain a proper AlSi alloy solution, uniformly string, and spraying and atomizing the solution in a closed system through high pressure nitrogen, the alloy solution can be instantly cooled and solidified to form an alloy powder.
Owner:LUXI COUNTY QUNXIANG NEW MATERIAL TECH CO LTD

Lead-free high-Curie temperature PTCR (positive temperature coefficient resistor) ceramic material and preparation method thereof

The invention relates to a lead-free high-Curie temperature PTCR (positive temperature coefficient resistor) ceramic material and a preparation method thereof. The composition of the ceramic material is of Ba1-x (Bi0.5Na0.5)xTiO3, wherein x is not less than 0 and not more than 0.06. A sol-gel method is adopted for preparing the lead-free PTCR material and the method, the sintering temperature of a traditional solid-phase reaction method is too high, when the temperature is above 1300 DEG C, BNT (Bi0.5Na0.5TiO3) is very easy to decompose during the sintering process, and the material is further difficult to be semi-conducted; and by adopting the sol-gel method according to the invention, the sintering can be performed at the temperature of 1250 DEG C, and the sintering temperature is reduced. When the BNT content is more than 2mol%, the sintering and the semi-conduction can not be performed in an air atmosphere by using the traditional solid-phase reaction method, and the sintering needs to be performed under a reducing atmosphere. However, when the BNT content is 5mol%, the material still has the properties of a semi-conductor by using the method disclosed by the invention, and the Curie temperature is obviously increased.
Owner:TIANJIN UNIV

Wire and cable teflon semiconductor thin film and preparation method thereof

The present invention provides a wire and cable teflon semiconductor thin film which is prepared from 92-98 wt % of polytetrafluoroethylene and 2-8 wt % of carbon black by the following method: taking the polytetrafluoroethylene and the carbon black, mixing evenly; pressing for moulding; sintering at high temperature; mechanically processing for film-forming, rolling and orientating. By optimum composition ratio, choosing of appropriate particle size, and use of a certain way for mixing, the problem of ununiform mixing and dispersing of the carbon black in the polytetrafluoroethylene powder can be solved, the product is high in quality, and good in effect, has good semiconductor characteristics and good flame retardant, can be used for wire and cable for balancing electric field and playing the effect of flame retardance, solves the defects of the worse fire retardant performance of PE and TPE wires and cables, is more competitive in price than imported product, is ultra-thin in thickness, fills the domestic blank, and breaks the common situation that black-filled teflon films on market in the prior art are basically used in other fields in which functional requirements are not high.
Owner:FOSHAN HUIFU POLYMER MATERIALS CO LTD

Method for preparing (Cu,Fe)3O4 spinel coating through magnetron sputtering method and application thereof

The invention relates to the field of preparation of (Cu,Fe)3O4 spinel coatings, in particular to a method for preparing a (Cu,Fe)3O4 spinel coating through a magnetron sputtering method and an application thereof. The method includes the following specific preparation steps that (1) pretreatment and pre-oxidation treatment are carried out; (2) sputtering deposition is carried out to obtain an alloy coating; and (3) thermal inversion is carried out to obtain the spinel coating. The method has the characteristics that the operation process is simple and the deposition speed is high, and the prepared spinel coating is compact, has good binding force with a substrate, has excellent long-time resistance to high temperature oxidation and conductivity, and can effectively suppress external diffusion of substrate Cr.
Owner:NORTHEASTERN UNIV

Preparation method of silicon-based surface-enhanced Raman substrate

The invention discloses a preparation method of a silicon-based surface-enhanced Raman substrate. Monocrystalline silicon acquires an ordered pyramid structure through a surface micro-structure preparation method, and the ordered pyramid is coated with a gold film. The preparation method comprises the steps that (1) the ordered pyramid structure on the surface of the monocrystalline silicon is obtained through corrosion of an alkaline solution; and (2) the surface of the monocrystalline silicon of the ordered pyramid structure is coated with the gold film with a certain thickness through an ion sputtering coating method. Composite nano particles obtained by the method have good chemical stability, substances with the concentration as low as 10-70 mol / L can be detected, and the absorption spectrogram obtained after long-time preservation hardly changes. The preparation method is easy and convenient to implement, low in cost, good in repeatability and capable of easily controlling the pyramid dimension and the thickness of the gold film.
Owner:YUNNAN NORMAL UNIV

