2results about How to "Reduce density difference" patented technology

This invention discloses a large-size molybdenum-titanium alloy target and its preparation method. The preparation method includes the following steps: S1, selecting raw materials molybdenum powder and titanium powder; S2, granulating the molybdenum powder under inert gas protection to prepare granulated molybdenum powder, wherein the particle size and tap density of the granulated molybdenum powder are matched with those of the titanium powder; S3, mixing the granulated molybdenum powder and titanium powder in a certain proportion under inert gas protection; S4, degassing the mixed powder; S5, hot isostatic pressing to form an ingot; S6, vacuum heat treatment of the ingot to obtain the large-size molybdenum-titanium alloy target. By adding the granulation and forming process of molybdenum powder, the morphology of the raw materials is controlled, effectively suppressing the tendency of the mixed powder to separate in subsequent processing. This method significantly improves the compositional uniformity and batch stability of the molybdenum-titanium alloy target, avoids product defects and scrap due to separation, thereby reducing production costs and improving product qualification rate.

This invention belongs to the field of directional solidification of high-temperature alloys, and provides an engineering-applicable anti-gravity effect single-crystal high-temperature alloy directional solidification growth device and its application, which reduces the formation of interdendritic segregation, avoids the formation of defects such as freckles, and meets the actual needs of high-temperature alloy directional solidification blade preparation. The device structure is as follows: a vacuum induction furnace is set at the bottom of the device, and a crucible is placed inside it. The crucible is located on a crucible lifting mechanism, and a graphite holding furnace is set above the crucible. A pulling mechanism is set at the top of the device, and a water-cooling plate is set below it. The top of the mold shell has a seed crystal mounting port for installing the seed crystal, and the bottom has an alloy liquid inlet. After the mold shell and the seed crystal are assembled, they are fixed on the water-cooling plate by a fixing clamp. The device also includes a heat insulation baffle and a vacuum system. The heat insulation baffle with through holes is set parallel to the crucible above the graphite holding furnace, and the inner diameter of the through holes of the heat insulation baffle is 10-20 mm larger than the maximum outer diameter of the mold shell.