93results about How to "Reduce heat treatment process" patented technology

This method for manufacturing a high resistivity silicon wafer includes pulling a single crystal such that the single crystal has a p-type dopant concentration at which a wafer surface resistivity becomes in a range of 0.1 to 10 kΩcm, an oxygen concentration Oi of 5.0×10¹⁷ to 20×10¹⁷ atoms/cm³ (ASTM F-121, 1979), and either one of a nitrogen concentration of 1.0×10¹³ to 10×10¹³ atoms/cm³ (ASTM F-121, 1979) and a carbon concentration of 0.5×10¹⁶ to 10×10¹⁶ atoms/cm³ or 0.5×10¹⁶ to 50×10¹⁶ atoms/cm³ (ASTM F-123, 1981) by using a Czochralski method, processing the single crystal into wafers by slicing the single crystal, and subjecting the wafer to an oxygen out-diffusion heat treatment process in a non-oxidizing atmosphere. A peak position of a resistivity serving as a boundary between a p-type region of a wafer surface side and a p/n conversion region of an inner side of a thickness direction is adjusted by the nitrogen concentration or the carbon concentration such that the peak position is set to a boundary depth in a range of 10 to 70 μm from the wafer surface.

The invention relates to a method for preparing a low carbon 9 nickel steel thick plate, the steps are that: steelmaking, the components which are weighted by weight percentages are that carbon is 0.02-0.04 percent, silicon is 0.2-0.3 percent, manganese is 0.4-0.7 percent, sulfur is equal or less than 0.005 percent, phosphorus is equal or less than 0.01 percent, nickel is 8.9-9.5 percent, the allowance is ferrum and impurities, and the components are made into steel. Red charge: molten steel is cast and is stood for 5 minutes and is red charged into a heating furnace. Hot rolling: module ingots are rolled in two stages. On-line heat treatment: when finish rolling temperature is in a dual-phase region, quenching after rolling and tempering heat treatment are used, when the finish rolling temperature is in an austenite region, the quenching after rolling, quenching after solid solution and the tempering heat treatment are used or the quenching after rolling, the quenching after solid solution, dual-phase region quenching and the tempering heat treatment or the quenching after keeping temperature in the dual-phase region for 10-20 minutes are used, and then water-cooling is done after tempering whose temperature is kept for 1 hour in 580 DEG C. The invention has the advantages of short technological process, low producing cost, and high low-temperature flexibility and other mechanical properties of 9 nickel steel.

The invention relates to a method for preparing a copper-coated aluminium composite material. The method comprises the following steps: spinning the head of a copper tube which is utilized as a raw material to form a cone, turning the head of the aluminium bar which is utilized as a raw material to form a cone, mechanically polishing the aluminium bar and then sleeving the aluminium bar with the copper tube to form an extrusion billet; coating a colloidal graphite lubricating film on the exterior of the extrusion billet and carrying out copper and aluminium soldering and sealing on the tail of the extrusion billet; ensuring the container temperature of a hot hydrostatic extruder to be 350-450 DEG C, the temperature of an extruding die to be 150-350 DEG C, the temperature of the copper tube forming the extrusion billet to be 350-450 DEG C and the temperature of the aluminium bar to be 150-250 DEG C; and feeding the extrusion billet into the container, filling extrusion media and then carrying out hydrostatic extrusion, thus obtaining the copper-coated aluminium composite material, wherein the internal diameter of the copper tube is the same as the external diameter of the aluminium bar; and the extrusion ratio is 4-100. The method has the following beneficial effects: the copper-coated aluminium composite material prepared by the method has high copper/aluminium interface bond strength and good bending and forming performance; the frequency of annealing needed in the preparation process is low and the annealing temperature is low; and the production procedure is simplified and the production cost is lowered.

The present invention relates to one kind of health beverage prepared with several kinds of vegetable and fruit. The composite vegetable and fruit juice of the present invention is produced through processing vegetables and fruits into concentrated juices; mixing juices of carrot, celery, Chinese cabbage, cabbage, rape, apple, orange, red tangerine, etc in certain weight proportion; blending, filtering, preheating, deairing, homogenizing and high pressure instantaneous sterilizing. The beverage of the present invention has rich nutrients, good flavor and scent of vegetable and fruit and good taste.

