45results about How to "Precise particle size control" patented technology

The invention relates to an electrochemical preparation method of a graphene/nickel-aluminum bimetal hydroxide composite material for a super capacitor, belonging to the technical field of capacitor preparation. The method comprises the following steps of: putting graphite oxide in a beaker; adding deionized water and supporting electrolyte; performing ultrasonic oscillation and constant-potential electrolysis; taking out the electrode; washing the electrode with the deionized water and drying; putting the obtained graphene-modified electrode into a solution containing the precursor of nickel salt and aluminum salt; adding the supporting electrolyte; performing constant-potential electrolysis for 10 seconds; taking out the electrode; and washing the electrode with the deionized water and drying. In the invention, the electrolysis is performed under controlled potential to electrically and alternately deposit the graphene and bimetal hydroxide on the surface of the electrode, therefore, the reduction and deposition of the graphene oxide are finished at the same time, and more importantly, the accurate control on the layer thickness of graphene as well as the size and distribution density of bimetal hydroxide particles is realized; and moreover, the preparation of the material does not produce the 'three wastes' (waste gas, waste water and waste residues).

The invention belongs to the technical field of metal and alloy powder preparation, and relates to a preparation method for AlSi10Mg aluminum alloy superfine powder for 3D printing. The preparation method is characterized by comprising the following preparation steps of: performing supersonic-speed gas atomization and ultrasonic-wave vibratory screening. By utilizing homemade equipment, the invention provides the preparation method for AlSi10Mg aluminum alloy superfine powder for 3D printing. Powder prepared by the method has the advantages such as small pollution in a process, high purity, low oxygen content, precise grain size control and low cost, can meet requirements of the 3D printing process, and also can realize replacing imported powder.

The invention provides sphere-like silver powder with particle size capable of being accurately controlled and a preparation method thereof. The method comprises the following steps: (1), mixing a nano-silver colloid with a dispersing agent solution to obtain a mixed solution, wherein the silver particles in the nano-silver colloid are approximately spherical; (2) under a stirring condition, dripping a silver salt solution and a reducing agent solution into the mixed solution in the step (1) in a parallel flow mode to react, so as to obtain silver powder slurry; and (3) carrying out solid-liquid separation, washing and drying on the silver powder slurry obtained in the step (2) to obtain the sphere-like silver powder. The silver salt solution and the reducing agent solution are dropwise added into the mixed solution of a dispersing agent and a seed crystal in a parallel flow mode to control the generation speed of elemental silver, so that the elemental silver uniformly grows on the provided nano-silver colloid seed crystal, the sphere-like silver powder with the particle size accurately controllable is obtained, and the reaction conditions are mild, normal temperature and normal pressure are achieved, equipment and process are simple, and the production period is short; it is easy to amplification and industrial application; the prepared silver powder is uniform in morphology,good in dispersity and high in tap density.

The invention discloses a roller crusher, which belongs to the technical field of mining machinery. The roller crusher includes sawtoothed rollers whose outer walls are driven to rotate by their mandrels. The rollers are two side by side. Both of the two rollers include a radial fixing part and a radial extension part; the tip of the sawtooth located on the outer wall of the radial extension part is provided with a pressure sensor electrically connected to the controller. The invention can solve the problems of inaccurate particle size control and inconvenient operation of existing roller crushers.

The invention discloses a method for preparing granularity controllable narrow range polymer micro-nano spheres. The granularity controllable narrow range polymer micro-nano spheres can be efficiently and continuously produced at normal temperature by using industrial grade polydisperse polymer products, recovered polymer materials, homopolymers and copolymers which are wide in source as raw materials by virtue of a two-step production process of mechanical stirring-micro jet flow. In a preparation process, the proportion of a dispersed phase to a continuous phase, the type and use level of surfactants and compounding schemes of types of organic solvents and high pressure chamber of the device are adjusted without high-temperature time-consuming polymerization reaction and cockamamie post-treatment as well as purification of raw materials, so that the grain size and grain size distribution of the micro-nano spheres can be controlled. The diameters are adjustable from 30nm to 3mu m, the polydispersity index is less than 0.2, and the micro-nano spheres are smooth and non-adhesive on the surfaces and can be re-dispersed in a solvent. The obtained polymer micro-nano spheres have a wide application range in the fields of standard metering, food industry, medicines, bioengineering, coating and plastic processing and the like.