Method for modifying properties of graphene

InactiveCN104555997AControlling pi BondingChange energy band propertiesCarbon compoundsSemiconductor/solid-state device manufacturingGraphiteCvd graphene
A method for modifying properties of graphene includes a graphene film provision step and a modification step. In the graphene film provision step, a graphene film is provided, and the graphene is formed on a substrate. In the modification step, the graphene film is placed in a vacuum environment and radiated by an electron beam to obtain a graphene material.
Owner:METAL INDS RES & DEV CENT

Metal-organic coordination polymer containing neodymium and copper and preparation method

The invention discloses a metal-organic coordination polymer containing neodymium and copper and a preparation method, and belongs to the technical field of metal-organic coordination polymer crystal. The structural unit of the molecular formula of the polymer is [NdCu1.5(pydc)3(H2O)5].7H2O, and the polymer is synthesized by adopting a solvothermal method; 5 mass parts of 2,5-pyridine-dicarboxylic acid, 3 mass parts of neodymium chloride hexahydrate and 2 mass parts of copper bromide are used as raw materials, and 100 to 120 mass parts of deionized water is used as a solvent; and the method comprises the following steps of: regulating the pH to 6-7, and putting into a stainless steel autoclave, wherein the volume ratio of the solution to the autoclave is 6:25; and reacting for 72 to 120 hours at the temperature of between 140 and 170 DEG C, slowly cooling to room temperature within 24 to 48 hours, and thus obtaining the metal-organic coordination polymer crystal. The polymer is high in thermal stability, and has semiconductor property..
Owner:BEIJING UNIV OF CHEM TECH

A kind of preparation method of silicon-based surface enhanced Raman substrate

The invention discloses a preparation method of a silicon-based surface-enhanced Raman substrate. Monocrystalline silicon acquires an ordered pyramid structure through a surface micro-structure preparation method, and the ordered pyramid is coated with a gold film. The preparation method comprises the steps that (1) the ordered pyramid structure on the surface of the monocrystalline silicon is obtained through corrosion of an alkaline solution; and (2) the surface of the monocrystalline silicon of the ordered pyramid structure is coated with the gold film with a certain thickness through an ion sputtering coating method. Composite nano particles obtained by the method have good chemical stability, substances with the concentration as low as 10-70 mol / L can be detected, and the absorption spectrogram obtained after long-time preservation hardly changes. The preparation method is easy and convenient to implement, low in cost, good in repeatability and capable of easily controlling the pyramid dimension and the thickness of the gold film.
Owner:YUNNAN NORMAL UNIV

Active biology carrier material

The invention discloses an active biology carrier material. The material comprises following components in percentage by weight: 85 to 95% of polypropylene, 0.1 to 10% of germanium powder and 5 to 15% of carbon powder. The components mentioned above are subjected to a modification process to be made into even micelles for injection moulding, and then the micelles are injection moulded into the biology carriers for water processing through a mould. The active biology carrier material is beneficial to form a firm biology membrane, increases biology capacity of unit volume, increases dissolving sources of the water body and improves the biology active ability.
Owner:梁锦雄

Bidirectional protection lubricating wear-resistant coupling

ActiveCN103603608AGood mechanical stabilityLow friction coefficient of lubricationDrilling rodsDrilling casingsLubricationWear resistant
A bidirectional protection lubricating wear-resistant coupling comprises a lubricating wear-resistant agent layer formed by coating lubricating wear-resistant agent on the surface of a sucker-rod coupling through the surface reinforcing treatment process. The thickness of the lubricating wear-resistant agent layer is less than 0.5mm. Defects conventionally existing in the prior art that hardness is low, strength is low, wear resistance is low, corrosion resistance is low, scratch resistance is low, heat resistance is low, friction coefficient is high, self-lubrication and oxidation resistance cannot be completed, impact resistance is low, high temperature stability is poor, and service life is short are avoided effectively.
Owner:大庆市盛日石油技术开发有限公司

Method for preparing diamond based on graphite under low pressure

The invention discloses a method for preparing diamond based on graphite under low pressure, which combines theoretical calculation and experimental research of a first principle, and realizes conversion from graphite to diamond under low pressure by depositing transition metal on the surface of graphite; the method has the advantages of being mild in condition, low in cost, low in equipment requirement, simple in process and easy to operate, the obtained transition metal terminated diamond has the semiconductor property, and a new material is provided for application of diamond electronic devices.
Owner:ZHEJIANG UNIV OF TECH