The present invention relates to a nano-material interalloy modifier and a preparation method thereof, and an alloy preparation method. The nano-material interalloy modifier comprises the following components, by mass, 5-15% of nano-powder, 1-3% of magnesium powder, 30-40% of sodium potassium ore powder, 40-50% of iron powder, 3-8% of hydroxypropyl cellulose, and 2-4% of water. The nano-material interalloy modifier is not easily oxidized and polymerized during processes of mixing and preparation, has a sufficient strength, is not easily decomposed during using and transportation, and can be rapidly molten when the nano-material interalloy modifier is added to a liquid steel, hot iron, or a nonferrous alloy liquid.

The invention provides a preparation method for a high-toughness 3.5Ni steel plate in order to reduce the production cost and belongs to the field of alloy steel manufacture. The preparation method comprises the steps that (1) hot rolling is conducted, a casting blank is put into a heating furnace with the temperature of 1150 DEG C-1200 DEG C for heat preservation for 1-2 h, the casting blank comprises, by weight, 0.04%-0.07% of C, 0.10%-0.25% of Si, 0.60%-0.90% of Mn, 0-0.005% of S, 0-0.008% of P, 0 or 3.3%-3.8% of Ni, 0-0.60% of Cr, 0-0.04% of Mo, 0.02%-0.05% of Alt and the balance Fe and impurities; two-stage rolling is adopted for hot rolling, and the total compression ratio of the steel plate is the thickness of the casting blank/the thickness of a finished product>=5.00; and (2) direct hot rolling is conducted, the rolled steel plate is quenched directly or after the relaxation for 10-20 s to below 300 DEG C through ultra fast cooling at the speed of larger than or equal to 20 DEG C/s, then the plate is put into a heating furnace with the temperature of 570 DEG C-620 DEG C for heat preservation, after that, the product is obtained after the steel plate is cooled through water or air to the room temperature. According to the preparation method, direct quenching and tempering processes are adopted, so that the process flow of hot treatment is shortened, and the cost is lowered; in addition, the austenite grain size is refined by controlling the rolling process, and the low-temperature toughness and other mechanical properties of 3.5Ni steel are significantly improved.

A solar cell including a first conductive type semiconductor substrate; a first conductive type first semiconductor layer on a back surface of the semiconductor substrate; a second conductive type second semiconductor layer on the back surface of the semiconductor substrate at a height different from the first semiconductor layer, the second semiconductor layer being separated from the first semiconductor layer; and a passivation layer on the back surface of the semiconductor substrate. The passivation layer covers at least a portion of the first semiconductor layer and at least a portion of the second semiconductor layer. The passivation layer includes impurities.

The invention relates to a medium carbon steel plate bell-type furnace spheroidizing annealing method, which orderly comprises the following steps that: (1) a hot-rolled blank steel coil is subject to the cutting and acid cleaning; (2) the longitudinal rolling is adopted, and the rolling deformation is between 28 and 41 percent; (3) the single sheet stack annealing is adopted, and a steel plate is loaded into an electric heating bell-type furnace; wherein, a. a plate temperature thermocouple is adopted to control the temperature, and at least two armored thermocouples are inserted; b. the heating in the furnace adopts two-section type furnace platform and furnace mantle resistance bands; c. protective gas in the furnace platform and the furnace mantle is nitrogen; d. after the steel sheet is loaded into the furnace, a safety cover and a heating mantle are fastened to electrify and increase the temperature for 60 to 70 hours, the heat preservation is performed for 4 to 6h when the temperature is increased to between 690 and 720 DEG C, and the surface temperature of the steel plate is less than or equal to 720 DEG C during the heat preservation; e. then the heating mantle is hoisted away to cool naturally, and the steel plate is taken out of the furnace when the temperature of the core of the steel plate is cooled to be below 250 DEG C. The medium carbon steel plate bell-type furnace spheroidizing annealing method adopts one-time annealing, and the spheroidizing qualification rate of metallurgical structures is apparently improved.