The invention discloses a generating method and device capable of adjusting particle size of atomized single liquid drops in the electrostatic atomization field. The device is characterized in that aliquid storage tank is connected to a metal capillary through a guide pipe and is in communication with the metal capillary, and a flow control valve and a flow meter are arranged on the guide pipe; adevice support comprises two square plates which are parallel to each other, and the metal capillary extends into an atomization area from the upper portion of the device support through a through hole in the upper square plate; a capillary support is tightly sleeved outside the upper section of the metal capillary, and the capillary support is connected to a high-voltage electrostatic generatorthrough a wire; and a lifting platform is arranged right below the metal capillary in the atomization area, a metal round copper plate is horizontally placed in the middle of the upper surface of thelifting platform, and the metal round copper plate is connected to the high-voltage electrostatic generator through the wire. According to the generating method and device capable of adjusting particle size of atomized single liquid drops, the action characteristic of the surface tension of the liquid is reduced through static electricity, the liquid drops are crushed into fine liquid drops, the particle size distribution of the atomized liquid drops is controlled through adjusting the voltage, the flow, the size of the polar distance and the specification of the metal capillary, and equal-particle-diameter atomized single liquid drops are generated.

The invention discloses a polymer nanosphere with a function of target recognition of cancer cells and a preparation method of the polymer nanosphere. The polymer nanosphere comprises polymer nanospheres with surfaces containing amino groups and aminated cancer cell target-mediated molecules, wherein the aminated cancer cell target-mediated molecules are fixedly arranged on the surfaces of the polymer nanospheres containing the amino groups through hydrogen bonds formed by the amino groups in the aminated cancer cell target-mediated molecules and the amino groups in the polymer nanospheres containing the amino groups. The polymer nanosphere prepared by virtue of the preparation method can be used as a drug carrier for coating anti-cancer drugs, and the nanosphere carriers have no cytotoxicity; and the aminated cancer cell target-mediated molecules are fixedly arranged on the surfaces of the nanospheres through the hydrogen bonds, and after the nanospheres are sent into a body in an intravenous injection or oral manner, the nanosphere carriers can be aggregated in a targeted manner adjacent to cancer cells so as to release drugs, so that the drug concentrations of local regions of the cancer cells are increased, and the targeted killing of the cancer cells is realized.

The invention discloses passivating metal magnesium particles and a passivating method thereof. The passivating metal magnesium particles comprise the following components in percentage by weight: less than or equal to 99% and greater than or equal to 92% of Mg, less than or equal to 0.002% of S, less than or equal to 0.01% of Cu, less than or equal to 0.001% of P and less than or equal to 1.2% and greater than or equal to 0.1% of H2O. The passivating method comprises the following steps: (I), preparing a metal magnesium particle passivator, placing metal magnesium particles in the passivator, and then naturally cooling to room temperature; (II), coating a coating on the surface of the magnesium particles: firstly, coating an organic silicon compound on the surface of the metal magnesium particles, coating magnesium oxide on the surface of the metal magnesium particles, then, coating compound rare earth on the on the surface of the metal magnesium particles, and finally coating graphite powder on the surface of the metal magnesium particles; and (III), sieving the metal magnesium particles cooled to room temperature. The metal magnesium particle passivating layer is uniform in coating, and the storage and use safety is ensured.

A method for preparing concave cubic platinum-rare earth alloy nanocrystals based on a eutectic solvent is disclosed, and belongs to the technical field of fuel cell catalyst preparation. The eutecticsolvent which is novel, green and non-aqueous is adopted as a medium to prepare the concave cubic platinum-rare earth alloy nanocrystals with a surface of a {hk0} high-index crystal face structure byelectrochemical cyclic voltammetry without the need of any surfactant. The high-index crystal face has an open type surface structure so that a high number of active sites can be provided and catalyst performance can be significantly improved through a double-function mechanism of an alloyed surface electron structure, and therefore, the nanocrystals have excellent electrocatalytic performance for fuel molecules such as formic acid, methanol and ethanol, and have broad application prospects in the field of fuel cells, the field of electrosynthesis, and the like.

The invention discloses a method for preparing a novel polyethylene glycol-poly gamma butyrolactone (PEG-PBL) di-block copolymer nano drug carrying microsphere. The provided PEG-PBL copolymer copolymer nano drug carrying microsphere has a small particle size, is narrowly distributed, has a high drug carrying capacity, can be slowly released for a long time, and can reduce the drug delivery frequency. In addition, according to results of biological evaluation, it is proved that the polyethylene glycol-poly gamma butyrolactone di-block copolymer nano drug carrying microsphere has excellent biocompatibility and anticancer activity. The provided novel polyethylene glycol-poly gamma butyrolactone di-block copolymer nano drug carrying microsphere has a simple preparation method, is easily produced on a large scale, and has broad application prospects in the field of drug slow release.