Water-based seal white primer

The invention relates to the technical field of woodenware seal primers, and particularly discloses a water-based seal white primer. The white primer is characterized in that the white primer containsthe following components in parts by weight: 30-50 parts of water-based polyurethane resin; 30-40 parts of water-based hydroxyl-terminated silicone resin; 15-30 parts of titanium dioxide; 45-60 partsof water-based silicon resin; 1-5 parts of silica powder; 1-10 parts of transparent powder; 1-10 parts of zinc powder; 3-10 parts of ethylene glycol monobutyl ether; 5-13 parts of deionized water; and 5-13 parts of absolute ethyl alcohol. Water-based polyurethane resin and water-based hydroxyl-terminated silicon resin permeate into wood and are crosslinked and cured to form a compact paint film tightly combined with the wood, so that pores of the wood are sealed and blocked, the crosslinking density is further improved through the water-based silicon resin, the sealing effect is improved, andsilicon micro-powder, transparent powder and zinc powder are combined, so the white filling and sealing material with good fluidity, high strength and high whiteness is formed; the use amount of subsequent white primer is effectively reduced while the filling and sealing effect is ensured, and the sealing treatment process is simplified.
Owner:广东新红阳科技有限公司

Negative electrode material for secondary battery, preparation method of negative electrode material, negative electrode plate and secondary battery

ActiveCN114335459AResolve small gapsSolve the problem that alkali metal deintercalation with large ionic radius cannot be achievedSecondary cellsNon-aqueous electrolyte accumulator electrodesVanadium disulfideElectrical battery
The invention provides a negative electrode material for a secondary battery, a preparation method of the negative electrode material, a negative electrode plate and the secondary battery. The negative electrode material comprises a nanocube framework and layered vanadium disulfide growing on the surface of the nanocube framework, a precursor of the nanocube framework is a zeolite imidazole metal organic framework. Compared with the prior art, the negative electrode material provided by the invention adopts the nanocube as a supporting framework and the zeolite imidazole metal organic framework as a precursor, so that the negative electrode material has relatively good stability in structure and can provide stable support for an overall layered three-dimensional structure; lamellar vanadium disulfide is grown on the surface of the nanocube framework, the lamellar vanadium disulfide is formed by S-V-S connection, the interlayer distance is large, electrons can be transmitted in a planar network formed by V-V bonds, and the electron transfer efficiency is improved. And the problem that the deintercalation of alkali metal with larger ion radius cannot be realized due to smaller interlayer spacing of the existing graphite negative electrode material can be effectively solved.
Owner:HUIZHOU LIWINON NEW ENERGY TECH CO LTD

A two-dimensional semiconductor material snse 2 Single crystal preparation method

The invention discloses a two-dimensional semiconductor material SnSe 2 Single crystal preparation method: mix Se powder and Sn powder evenly, put them into a quartz tube, put elemental iodine, pump the air pressure in the quartz tube to ≤0.1mbar, seal the tube; put the quartz tube into a double temperature zone tube furnace , put one end containing the raw material in the high temperature zone and the other end in the low temperature zone. Keep at 560-600°C for 5-7 days; then lower to room temperature, keep the temperature difference between the high-temperature zone and the low-temperature zone at 10-50°C during the cooling process, and obtain flake, large-area, high-quality SnSe 2 single crystal. The present invention can prepare SnSe in one step 2 Single crystal, single crystal is bright black, in thin sheet shape, single crystal composition is uniform, the surface is smooth, easy to mechanically peel off, which is conducive to micro-processing of materials such as photolithography.
Owner:NANJING TECH UNIV

Lead-free high-Curie temperature PTCR (positive temperature coefficient resistor) ceramic material and preparation method thereof

The invention relates to a lead-free high-Curie temperature PTCR (positive temperature coefficient resistor) ceramic material and a preparation method thereof. The composition of the ceramic material is of Ba1-x (Bi0.5Na0.5)xTiO3, wherein x is not less than 0 and not more than 0.06. A sol-gel method is adopted for preparing the lead-free PTCR material and the method, the sintering temperature of a traditional solid-phase reaction method is too high, when the temperature is above 1300 DEG C, BNT (Bi0.5Na0.5TiO3) is very easy to decompose during the sintering process, and the material is further difficult to be semi-conducted; and by adopting the sol-gel method according to the invention, the sintering can be performed at the temperature of 1250 DEG C, and the sintering temperature is reduced. When the BNT content is more than 2mol%, the sintering and the semi-conduction can not be performed in an air atmosphere by using the traditional solid-phase reaction method, and the sintering needs to be performed under a reducing atmosphere. However, when the BNT content is 5mol%, the material still has the properties of a semi-conductor by using the method disclosed by the invention, and the Curie temperature is obviously increased.
Owner:TIANJIN UNIV

