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179results about How to "Easy processing conditions" patented technology

Method of filling structures for forming via-first dual damascene interconnects

A method of forming via-first, dual damascene interconnect structures by using a gap-filling, bottom anti-reflective coating material whose thickness is easily controlled by a solvent is provided. After application to a substrate, the bottom anti-reflective coating is partially cured by baking at a low temperature. Next, a solvent is dispensed over the coated wafer and allowed to contact the coating for a period of time. The solvent removes the bottom anti-reflective coating at a rate controlled by the bottom anti-reflective coating's bake temperature and the solvent contact time to yield a bottom anti-reflective coating thickness that is thin, while maintaining optimum light-absorbing properties on the dielectric stack. In another possible application of this method, sufficient bottom anti-reflective coating may be removed to only partially fill the vias in order to protect the bottoms of the vias during subsequent processing. The solvent is removed from the wafer, and the bottom anti-reflective coating is cured completely by a high-temperature bake. The wafer is then coated with photoresist, and the trench pattern exposed. The bottom anti-reflective coating material used maintains a greater planar topography for trench patterning, eliminates the need for an inorganic light-absorbing material layer on the top of the dielectric stack, protects the bottom of the vias during the trench etch, and prevents the formation of fencing problems by using a solvent to control the thickness in the vias.
Owner:BREWER SCI

Gas chromatography-mass spectrometer (GC-MS)/MS measuring method for 20 pesticide residues in tobaccos and tobacco products

A gas chromatography-mass spectrometer (GC-MS) / MS measuring method for 20 pesticide residues in tobaccos and tobacco products is characterized by comprising adding acetonitrile and an internal standard substance after a to-be-measured sample is soaked by water, then performing vortex extraction and salting-out layering, adding toluene to perform liquid-liquid extraction, taking supernatant to perform dispersive solid-phase extraction (d-SPE), and using a GC-MS / MS method to perform measurement. The method has the advantages that the water is utilized to soak the sample, and extraction effects of organic solvent acetonitrile added later on on pesticide targets are improved; freezing treatment is performed in advance before anhydrous magnesium sulfate is added, so that thermal degradation of part of the targets caused by severe heat release of anhydrous magnesium sulfate in the dewatering process is avoided; toluene is added in the sample extract liquid after extraction salting-out, the obtained extract liquid has shallower color than when acetonitrile is independently used, and the effects of diluting the extract liquid and partially removing impurities for the extract liquid are achieved actually.
Owner:CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT

Single-cylinder plug pin type telescopic arm, crane and telescoping method of single-cylinder plug pin type telescopic arm

The invention relates to a single-cylinder plug pin type telescopic arm, a crane and a telescoping method of the single-cylinder plug pin type telescopic arm. The single-cylinder plug pin type telescopic arm comprises a basic arm and at least one section of telescopic arm which is sleeved in the basic arm, wherein coaxial central holes are formed in the tails of the telescopic arms; a telescopic oil cylinder is arranged in the central holes and comprises a cylinder rod and a cylinder barrel; at least two cylinder heads are fixedly sleeved outside the cylinder barrel in the longitudinal direction; at least three arm pin holes are respectively formed in the basic arm and the telescopic arm in the longitudinal direction. The single-cylinder plug pin type telescopic arm provided by the invention adopts the telescopic oil cylinder and the at least two cylinder heads; each cylinder head can be used for locking and unlocking the telescopic oil cylinder and any one telescopic arm; in a relay manner, the telescopic arms stretch or shrink; telescoping of the single-cylinder plug pin type telescopic arm is realized; the length of the oil cylinder is reduced; the cylinder diameter and the rod diameter of the oil cylinder are reduced; the cost of the oil cylinder is lowered; the loading weight is reduced; the hoisting capability is improved; the design capability of the crane is improved.
Owner:XUZHOU HEAVY MASCH CO LTD

Test method of banned azo-dye in cigarette paper

The invention discloses a test method of a banned azo-dye in cigarette paper and belongs to the technical field of physical and chemical inspection of harmful substance residues in lined paper, tipping paper and carton packaging paper for cigarettes. The test method is characterized by comprising the following steps: cutting a cigarette paper sample, adding a reduction solution, reducing an azo substance into aromatic amine by sodium hydrosulfite in a citric acid buffer solution, extracting aromatic amine from the solution by a liquid-liquid extraction method, concentrating, redissolving by methanol, testing by a liquid chromatography-tandem mass spectrometry combined instrument, and quantifying by an internal standard method. According to the method, the deficiencies of a sample treatment method in the prior art are overcome, and a sample pre-treatment method and instrument test conditions are optimized for the tipping paper, the lined paper and the carton packaging paper for the cigarettes; as a solid-phase extraction column does not need to be passed, cumbersome purification and concentration steps such as rotary evaporation are not required, and the method has the advantages of accuracy for operation, high recovery rate, quickness, simplicity, convenience, high sensitivity and the like.
Owner:CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT

Hybridization system for real-time monitoring parsing process of micro array chip

