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192results about How to "Increase interface area" patented technology

Preparation method of compound graphite material for lithium ion secondary battery

The invention discloses a preparation method of a compound graphite material for a lithium ion secondary battery. The preparation method comprises the following steps of: firstly pouring natural graphite, a binding agent and a graphite catalyst which are taken as raw materials into a roller furnace, wherein the roller furnace rotates all the time in a raw material pouring process; then progressively heating the raw materials, namely heating the raw materials in the roller furnace by adopting a progressive heating mode while the roller furnace rotates in a heating process, and then carrying out natural cooling to normal temperature after the raw materials in the roller furnace are heated; and finally carrying out graphitizing treatment on the raw materials, thus the binding agent forms artificial graphite, and the artificial graphite forms a coating on natural graphite particles, so as to form a shell-core structure, and compound particles of the shell-core structure are further spliced to form compound graphite particles with the required grain diameter. The compound graphite material prepared by the invention is of the shell-core structure with the natural graphite as an inner core and an artificial graphite layer as a coating, and the compound graphite has good isotropy, high capacity, high compactness, excellent multiplying, low temperature and cyclic performances and low electrode expansion. The preparation method of the compound graphite material for the lithium ion secondary battery adopts a method that coating and splicing are carried out at the same time, the preparation method is simple and practicable, and the cost is low.
Owner:DONGGUAN KAIJIN NEW ENERGY TECH

Improved process for producing cyclohexanol and pimelinketone

The invention discloses an improved method for preparing cyclohexanol and cyclohexanone. The invention is characterized in that the decomposition reaction of cyclohexyl peroxide is accomplished with two steps; during the first decomposition reaction, the flow of circulated alkaline is equal to or larger than that of cyclohexane oxydic liquid, thereby ensuring the alkaline water phase to become a continuous phase of the material in the first decomposition reaction; the cyclohexane phase is dispersed; the decomposition reaction is accomplished under an emulsification state, or is called even phase decomposition; the compound from the decomposition reaction is rough separated through a hydrocyclone separator; a large amount of alkaline liquid is separated from the lower outlet of the hydrocyclone separator to be recycled; the material of cyclohexane from the upper outlet of the hydrocyclone separator is changed to the continuous phase, while little alkaline liquid is changed into the dispersing phase; the waste alkaline liquid is separated by lifting a separation groove through gravity; the second decomposition reaction is then accomplished to ensure a full decomposition reaction. With the technical improvement, the total mol yield of the oxidation of cyclohexane prepared cyclohexanol and the cyclohexanone device is increased by 5 percent.
Owner:肖藻生

Organic-inorganic nano composite resin and preparation method thereof

The invention relates to organic-inorganic nano composite resin and a preparation method thereof, belonging to the technical field of biomedical high-molecular materials. The organic-inorganic nano composite resin is characterized in that polyfunctional reactive nano monomer, i.e. polyhedral oligosilsesquioxane (POSS) is added on the basis of organic matrixes and inorganic fillers. The preparation method comprises the steps of adding the POSS into the resin matrixes, placing in a constant-temperature oven, fully dissolving the POSS in the resin matrixes and even agitating; adding an initiator system and evenly agitating; adding the inorganic fillers which are subject to surface silanization treatment, fully and evenly agitating in a vacuum agitator and removing air bubbles to obtain nano composite resin paste. By adding the POSS into dental composite resin, polymerization shrinkage can be obviously reduced, the mechanical property of the composite resin is comprehensively improved, the micro-leakage performance and the biocompatibility are good and the application prospect in the field of oral rehabilitation is wide. Besides, the preparation process is simple, the cost is lower and the popularization value and the application value are great.
Owner:HARBIN INST OF TECH

Preparation method of high-strength high-conductivity copper-niobium multi-core composite wire

The invention provides a preparation method of a high-strength high-conductivity copper-niobium multi-core composite wire. The preparation method comprises the following steps that 1, oxygen-free copper foil and niobium foil are stacked in order and wound around an oxygen-free copper bar to obtain a copper-niobium winding body, then, the copper-niobium winding body is installed in a first oxygen-free copper tube, and a copper-niobium composite sleeve is obtained after seal welding; 2, isostatic cool pressing forming is carried out, and a copper-niobium pressed formed part is obtained; 3, hot extrusion machining is carried out to obtain a copper-niobium extrusion bar billet; 4, multi-pass drawing machining is carried out to obtain a copper-niobium single-core wire; 5, sizing, shearing, straightening and acid pickling treatment are carried out in sequence; 6, bundling assembling is carried out to prepare a copper-niobium bundle sleeve, the steps 2-5 are repeatedly executed, and the high-strength high-conductivity copper-niobium multi-core composite wire is obtained. The initial machining size of a niobium core wire can be lowered, the machining hardness of materials is reduced, the machining period is shortened, and the preparation method is the novel method for preparing the high-strength high-conductivity copper-niobium multi-core composite wire.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Method for preparing lithium-sulfur battery by taking graphitized carbon nanotube flexible film as current collector of lithium-sulfur battery

A method for preparing a lithium-sulfur battery by taking a graphitized carbon nanotube flexible film as a current collector of the lithium-sulfur battery comprises the following steps of (1) taking sulfur as an active material, adding a conductive agent and a binding agent, taking N-methylpyrrolidone or deionized water as a solvent, and mixing paste; (2) coating the active material subjected to paste mixing already on the graphitized carbon nanotube flexible film, performing drying after coating, cutting the graphitized carbon nanotube flexible film to a product with the same size as a negative pole plate, and performing vacuum drying to obtain a positive pole plate; and (3) taking a lithium sheet as the negative pole plate, adding an electrolyte in a vacuum glove box, and assembling the battery according to a sequence of a negative electrode shell, the negative pole plate, a separator, the positive pole plate, foamed nickel and a positive electrode shell. The nanotube flexible film has a large amount of micropores with different sizes, the sulfur are very favorably deposited and absorbed into the micropores, thus, sulfur loading quantity in the positive pole plate and electrochemical reaction interface area are effectively increased, electron and ion conduction are enhanced, and the charge/discharge performance of the lithium-sulfur battery can be substantially improved.
Owner:NANCHANG UNIV

Steel-based carbon fibre composite material and preparation method thereof

The invention relates to a steel-based carbon fibre composite material and a preparation method thereof. The steel-based carbon fibre composite material comprises a plurality of bent carbon fibres which intertwine one another, a steel-based material and an adhesive which is adhered to the surface of the carbon fibres, wherein the carbon fibres, the adhesive and the steel-based material are formed by connecting through chemical bonds; a coral-like interface is formed between the adhesive which is adhered to the surfaces of the carbon fibres and the steel-based material through the chemical bonds; the preparation method for the steel-based carbon fibre composite material comprises the following steps: infiltrating the carbon fibres by utilizing the liquid adhesive; intertwining the carbon fibres after excessive adhesive is extruded away so that three-dimensional structural sponge-shaped carbon fibres which are adhered with the adhesive are formed; compounding the carbon fibres with the steel-base material after vacuumizing treatment is performed; finally, placing the composite material into a mould, pressurizing, cooling and moulding to obtain the steel-based carbon fibre composite material which is connected through the chemical bonds. The composite material prepared by the preparation method is far beyond the upper modulus limit of various types of conventional steel substrate materials; the rigidity, the tensile strength, the breaking power and the shearing strength are greatly improved.
Owner:靳普
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