Method for preparing nanometer titanium dioxide microcrystalline by utilizing solid state feeding manner

The invention discloses a method for preparing nanometer titanium dioxide microcrystalline by utilizing solid state feeding manner, belongs to the technical field of chemical technology and novel material synthesis, and relates to a production technology for preparing the nanometer titanium dioxide microcrystalline by adopting a high-frequency plasma vapor deposition method. The method disclosed by the invention comprises the following steps: adopting solid state titanium dioxide powder as a basic material, completing decomposition and an oxidation reaction under an oxygen-rich high-frequency plasma state jet flow atmosphere, and carrying out shock cooling to obtain the nanometer titanium dioxide microcrystalline with an average grain diameter range of 20-50 nm. Compared with the other methods, the microcrystalline prepared by the method is high in purity and approximately spherical; the particle size of the microcrystalline can be controlled; the method is short in technological process, and continuous in operation, and facilitates industrial production.
Owner:TAIYUAN UNIV OF TECH

Organic heteropolymer and method for manufacturing same

This organic heteropolymer is useful in forming organic semiconductors and is a copolymeric heteropolymer that comprises a structural unit represented by formula (1) and a structural unit represented by formula (2). (In the formulas: M1 and M2 represent heteroatoms selected from mutually differing groups among the group 8 elements, the group 9 elements, the group 10 elements, the group 14 elements, the group 15 elements, and the group 16 elements on the periodic table; the atomic valence (v) of M1 and M2 is in the range 2-6; R1a and R1b each represent a halogen atom, an alkyl group, a cycloalkyl group, an aryl group, or a heteroaryl group and may be the same or different; R2a and R2b each represent a halogen atom, an alkyl group, a cycloalkyl group, an aryl group, a heteroaryl group, a monovalent or bivalent heteroatom selected from the group consisting of the group 16 elements and the group 11 elements on the periodic table, or a metal atom that has formed a complex with a ligand and may be the same or different; m1, m2, n1, and n2 each represent 0 or 1; circled Ar represents an aromatic ring; R3 represents a straight-chain or branched-chain alkyl group, a straight-chain or branched-chain alkoxy group, or a straight-chain or branched-chain alkylthio group; and p represents 0 or an integer in the range 1-3.)
Owner:DAICEL CHEM IND LTD +1

An active biological carrier material

The invention discloses an active biology carrier material. The material comprises following components in percentage by weight: 85 to 95% of polypropylene, 0.1 to 10% of germanium powder and 5 to 15% of carbon powder. The components mentioned above are subjected to a modification process to be made into even micelles for injection moulding, and then the micelles are injection moulded into the biology carriers for water processing through a mould. The active biology carrier material is beneficial to form a firm biology membrane, increases biology capacity of unit volume, increases dissolving sources of the water body and improves the biology active ability.
Owner:梁锦雄

Flexible substrate and preparation method thereof

The invention relates to a flexible substrate and a preparation method thereof. The flexible substrate comprises a substrate and a coating layer stacked on the substrate, wherein the coating layer comprises a first graphene layer, a first ITO layer, a second graphene layer and a second ITO layer which are stacked in sequence, and the first graphene layer is stacked on the substrate. The adhesion between the substrate and the coating layer in the flexible substrate is good, it is not prone to cracking, and the bending property of the flexible substrate is good.
Owner:WGTECH JIANGXI

Heating device, preparation method of device and high-temperature heating equipment

The invention provides a heating device which is ultrathin, good in high-temperature resistance, safe, reliable, high in heating efficiency, simple in structure and resistant to oxidation, a preparation method of the device and high-temperature heating equipment comprising the heating device. The heating device comprises an insulating substrate layer (1), wherein a titanium diboride semiconductorfilm layer (2) is sputtered on one surface of the insulating substrate layer, and an antioxidant and insulating protective film layer (3) is sputtered outside the titanium diboride semiconductor filmlayer. The preparation method comprises the following steps of a, preparing the insulating substrate layer, and preparing a titanium diboride target material; b, sputtering the titanium diboride target material on the surface of the insulating substrate layer and preparing an electrode; and c, sputtering the antioxidant and insulating protective film layer (3) on the surface of the formed titaniumdiboride semiconductor film layer. The high-temperature heating equipment comprises a main body (4), wherein a heating plate (5) is arranged on the surface of the main body, and the heating device isattached to the lower surface of the heating plate. The heating device, the preparation method of the device and the high-temperature heating equipment are applied to the field of high-temperature heating.
Owner:珠海尔康智能厨卫科技有限公司