The invention discloses a hot-rolled wire rod for manufacturing a high-strength steel strand of a strong and smart grid and a production method of the hot-rolled wire rod, and relates to a hot-rolled wire rod for manufacturing a high-strength steel strand of a grid. Chemical composition of the hot-rolled wire rod is composed of the following substances in percentage by weight (%): 0.70-0.74% of C, 0.17-0.37% of Si, 0.70-0.80% of Mn, 0.07-0.14% of Cr, less than or equal to 0.025% of P, less than or equal to 0.025% of S, less than or equal to 0.30% of Ni, less than or equal to 0.25% of Cu and the balance of Fe. According to the phi6.5mm hot-rolled wire rod produced by the method disclosed by the invention, tensile strength is 1120-1200Mpa, area reduction is 40-50% and percentage of elongation is more than or equal to 18%. The hot-rolled wire rod disclosed by the invention has the advantages that process equipment and parameter setting are reasonable, longstanding problems are solved and product quality is improved; the wire rod is drawn into a steel wire to enhance strength, and a loading bearing capacity of a steel strand processed from the steel wire is greatly improved; and the hot-rolled wire rod is easy to draw, and capable of avoiding an intermediate heat treatment process and saving energy.

The invention relates to and aims at providing a method for producing a high-strength titanium alloy seamless tube and belongs to the field of metallurgy. The method for producing the high-strength titanium alloy seamless tube sequentially comprises the following steps: heating a round billet, perforating, sizing, carrying out hydraulic drawing and temperature correcting, and the like, thereby obtaining the titanium alloy seamless tube finally. The method for producing the high-strength titanium alloy seamless tube has the advantages that deformation at the medium temperature of 750-850 DEG C is increased to directly obtain the titanium alloy tube meeting performance requirements, a heat treatment process is eliminated, and the aims of simplifying working procedures, optimizing a technology, reducing cost, shortening a production cycle, improving production efficiency and improving product quality are achieved. The titanium alloy tube produced by the method has the advantages of thin gas permeable layer, high outer diameter and wall thickness dimensional accuracy, few inner and outer surface defects, high yield and the like. The method provides a new choice for production of the titanium alloy tube and has broad application prospects.

The invention discloses high-toughness quantitative-reduction ship plate marine steel. A steel plate comprises the following chemical components by weight percent: 0.04%-0.14% of C, 0.15%-0.45% of Si,0.90%-1.50% of Mn, less than or equal to 0.015% of P, less than or equal to 0.010% of S, 0.010%-0.040% of Nb, 0-0.20% of Cr, 0-0.030% of V, 0.005%-0.020% of Ti, 0.015%-0.050% of Als, less than or equal to 30 ppm of N, less than or equal to 30 ppm of O, less than or equal to 2 ppm of H, and the balance Fe and inevitable impurities, wherein Als is acid-soluble aluminum; a welding crack sensitivityindex (Pcm) of the steel plate is less than or equal to 0.22%; and a carbon equivalent value (CEV) is less than or equal to 0.39%. The steel plate is not liable to be broken and damaged, and has goodstrength and toughness, welding performance and crack arrest performance.

The invention discloses a preparation method for a polycrystal/monocrystal-like solar cell selective emitting electrode structure. The preparation method for the polycrystal/monocrystal-like solar cell selective emitting electrode structure comprises the following steps: (1) chemically removing a surface energy affected layer; (2) carrying out heavy doping by the one-time diffusion technology to form a PN junction; (3) growing or forming a dielectric layer or a mask layer on the surface of a silicon wafer; (4) corroding the dielectric layer of a non-electrode grid line area with a chemical corrosion method, and keeping the mask layer under an electrode grid line area; (5) etching a pyramid matte structure of 100-300nm in the non-electrode grid line area by reactive ion etching (RIE), and meanwhile, forming a shallow doped area in one time; and (6) removing a surface affected layer formed by RIE and a lower mask layer under the electrode grid line area with a wet chemistry method to obtain the selective emitting electrode structure. According to the preparation method for the polycrystal/monocrystal-like solar cell selective emitting electrode structure, which is disclosed by the invention, the light doping and the heavy doping required by the selective emitting electrode polycrystal/monocrystal-like solar cell and a low-reflectivity nanoscale surface texture can be finished by one-time diffusion combined with the RIE technology, the process path is simplified, the conversion efficiency is high, and the preparation method for the polycrystal/monocrystal-like solar cell selective emitting electrode structure is suitable for industrial volume production.

