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64results about How to "Improve oil-water separation effect" patented technology

Nano composite high-temperature-resistant extraction aid for thickened oil and super-thickened oil recovery and preparation method thereof

The invention discloses a nano composite high-temperature-resistant extraction aid for thickened oil and super-thickened oil recovery. The nano composite high-temperature-resistant extraction aid is prepared from 3-8 weight percent of modified nano-silica, 3-8 weight percent of petroleum sulfonate, 10-40 weight percent of a viscosity reducer, 5-15 weight percent of an emulsifier, 2-10 weight percent of a surface wetting agent, 2-10 weight percent of a penetrating agent, 5-10 weight percent of a high polymer modifier, 1-8 weight percent of a catalyst and the balance of water. The preparation method comprises the following steps: polymerizing the petroleum sulfonate, viscosity reducer, a promoting agent and the catalyst at the temperature of 60-150 DEG C for 2-6 hours according to a ratio, adding the modified nano inorganic aid, and uniformly mixing; and finally, adding the emulsifier, surface wetting agent, penetrating agent, high polymer modifier and water according to the ratio, and mixing for 1-2 hours. The nano composite high-temperature-resistant extraction aid for thickened oil and super-thickened oil recovery has high high-temperature resistance and excellent emulsification and salt resistance, the production efficiency can be greatly improved, and the recovery rate is reduced.
Owner:GUNGHO CHARGE TIANJIN REFINED PETROLEUM TECH DEV

Method for coating surface of underwater oleophobic net film with nano-material

The invention provides a method for coating the surface of an underwater oleophobic net film with a nano-material. The method comprises the following steps of carrying out chemical etching on a cleaned and dried stainless wire net film by a chemical etching agent, carrying out ultrasonic cleaning and drying, immersing the stainless wire net film in a cation precipitating agent solution so that chemical modification is realized, taking out the stainless wire net film, carrying out washing by deionized water, carrying out blow-drying by a nitrogen flow, immersing the stainless wire net film in a silicon dioxide dispersion liquid of graphene oxide so that a coating process is realized, taking out the treated stainless wire net film, carrying out washing by deionized water, repeating chemical modification-coating processes multiple times to obtain a coated stainless wire net film, carrying out drying, carrying out calcination at a temperature of 500-550 DEG C in a nitrogen protective atmosphere for 3-4h and carrying out cooling to obtain the stainless wire net film finished product. The method is carried out at a normal temperature, has simple processes and a low cost, utilizes an etching agent and a modified agent with low environment pollution and does not cause secondary pollution. The stainless wire net film has strong corrosion resistance, substantial oil-water separation effects, a long service life and good escherichia coli inhibition effects.
Owner:JIANGSU UNIV

Super-oleophylic and super-hydrophobic sponge for oil-water separation, and preparation method and application of super-oleophylic and super-hydrophobic sponge

InactiveCN110387062AGood super-oleophilic and super-hydrophobic propertiesImprove hydrophobicityLiquid separationPolymer scienceOil water
The invention discloses a super-oleophylic and super-hydrophobic sponge for oil-water separation, and a preparation method and application of the super-oleophylic and super-hydrophobic sponge, and belongs to the technical field of oil-water separation materials. Nano-silica and an organic dispersion liquid of MQ silicone are painted on the surface of a sponge by adopting the dip-coating method, inthe process of drying, with the volatilization of a solvent, the MQ silicone and the nano-silica produce phase separation and deposit on the surface of the sponge, a micron-nanometer secondary composite structure is formed on the surface of the sponge, and a good structural basis is provided for the super-oleophylic and super-hydrophobic properties of the sponge. In addition, according to the MQsilicone and the nano-silica treated by a silane coupling agent which are deposited on the surface of the sponge, the surface of the sponge has a lot of silicon elements, since the silicon elements have very low surface energy and good affinity with non-polar oil, and good hydrophobic and oleophylic properties are achieved on the sponge. The sponge prepared by the preparation method has excellentoil-water separation performance, the process is simple, the raw materials are easy to obtain, the cost is low, and volume production can be achieved.
Owner:XI'AN POLYTECHNIC UNIVERSITY

Marine diesel engine oil composition and preparation method and application thereof

The invention discloses an oil composition for a marine diesel engine and a preparation method and application thereof, and mainly solves the technical problem that a demulsifier needs to be added into the oil composition for the marine diesel engine to improve the oil-water separation performance in the prior art. The oil composition for the marine diesel engine is prepared from the following components in parts by mass: 0.1-20 parts of a clearing agent; 0.1-20 parts of a dispersant, 0.6-15 parts of an antioxidant; 0.001-1 part of an anti-foaming agent; an 50-98 parts of base oil. The preparation method of the marine diesel engine oil composition comprises the following steps: adding the clearing agent, the dispersing agent, the antioxidant and the anti-foaming agent into the base oil atthe temperature of 50-60 DEG C, performing stirring for 0.5-3 hours, and performing complete dissolving to obtain the marine diesel engine oil composition. The present invention discloses the application of the marine diesel engine oil composition in marine diesel engines, thereby better solving the problems. The marine diesel engine oil composition and preparation method and application thereof are suitable for industrial application of lubrication of marine diesel engines.
Owner:CHINA PETROLEUM & CHEM CORP

Method for preparing catechol-based hydrophilic modified organic tubular membrane