Semiconductor graphene nanobelt as well as preparation method and application thereof

The invention provides a semiconductor graphene nanobelt and a preparation method and application thereof, and the preparation method comprises the following steps: carrying out annealing treatment on single-walled carbon nanotubes in air, then adding the single-walled carbon nanotubes into concentrated sulfuric acid, and stirring to obtain a single-walled carbon nanotube suspension; adding potassium permanganate into the single-walled carbon nanotube suspension for reaction; after the reaction is completed, pouring reaction liquid into ice water, filtering and drying to obtain the single-walled carbon nanotube with defects; adding the obtained single-walled carbon nanotube with defects into a sodium dodecyl benzene sulfonate aqueous solution for ultrasonic treatment, filtering and drying to obtain a semiconductor graphene nanobelt, and annealing at high temperature to obtain the high-quality semiconductor graphene nanobelt. The method disclosed by the invention is simple in process and easy for large-scale preparation, and the obtained semiconductor graphene nanobelt is high in quality and good in uniformity. The field effect transistor based on the obtained graphene nanobelt not only obtains a current on-off ratio of more than 105, but also has a photoluminescence effect.
Owner:SHANDONG UNIV

Preparation of (cu,fe) by a magnetron sputtering method 3 o 4 Method of spinel coating and its application

The present invention relates to (Cu, Fe) 3 O 4 The field of preparation of spinel coatings, specifically involving the preparation of (Cu, Fe) by magnetron sputtering 3 O 4 The method and application of spinel coating, the specific preparation steps are as follows: (1) pretreatment and pre-oxidation treatment; (2) sputtering deposition to obtain alloy coating; (3) thermal conversion to obtain spinel coating . This method has the characteristics of simple operation process and fast deposition rate. The prepared spinel coating is dense and has good bonding force with the substrate. It has excellent long-term high temperature oxidation resistance and conductivity, and can effectively inhibit the external diffusion of Cr from the substrate. .
Owner:NORTHEASTERN UNIV LIAONING

Metal-organic coordination polymer containing neodymium and copper and preparation method

The invention discloses a metal-organic coordination polymer containing neodymium and copper and a preparation method, and belongs to the technical field of metal-organic coordination polymer crystal. The structural unit of the molecular formula of the polymer is [NdCu1.5(pydc)3(H2O)5].7H2O, and the polymer is synthesized by adopting a solvothermal method; 5 mass parts of 2,5-pyridine-dicarboxylic acid, 3 mass parts of neodymium chloride hexahydrate and 2 mass parts of copper bromide are used as raw materials, and 100 to 120 mass parts of deionized water is used as a solvent; and the method comprises the following steps of: regulating the pH to 6-7, and putting into a stainless steel autoclave, wherein the volume ratio of the solution to the autoclave is 6:25; and reacting for 72 to 120 hours at the temperature of between 140 and 170 DEG C, slowly cooling to room temperature within 24 to 48 hours, and thus obtaining the metal-organic coordination polymer crystal. The polymer is high in thermal stability, and has semiconductor property..
Owner:BEIJING UNIV OF CHEM TECH

A kind of Teflon semiconductor thin film for electric wire and cable and preparation method thereof

ActiveCN104910563BSolve the problem of uneven mixing and dispersionSolve the defect of poor flame retardancyPlastic/resin/waxes insulatorsFire retardantFunctional requirement
The present invention provides a wire and cable teflon semiconductor thin film which is prepared from 92-98 wt % of polytetrafluoroethylene and 2-8 wt % of carbon black by the following method: taking the polytetrafluoroethylene and the carbon black, mixing evenly; pressing for moulding; sintering at high temperature; mechanically processing for film-forming, rolling and orientating. By optimum composition ratio, choosing of appropriate particle size, and use of a certain way for mixing, the problem of ununiform mixing and dispersing of the carbon black in the polytetrafluoroethylene powder can be solved, the product is high in quality, and good in effect, has good semiconductor characteristics and good flame retardant, can be used for wire and cable for balancing electric field and playing the effect of flame retardance, solves the defects of the worse fire retardant performance of PE and TPE wires and cables, is more competitive in price than imported product, is ultra-thin in thickness, fills the domestic blank, and breaks the common situation that black-filled teflon films on market in the prior art are basically used in other fields in which functional requirements are not high.
Owner:FOSHAN HUIFU POLYMER MATERIALS CO LTD
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