The invention relates to a method for producing a significant-purpose steel wire for manufacturing a rope. The method comprises the following production processes: coiling, performing acid pickling rusting, pulling a half-finished product, performing EDC coiling, pulling a finished product steel wire, and inspecting the steel wire, and comprises the following production steps: (1) after the half-finished product is pulled, performing EDC coiling, soaking a coiled strip in an austenite state into water and cooling rapidly, thereby obtaining austenite texture, wherein the austenite rate is 85-95%; and (2) according to a Linhof equation as shown in the specification, enabling the strength of the finished product steel wire and the strength of a raw material are in a linear relationship, wherein the pull resistance sigma c of the EDC coiled strip is 1050-1120Mpa. The method has the advantages that the experiment shows that the significant-purpose steel wire which is pulled by using the method and is used for manufacturing the rope can meet relevant requirements in the national standard (YB/T5343-2009). The technical indexes of the product completely meet the national standard and use requirements.

The invention discloses a progress regulation method of an automotive high-formability aluminum alloy heterogeneous structure, and belongs to the technical field of aluminium alloy. The progress regulation method comprises the following steps of configuring the automotive high-formability Al-Mg-Si-Cu-Zn alloy, smelting the alloy through medium-frequency induction in non-vacuum, and casting the alloy in a cold cooling steel die for cooling; performing short-time low-temperature structure stability treatment; taking out an ingot heated in short time from a heating furnace, and directly performing hot rolling treatment; performing two-stage thermal treatment to regulate the distribution state of alloy primary iron-rich phase and a solute element; performing hot rolling, cold rolling, intermediate annealing and cold rolling treatment in sequence; performing high-temperature short-time solid-solution treatment, and then carrying out quench cooling on the alloy test sample subjected to solid-solution treatment from the solid-solution treatment temperature to room temperature; and transferring a quenched test sample in an ageing furnace for cooling and preliminary ageing treatment. The treatment method can effectively control the crystal grain in the alloy and the size and the distribution of a precipitating phase, and the heterogeneous structure having remarkable prompting effects onthe alloy formability is formed.

The invention provides a casting method of bi-metal for a plunger pump rotor and belongs to the technical field of bi-metal casting. The casting method comprises the following steps: machining a steelsubstrate; pretreating the steel substrate; carrying out a heat-treatment annealing process on the steel substrate; carrying out Ni-Cu-P multi-component nickel plating on the inner surface of the steel substrate; preheating the steel substrate; smelting a lead-tin bronze alloy; casting the lead-tin bronze alloy; and machining the plunger pump rotor. A bi-metal binding surface obtained by adoptingthe casting method provided by the invention has the advantages that not only do the properties reach the standards, but also the equipment investment is low, the process operation is simple and convenient, and the workpiece cost is reduced; the casting method is suitable for extensive popularization and application, and has broad prospects; and compared with a powder metallurgy method, the casting method has the advantages that the performance is superior, the heat treatment procedure is eliminated, the time is saved, and the cost is reduced.

The invention relates to smelting equipment and a smelting method. Specifically, the smelting equipment includes: a crystallizer; an ingot pulling mechanism, which is connected to the bottom of the crystallizer; a vibrating mechanism, which is suitable for vibration of the ingot pulling mechanism. The equipment and method provided by the invention simplify the metal grain refinement process whilereducing the grain size of the ingot, make the later TMP (plastic deformation and recrystallization process) operation simple, and also reduce the heat treatment procedure and equipment investment, thereby substantially lowering the production cost.