The invention discloses a method for preparing a catechol-based hydrophilic modified organic tubular membrane, which comprises the following steps: soaking a membrane tube in pure water to obtain a completely infiltrated membrane tube; adding a catechol group-containing hydrophilic modifier and a silane coupling agent into a pH buffer solution to prepare a solution; and completely immersing the infiltrated membrane tube in the hydrophilic modifier solution, carrying out aeration treatment at the bottom of a hydrophilic modifier solution container to enable the hydrophilic modifier to be subjected to a full oxidation reaction, then conducting immersing in pure water to remove residues on the surface of the membrane tube, and conducting packaging to obtain a tubular membrane product. According to the method for hydrophilically modifying the organic tubular membrane through the catechol groups, the catechol group-containing hydrophilic modifier such as dopamine and tannic acid and the silane coupling agent are subjected to composite deposition on the surface of the membrane, so that the hydrophilicity of the membrane is improved, and the organic tubular membrane which is large in membrane flux, good in hydrophilicity and easy to clean is prepared. The method is simple to operate and easy for industrial production, improves the oil-water separation performance of partial material membranes, and expands the application range.
Owner:安徽普朗膜技术有限公司

Preparation method of bacterial cellulose membrane for oil-water separation and with pore diameter adjusted by potato starch

The invention discloses a preparation method of a bacterial cellulose membrane for oil-water separation and with the pore diameter adjusted by potato starch. The invention discloses a novel bacterialcellulose/silicon dioxide/hexadecyltrimethoxysilane oil-water separation composite membrane with good oil-water separation capability and high biodegradability, and a preparation method thereof, and belongs to the technical field of functional materials. The preparation method comprises the following steps: (1) culturing and purifying a bacterial cellulose/starch membrane; (2) preparing an ethyl orthosilicate/ethanol solution and a hexadecyl trimethoxy silane/ethanol solution; and (3) preparing the bacterial cellulose/silicon dioxide/hexadecyltrimethoxysilane oil-water separation composite membrane. The preparation method is simple, compared with a traditional oil-water separation mode, the prepared composite membrane not only has good oil-water separation capacity, but also has a series of advantages of high biodegradability, no toxicity or harm, shape plasticity and the like, and technical support is provided for saving water and oil resources and protecting the environment.
Owner:TIANJIN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Phenyl-reinforced flexible silicon dioxide aerogel as well as preparation method and application thereof

The invention discloses phenyl reinforced flexible silicon dioxide aerogel as well as a preparation method and application thereof, wherein the phenyl reinforced flexible silicon dioxide aerogel is prepared by taking at least one first silicon source comprising a phenyl group and at least one second silicon source comprising a methyl group as precursors through a sol-gel method. The aerogel has the advantages of super-hydrophobicity, excellent mechanical property, good oil-water separation capacity, excellent thermal stability and excellent flame retardance. The preparation method comprises the following steps: step 1, preparing materials according to the phenyl reinforced flexible silicon dioxide aerogel; step 2, acidification hydrolysis: dissolving CTAB in an acid solution to obtain a mixed solution, adding a first silicon source and a second silicon source into the mixed solution, and continuously stirring to acidify and hydrolyze the first silicon source and the second silicon source; step 3, alkalization and polycondensation: alkali is added into the solution after acidification and hydrolysis, and gel is formed through alkalization and polycondensation; step 4, aging and drying the gel to obtain the phenyl reinforced flexible silicon dioxide aerogel.
Owner:SOUTHWEST UNIV

Device and method for separating oil and water on top of debenzolization tower with excellent separation effect

The present invention discloses a device and method for oil-water separation on the top of a debenzolization tower with excellent separation effect, and relates to the technical field of debenzolization of chemical production, and the device and method are used for improving the oil-water separation effect on the top of the debenzolization tower. The technical proposal is as follows: according tothe device and method, a plurality of liquid level gauges are adopted to display height of an oil-water separation interface of each part of a tank body, and the separation interface of an oil-water mixture in the tank body is controlled between a separation oil outlet and an oil-water mixture inlet through regulating control valves of different separated water outlets and different oil return ports, thus the oil-water separation effect is improved, it is ensured that separated oil does not carry water, and separated water does not carry oil, benzene oil is fully returned to the debenzolization tower, and the separated water is continuously discharged outside the debenzolization tower, debenzolization distillation operation is stabilized, the light benzene yield and quality are greatly improved, and significant economic benefits are achieved; and oil-water separation control operation is normalized and standardized, the operation efficiency is improved, the time for regulating oil-water separation to achieve optimal effect is effectively shortened, and safe and stable production of debenzolization distillation is ensured.
Owner:宣化钢铁集团有限责任公司

Preparation method of polyacrylonitrile/reduced graphene oxide composite oil absorption material

The invention discloses a preparation method of a polyacrylonitrile/reduced graphene oxide composite oil absorption material, belongs to the field of oil absorption materials, and aims to solve the problems that an existing polymer porous oil absorption material is low in oil absorption rate and complex in preparation process. The preparation method comprises the following steps of: chopping polyacrylonitrile fibers to 3-5mm; putting the chopped polyacrylonitrile fibers into a crusher; uniformly dispersing and infiltrating the chopped polyacrylonitrile fibers into a reduced graphene oxide aqueous solution; carrying out ultrasonic treatment for 10-30min; sealing an obtained product in a container; putting the container into a drying oven; carrying out hydrothermal reaction; cooling to roomtemperature; washing a reaction product with distilled water; freezing the reaction product in a refrigerator; and finally drying the reaction product in a freeze dryer to obtain the polyacrylonitrile/reduced graphene oxide composite oil absorption material. According to the preparation method, the polyacrylonitrile fibers are taken as a framework, and the reduced graphene oxide is taken as a reinforcing phase; the oil absorption material which is ultra-light, high in saturated oil absorption rate, high in oil absorption rate, stable in structure and capable of being recycled for multiple times is prepared through the hydrothermal method and freeze drying, and the oil absorption material is widely applied to the fields of oil stain leakage and the like.
Owner:TAIYUAN UNIV OF TECH
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