The invention discloses a hybridization system for real-time monitoring parsing process of a micro array chip, which comprises a hybridization cavity body, a temperature control device, a peripheral flow path and a real-time imaging module, wherein the hybridization cavity body is composed of the micro array chip, a cavity body cofferdam and a cover plate, and a fluid inlet and a fluid outlet are formed on the cover plate; the temperature control device is connected with the hybridization cavity body; the peripheral flow path is communicated with the hybridization cavity body by the fluid inlet and the fluid outlet; and the real-time imaging module comprises a light source and a photodetection device, and the light of the light source irradiates the surface of the micro array chip, reflected by the surface of the micro array chip and then projected to the photodetection device. The micro array chip hybridization system can realize dynamic hybridization, cleaning, drying and other flows of the chip; and the real-time imaging module can realize real-time monitoring on the magnetic bead intensity of the processing flows of the chip. According to the signal change condition, the chip processing condition is optimized; and the hybridization system can also be used for studying the dynamic problems of solid-liquid phase hybridization.
Owner:BOAO BIOLOGICAL CO LTD +1

Method and device for measuring high polymer molten volume flow

ActiveCN101408443AEliminate measurement error interferenceAccurate Indirect Determination CalculationsVolume/mass flow measurementDirect flow property measurementEngineeringMeasurement precision
The invention discloses a measuring device for high polymer fusant volume flow and a measuring method thereof. The invention is characterized in that one end of a slit flow passage or a conduit flow passage (4) is connected with a flow passage actuating unit (1), the other end thereof is connected with a fusant external flow passage (5), the external flow passage is connected with the flow passage actuating unit by a loop flow passage (8), the slit flow passage or the conduit flow passage is provided with a temperature sensor (7) and a plurality of pressure sensors (2, 3), and the temperature sensor and a plurality of pressure sensors are respectively connected with a collecting and processing system (6) for temperature and data. The actuating unit pushes the high polymer fusant to enter the flow passage at a certain speed, and the passing time of fluid is measured by two pressure sensors, therefore, the volume flow of the high polymer in the flow passage can be obtained according to the physical dimension of the flow passage and the passing time. The measuring device of the invention can measure the volume flow of the high polymer fusant in the flow passage without the influence of the change of the pressure and the dimension of the flow passage. In addition, the invention provides a method which can improve and enhance the rheological measurement precision of the high polymer.
Owner:浙江博发新材料股份有限公司

Ultraviolet-visible light full-wavelength scanning sewage quality online rapid detection method and application thereof

The invention relates to an ultraviolet-visible light full-wavelength scanning sewage quality online rapid detection method and an application thereof. A full-waveband spectrum detection system is used for carrying out full-waveband scanning on sewage, a water body is directly scanned in an immersion mode, and obtained spectral absorption information of the sewage is transmitted to the full-waveband spectrum detection system; an absorption full-spectrum chart of the sewage is calculated by utilizing the full-waveband spectrum detection system; a multiple regression equation of each to-be-detected substance is obtained by fitting through a multiple regression equation model by utilizing the full-waveband spectrum detection system, wherein the multiple regression equation model is as follows: Yn = A1 * x1 + A2 * x2 +... + A210 * x210 +... + An * xn (n = 215-217), Yn is a target parameter prediction value, and A1 to An are respectively a coefficient of a wavelength corresponding to each model. The full-waveband spectrum detection system is used for detecting water quality parameter values. The simultaneous detection of various substances is realized, the detection time is short and is15 seconds, and the result can be obtained.
Owner:QINGDAO TECHNOLOGICAL UNIVERSITY

Self-inductive-internal flushing liquid electric spark processing method for metal with insulating ceramic coating

The invention relates to a self-inductive-internal flushing liquid electric spark processing method for metal with an insulating ceramic coating, belonging to the technical field of electric spark processing and forming. In order to solve the technical problem that the metal with the insulating ceramic coating cannot be processed with high quality and high efficiency, the invention provides the self-inductive electric spark processing method, and on the basis, a processing form of the internal flushing liquid of a rotating electrode is adopted. The whole processing process is carried out in an oil-base working liquid. The tubular electrode rotates around the axis and is assisted by a high pressure flushing liquid in an inner hole of the electrode, and flushing by the working liquid has good chip removal effect. A conductive material is arranged on the surface of the insulating ceramic coating, and the conductive material is connected to the positive electrode of a power supply. In the initial processing stage, according to the thermal chemical reaction of electrical discharge processing, a workpiece discharging area is self-induced to generate conductive films which are continuously produced in the processing process, and the process is continuously carried out, so that the insulating ceramic is processed. According to the self-inductive-internal flushing liquid electric spark processing method for the metal with an insulating ceramic coating provided by the invention, micropores of the metal material with the insulating ceramic coating can be processed with high precision and high efficiency.
Owner:HARBIN INST OF TECH

Method for simultaneous determination of caffeic acid and 8 flavonoids in propolis by using high performance liquid chromatography

