30results about How to "Process pollution is small" patented technology

The invention relates to a preparation process of high-purity 4-chloro-2-pyridinecarboxylate hydrochloride, which comprises the following steps of reacting 2-methyl-4-nitropyridine-N-oxide taken as a starting raw material with hydrochloric acid to obtain 4-chloro-2-methyl-pyridine-N-oxide; then dripping phosphorus trichloride into an organic solvent, carrying out reaction for generating 4-chloro-2-methylpyridine, further adding potassium permanganate into water for carrying out oxidation reaction, thus obtaining 4-chloro-2-picolinate; and mixing the 4-chloro-2-picolinate with the catalytic amount of DMF (dimethyfumarate), dripping thionyl chloride, and finally carrying out esterification reaction with methanol so as to obtain the 4-chloro-2-pyridinecarboxylate hydrochloride. The total yield can be up to 36.8%, and the purity can be 99.8% according to the HPLC (high performance liquid chromatography) detection. The process has the advantages of being rich in raw material resources, small in whole process pollution, conductive to controlling three wastes and easy for realizing industrial production.

The invention relates to a preparation method for a basalt fiber conveying belt, and belongs to the technical field of rubber products. The preparation method comprises the following steps: performing hydrochloric acid treatment, coupling agent treatment and plasma grafting and impregnation treatment on basalt fiber cloth; mixing natural rubber, synthesized rubber, an activating agent, an anti-aging agent, a reinforcement agent and a plasticizer to obtain a first section of mixed rubber; adding a promoter and a vulcanizer for mixing to obtain a second section of mixed rubber, and extruding the second section of mixed rubber to obtain a coverage rubber sheet; mixing the natural rubber, the synthesized rubber, the activating agent, the anti-aging agent, an adhesive, the reinforcement agent and the plasticizer to obtain a first section of mixed rubber; then adding the promoter, the vulcanizer and an adhesive RA for mixing to obtain a second section of mixed rubber, freshening after the second section of mixed rubber is stewed, and attaching the second section of mixed rubber and the basalt fiber cloth to obtain rubberized canvas; attaching the basalt fiber rubberized canvas layer by layer to obtain a framework, attaching the coverage rubber sheets to the upper surface and the lower surface of the framework to obtain a belt blank, and vulcanizing the belt blank to obtain the basalt fiber conveying belt. The conveying belt prepared by the preparation method is low in cost, light in mass, high in intensity, fatigue-resistant and long in service life; the conveying energy consumption can be greatly reduced.

The invention relates to a method for extracting high-purity scutellarin from breviscapin. The method comprises the following steps: the breviscapin raw material is extracted by using organic solvent, the filtrate is added with clarifying agent for coagulation and clarifying, the coagulated and clarified filtrate is absorbed by macroporous absorbent resin and is eluted with water, the water eluent is concentrated through a reverse osmosis membrane or nanofiltration membrane, the concentrated solution is added with the organic solvent for standing and precipitation, the sediment is filtered and collected, the aqueous solution of the organic solvent is added and stirred to be suspendible, and after standing a night, the sediment is filtered, collected and washed to be near-neutral with water to obtain the high-purity scutellarin after drying. The alkali is not used in the entire process, the clarifier is used for removing the water insoluble matter, the impurity removal is carried out by using the macroporous absorbent resin, the concentration is carried out by using the reverse osmosis membrane or the nanofiltration membrane, the scutellarin plant salt is prevented from being heated and degraded in water, the content of the prepared scutellarin can reach above 97 percent, the quality is stable, the process is simple and the pollution is little.