The invention provides an opposite roller spinning and deformation heat treatment combined manufacturing process for large bellows. The deformation heat treatment mode is used in an opposite roller spinning process, and novel internally and externally rotated roller sets provided with one or more corrugation shapes are used for spinning corrugation sequentially under the condition of local heating. The manufacturing process can process the bellows with large diameter, large wall thickness and high strength and has the characteristics of high processing capability and high adaptability.

The invention discloses transparent Ce:YAG microcrystalline glass and application of the transparent Ce:YAG microcrystalline glass in a white LED. The microcrystalline glass is self-crystallized, and is prepared from the following active materials in percentage by mole: 19-30mol% of SiO2, 15-30mol% of Al2O3, 5-20mol% of Y2O3, 40-60mol% of PbO, 0.5-5mol% of CeF3 and 2-10mol% of B2O3, wherein the sum of the mole percentage of the components is 100 percent. The Ce:YAG microcrystalline glass disclosed by the invention meets the requirements that the glass melting temperature is low, a preparation method is simple, the raw materials are readily available, the production cycle is short, the batch production is easily realized, and the glass is stable in physicochemical properties, high in uniformity, long in service life and high in heat conductivity; and moreover, the Ce:YAG microcrystalline glass emits bright yellow light under blue light excitation of 465nm, the yellow light and blue light are combined to generate strong white light, and the microcrystalline glass can be used for preparing the white LED.

The invention discloses a steel wire for an aerial cable steel core with a spanning degree not smaller than 3500m and a production method thereof. The steel wire comprises the following components in percentage by weight in terms of content: 0.79-0.84% of C, 0.70-0.90% of Mn, 0.15-0.30% of Si, not more than 0.01% of P, not more than 0.01% of S, 0.28-0.35% of Cr, and 0.015-0.035% of V. The production method comprises the steps of: selecting a wire rod with the diameter being 9-11mm and the tensile strength not lower than 1180MPa; carrying out acid washing and phosphating treatment on the wire rod; drawing the wire rod; and galvanizing the drawn wire rod to obtain a steel wire for later use. According to the galvanized steel wire with phi being 2.70-4.60mm, produced according to the invention, the wire rod is directly drawn without undergoing lead hardening treatment, so that the pollution to the environment is reduced, thermal treatment procedures such as the lead hardening and the like as well as corresponding equipment maintenance works are reduced; and in addition, under the condition of simple components, the steel wire is at least 1900MPa in tensile strength, at least 1600MPa in 1% elongation stress and at least 20 in torsion number.

The invention relates to a welding technique of a back suspension fork of an automobile; a reinforced plate is connected with a dragging arm; the invention is characterized in that the head part of a welding line is welded with a smooth arc and then is transited to the bottom side of the dragging arm; the welding technique of the invention has the advantages of removing the heat treatment after the welding and eliminating welding residual stress of the welding joint of the reinforced plate, thereby simplifying the technique during manufacture, being easy to control the quality, improving the fatigue strength of a product and reducing the manufacturing cost.

The invention relates to 100 mm-120 mm Q460D extra-thick high-strength steel which comprises the following chemical components including, by mass, 0.10% to 0.13% of C, 0.30% to 0.50% of Si, 1.40% to 1.60% of Mn, less than or equal to 0.0070% of P, less than or equal to 0.0020% of S, 0.020% to 0.050% of Nb, 0.008% to 0.020% of Ti, 0.020% to 0.040% of Al, 0.10% to 0.20% of Cu, 0.10% to 0.20% of Cr, 0.10% to 0.20% of Ni and the balance Fe and inevitable impurity elements. The production process flow comprises the following steps of converter smelting, LF refining, RH vacuum degassing, Ca treatment, continuous casting, casting blank dehydrogenation treatment, heating, normalizing rolling, air cooling, steel plate stacking and slow cooling and unstacking. The yield strength of a steel plate ranges from 430 MPa to 470 MPa, the tensile strength ranges from 550 MPa to 570 MPa, the ductility is larger than or equal to 20%, and the Charpy impact energy at the 1/4 position and the 1/2 position of the thickness of -20 DEG C is larger than or equal to 200 J. The flaw detection result meets the ASTM A 578C level requirement, and the surface of the steel plate has no defect.