The invention relates to a method for preparing large-particle high-purity vanadium pentoxide. The method comprises the following steps: after dissolving ammonium metavanadate, adding an impurity removing agent; regulating the pH (Potential of Hydrogen) of a solution to 6.5 to 8.2 and carrying out vanadium dissolving; after the vanadium dissolving is finished, carrying out solid-liquid separationto obtain a vanadium-contained purification solution; heating the vanadium-contained purification solution; then regulating the pH to 6 to 5.8, 5.7 to 5.4, 4.8 to 4.0 and 2.4 to 1.9 in sequence at four phases and carrying out gradient vanadium deposition; after vanadium deposition is finished, carrying out the solid-liquid separation to obtain a vanadium deposition mother solution and solid-phaseammonium polyorthovanadate; carrying out calcination and deamination on the ammonium polyorthovanadate to obtain a vanadium pentoxide product with the purity of greater than or equal to 99.95 weight percent and the granularity of greater than or equal to 150mum. According to the method provided by the invention, a vanadium dissolving and gradient vanadium deposition method is adopted and impurityelements are greatly removed; meanwhile, the granularity of the vanadium pentoxide is accurately controlled, so that the content of particles with the size in a range of 180 to 230mum is greater thanor equal to 60 percent; the requirements of customers are met and the method has a good application prospect.

The invention provides catalyst particles for air purifiers and a method for forming the same by means of layer-by-layer cladding. The method includes acquiring core-shell structures by means of layer-by-layer cladding in particle forming procedures; manufacturing cores from selective clay mineral materials; cladding catalysts on the outsides of the cores; cladding safe and harmless inorganic porous materials such as activated carbon on the outermost layers of the cores by the aid of non-perishable inorganic adhesive in cladding procedures to obtain the spherical catalyst particles. The safe and harmless inorganic porous materials are used as framework materials. The spherical catalyst particles have uniform particle sizes, are high in catalytic activity and are non-perishable and non-mildew when stored at the room temperature for a long time The catalyst particles and the method have the advantages that the material adding speeds are automatically controlled, so that the uniformity of particle structures can be guaranteed; the spherical catalyst particles prepared by the aid of the method are high in catalytic efficiency, are non-perishable, have the uniform particle sizes and are safe and healthful.

The invention discloses a chain plate type powder sorting machine and belongs to the technical field of mine equipment. The chain plate type powder sorting machine comprises a driving wheel, a driven wheel and a transmission chain, wherein the transmission chain is assembled on the driving wheel and the driven wheel and is arranged in an inclined way; a plurality of sorting gas chambers are formed in the surface of the transmission chain and are connected with a gas distribution device through gas pipes; the gas distribution device is connected with a gas source; a feeding hole is formed above the working surface of the transmission chain ; a coarse powder discharging hole is formed below the low end of the inclination surface of the transmission chain; a fine powder discharging hole is formed below the high end of the inclination surface of the transmission chain. According to the chain plate type powder sorting machine, fine powder with any particle size can be sorted by adjusting the pressure of gas and the inclination angles of the sorting gas chambers, so that the stepless sorting of materials on the same machine is realized. Compared with a powder sorting machine, the chain plate type powder sorting machine has the advantages that not all materials need to be blown, and fine powder collecting equipment is not needed, so that the energy consumption is greatly reduced.

The invention discloses flower-like CuS submicron spheres and an ionic liquid microemulsion thermal synthesis method thereof. The synthesis method mainly comprises the following steps: (1) adding a sulfur source into an ionic liquid, and heating, stirring and dissolving to obtain a mixture A; (2) uniformly mixing and stirring bivalent copper salt, a surfactant, a cosurfactant and vegetable oil toobtain a mixture B; (3) uniformly mixing and stirring the mixture A and the mixture B to obtain a microemulsion C; (4) transferring the microemulsion C into a hydrothermal reaction kettle with a polytetrafluoroethylene lining, sealing, placing at the temperature of 60-160 DEG C, carrying out a reaction for 2-24 h, and naturally cooling at room temperature to obtain a black solution; and (5) separating, washing and drying the black solution to obtain the final product black powder. The CuS particles prepared through ionic liquid microemulsion assisted thermal synthesis are of a flower-like submicron sphere structure, and are large in specific surface area, regular in morphology, uniform in size, high in crystallinity and high and stable in photocatalysis efficiency.

