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78 results about "Sinapic acid" patented technology

Sinapinic acid, or sinapic acid (Sinapine - Origin: L. Sinapi, sinapis, mustard, Gr., cf. F. Sinapine.), is a small naturally occurring hydroxycinnamic acid. It is a member of the phenylpropanoid family. It is a commonly used matrix in MALDI mass spectrometry.

Method for detecting platelet factor-4 without depending on antibody

The invention discloses a method for detecting platelet factor-4 without depending on antibody, which belongs to the technical field of biology. The method comprises the following steps: split-charging magnetic beads labeled with -NH2 or -COOH functional groups into a PCR tube, and then placing the PCR tube on a magnetic processor and removing liquid in the tube; taking the PCR tube out, then adding buffer solution into the PCR tube, and mixing the mixture evenly; placing the PCR tube on the magnetic processor and removing the buffer solution in the tube; taking the PCR tube out, adding serum or blood plasma sample into the PCR tube, and mixing the mixture evenly and then standing the mixture; placing the PCR tube on the magnetic processor and removing the liquid in the tube; taking the PCR tube out, adding the buffer solution into the PCR tube, and mixing the mixture evenly; placing the PCR tube on the magnetic processor and removing the buffer solution in the PCR tube; taking the PCR tube out, adding eluent into the PCR tube, and mixing the mixture evenly and then standing the mixture; placing the PCR tube on the magnetic processor and removing the liquid in the tube; and mixing the sucked liquid and saturated sinapic acid solution evenly, sucking the mixed solution to a target of matrix-assisted laser resolution ionization mass spectrometry, and putting the target into a mass spectrometer to detect the target after the solution on the target is crystallized. The method has the advantages of low price and reliable detection result.
Owner:ZHEJIANG CANCER HOSPITAL

Sinapic acid grafted modified starch and degradable preservative film and preparation method thereof

InactiveCN110981982AAvoid the problem that the concentration drops and the antibacterial effect is not durableMild reaction conditionsSinapic acidSide product
The invention relates to a sinapic acid grafted modified starch and degradable preservative film and a preparation method thereof. The preservative film is characterized in that the hydrogen atoms ofthe hydroxyl groups of the 3th and 5th positions of a glucose ring of a starch molecule are replaced by sinapic acid. The preparation method comprises following steps: (1) adding a solvent DMSO into an enclosed container, adding sinapic acid, succinic anhydride, and DMAP according to a mole ratio of 3:9:2, and carrying out reactions for 12 to 18 hours at a temperature of 50 to 60 DEG C; (2) introducing nitrogen into the container, adding CDI into the container, wherein the mole ratio of CDI to sinapic acid is 6:5, and carrying out reactions for 8 to 12 hours at a temperature of 60 to 70 DEG C;(3) dissolving starch by DMSO, adding DMSO into the container, wherein the mole ratio of starch to sinapic acid is 1:1, carrying out reactions for 36 to 48 hours at a temperature of 75 to 90 DEG C, adding acetone, wherein the ratio of acetone to starch is 4-6:1, and carrying out centrifugation; and (4) washing the precipitates, dissolving precipitates by DMSO, carrying out dialysis by using a dialysis bag, then using distilled water to carry out dialysis, and freeze-drying the dialysate to obtain SA-g-S. The preparation method has the advantages that CDI mediation is adopted to prepare the sinapic acid grafted modified starch, the reaction conditions are mild, the grafting rate is high, the byproducts are nontoxic and can be removed; and the degradable preservative film has a wide antibacterial spectrum and a strong anti-oxidation performance and is harmless to the human body.
Owner:蚌埠天成包装科技股份有限公司
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