The invention relates to a method for simultaneous determination of caffeic acid and 8 flavonoids in propolis by using high performance liquid chromatography. Simultaneous quantitative determination of flavonoids and caffeic acid has not been reported so far. The method provided by the invention is characterized in that a high performance liquid chromatograph is used for determination, the method comprises the procedures consisting of preparation of standard stock solutions, preparation of standard intermediate solutions, preparation of standard working solutions, drafting of standard curves, treatment of samples and determination of the samples, and in the procedure of preparation of the standard stock solutions, a caffeic acid standard stock solution, a rutin standard stock solution, a quercetin standard stock solution, a myricetin standard stock solution, an apigenin standard stock solution, a kaempferol standard stock solution, a pinocembrin standard stock solution, a chrysin standard stock solution and a galangin standard stock solution can be obtained. According to the invention, high performance liquid chromatography is employed for simultaneous determination of caffeic acid and 8 flavonoids in propolis, and pre-treatment of samples is easy and convenient and is rapid to operate.
Owner:杭州蜂之语蜂业股份有限公司

Artificial wetland high-efficiency pre-aeration sewage treatment system

The invention relates to an artificial wetland high-efficiency pre-aeration sewage treatment system, which comprises a bar screen, a primary sedimentation tank, a venturi, a splash board and an artificial wetland connected in turn, wherein the bar screen is positioned in the front of the primary sedimentation tank; the inlet of the gradually reducing part of the venturi is connected with the upper part of the primary sedimentation tank through a high-pressure pump, the throat part is connected with the atmosphere through an air inlet pipe, and the outlet of the gradually expanding part is provided with a jet pipe extending forwards; and the splash board is positioned above the artificial wetland in front of the jet pipe. The artificial wetland adopts a horizontal baffling structure, the water outlet is provided with a water storage tank, and the water storage tank is provided with a backflow pipe connected with the water inlet end of the artificial wetland. The artificial wetland high-efficiency pre-aeration sewage treatment system has a simple structure and reasonable process, and through the high-efficiency aeration of the venturi and the splash board, the artificial wetland high-efficiency pre-aeration sewage treatment system improves the biochemical reaction types and the reaction speed in the artificial wetland, improves the surrounding environment, and is helpful to improve the purification degree of the yielding water of the artificial wetland. The artificial wetland high-efficiency pre-aeration sewage treatment system has the advantages of simple structure, convenient operation and good adaptability, allows the sewage quantity to have large range of variation, and is mainly adapted to the treatment of domestic sewage.
Owner:HAISIBOTE BEIJING SCIENE & TECH

Method of measuring residual amount of 4-aminoazobenzene in paper for cigarettes

The invention belongs to the technical field of physical and chemical inspection of harmful substance residues in inner liners, tipping paper and carton packaging paper for cigarettes, and particularly relates to a method of measuring the residual amount of 4-aminoazobenzene in paper for the cigarettes. The method specifically comprises the following steps: reducing an azo substance into aromatic amine by sodium dithionite in an alkaline solution; then extracting the aromatic amine in the solution by using tert-butyl methyl ether; carrying out solid-phase dispersion extraction, and then measuring by using a liquid chromatography-tandem mass spectrometry; carrying out internal standard method determination. According to the method disclosed by the invention, the defects of a sample processing method in the prior art are overcome; a sample pretreatment method and instrument detection conditions are optimized, aiming at the tipping paper and the inner liners for the cigarettes, cigarette strips and carbon packaging paper samples. Since a solid-phase extraction column is not needed to pass, instead the simpler and more convenient solid-phase dispersion extraction is used, and the tedious purification and concentration steps, such as rotary evaporation is not needed, the method disclosed by the invention has the advantages of accuracy in operation, high recovery rate, high sensitivity and the like and is rapid, simple and convenient.
Owner:CHINA NAT TOBACCO QUALITY SUPERVISION & TEST CENT

Honeysuckle quality evaluation method

The invention discloses a honeysuckle quality evaluation method. According to the honeysuckle quality evaluation method, chlorogenic acid, galuteolin and six iridoid glycoside ingredients in honeysuckle are determined, wherein the six iridoid glycoside ingredients are loganic acid, morroniside, loganin, chiratin, secoxyloganin and secologanin dimethyl acetal. The honeysuckle quality evaluation method disclosed by the invention has the advantages that the iridoid glycoside ingredients in the honeysuckle are included in a honeysuckle quality evaluation system for the first time, six representative iridoid glycoside ingredients in the honeysuckle are selected and determined at the same time for guaranteeing reliability and effectiveness of the quality evaluation method, and a dispersive solid phase extraction-high performance liquid chromatography (DSPE-HPLC) is established for the first time and used for detecting the six iridoid glycoside ingredients of different structures, so that reliability and effectiveness of honeysuckle quality evaluation are obviously improved, quality control level of traditional Chinese medicine honeysuckle and related patent medicines is further improved, and the honeysuckle quality evaluation method disclosed by the invention is significant on guidance of clinical application.
Owner:SHANDONG ANALYSIS & TEST CENT
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