The invention provides a lipidosome extruding and filtering device which comprises a material discharge pipe, an upper cover, an extruding outer seal gasket, a support plate, a filtering plate, a filtering membrane, an extruding inner seal gasket, a connector, a hoop and a hoop locking bolt; the center of the connector is provided with a material charge through hole; the center of the upper cover is provided a material discharge through hole of which the opening at the upper end is connected with the material discharge pipe; the bottom surface of the upper cover is provided with an annular seal groove and an internally sinking cylindrical groove; the support plate, the filtering plate, the filtering membrane and the extruding inner seal gasket are sequentially arranged in the cylindrical groove from inward to outward; the extruding outer seal gasket is arranged in the annular seal groove; the upper cover and the connector are fixed together through the hoop and the hoop locking bolt. According to the invention, nanocrystallized equipment and homogenized equipment are designed integrally; material particle size can be controlled accurately through replacing different filtering membranes; cross contamination is prevented; and the lipidosome extruding and filtering device is convenient to use, and can be widely applied to the nano medicament field.

The invention belongs to the technical field of functional material preparation, and discloses a method for reducing the supercooling degree of an alkane phase change microcapsule by using different shell materials, the microcapsule prepared by the method and application of the microcapsule. The method comprises the following steps: preparing an intermediate phase, a continuous phase and a collection phase, respectively feeding a dispersed phase, the intermediate phase and the continuous phase into a micro-fluidic chip through an injection pump, and respectively introducing the dispersed phase, the intermediate phase and the continuous phase into the micro-fluidic chip from a small sharp-nose glass capillary tube, a first closed liquid storage tank and a second closed liquid storage tank; enabling the dispersed phase to flow out of the small sharp-nose glass capillary tube, to be wrapped by the intermediate phase and then flow into the small sharp-nose glass capillary tube under the flowing of the continuous phase, radiating an initiator in the intermediate phase by an ultraviolet lamp to initiate a polymerization reaction of a shell material, forming a thin film layer to wrap the phase change material, and obtaining the phase change microcapsule after drying. Precision control over particle size control and supercooling degree reduction of the phase change microcapsules is achieved, and the method is suitable for industrial production of the phase change microcapsules.

The invention discloses an adjustable solid material continuous feeding and discharging grinding method and device. A feeding shaft is driven by a driving mechanism to rotate, a feeding strip on the feeding shaft coarsely crushes materials entering a shell, and then the coarsely crushed materials are fed into a grinding disc and an adjustable grinding disc through feeding holes; and the materialsare further crushed through relative rotation of the grinding disc and the adjustable grinding disc. The adjustable solid material continuous feeding and discharging grinding method and device provided by the invention are applied to the preparation process of coal or mineral particles and used for obtaining the coal or mineral particles with a certain particle size. Collision between metal objects is avoided in the preparation process of a coal sample, and the device is small in size, low in noise in the working period and high in sample preparation efficiency. By accurately adjusting the distance between grinding faces, collision between the grinding faces is avoided, and meanwhile the maximum particle size of ground material particles can be accurately controlled.

The invention relates to the field of materials, particularly to a production process of a foamed ceramic thermal insulation board by recycling ceramic fiber paper. The process comprises: mixing and grinding, drying, firing, and cooling, wherein in the firing step, the temperature of a firing furnace on the inner wall of the firing furnace is kept by using ceramic fiber paper to obtain waste ceramic fiber paper, and in the step of mixing and grinding, the waste ceramic fiber paper is added into raw materials. According to the invention, thermal insulation is performed by using ceramic fiber paper in a firing process so as to reduce energy consumption, and the fired waste ceramic fiber paper is added into raw materials, so that waste is utilized, and the mechanical strength of the foamed ceramic thermal insulation board can be improved.

The embodiment of the invention discloses a method and device for adjusting the vibration frequency of an ore feeder in the ore grinding process. The method comprises the steps that according to the actual feeding quantity which is detected and stored in advance, the deviation ratio that the current feeding quantity deviates from the control feeding quantity is calculated; according to the numerical range of the deviation ratio, a current constraint period corresponding to the deviation ratio is determined; whether time lasting from the moment when the current vibration frequency of the ore feeder is adjusted at the last time to the current moment is longer than the time of the current constraint period or not is judged, if the answer is positive, the current vibration frequency is adjusted according to the deviation ratio, and if the answer is negative, the current vibration frequency is not adjusted at the current moment. According to the technical scheme, excessive adjustment to the current vibration frequency can be avoided and the actual feeding quantity of an ore grinding chamber is prevented from being over adjusted and deviating from the control feeding quantity, so that accurate control over the feeding quantity of the ore grinding chamber is achieved and accurate control over granularity of ground ore is indirectly achieved.