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89results about How to "Overcome surface tension" patented technology

Melt differential three-dimensional printer

The invention discloses a melt differential three-dimensional printer. The melt differential three-dimensional printer mainly comprises a material melting unit, a micro-droplet jetting unit, a cylindrical-coordinate system molding unit and a rack, wherein a servo motor drives a screw rod to rotate in the material melting unit; a heater, which is fixedly arranged inside a machine cylinder, ensures that granules are entirely plastified through temperature regulation; a molten material is transmitted by the screw rod to the micro-droplet jetting unit; in the micro-droplet jetting unit, the molten material is transmitted into a valve body through a hot runner in a runner plate; a linear servo motor drives a valve needle to do reciprocating motion in the valve body so as to quantitatively and intermittently squeeze the molten material out of a nozzle to form melt micro-droplets; in the cylindrical-coordinate system molding unit, the molten micro-droplets are injected to a bearing table for cooling and deposition molding; the servo motors in the left-right direction and in the vertical direction are respectively engaged with the corresponding screw rod to rotate so as to drive the material melting unit and the micro-droplet jetting unit to move along the left-right direction and the vertical direction; a circumference servo motor drives the bearing table with a worm gear to rotate through a worm rod so as to realize three-dimensional movement under a cylindrical-coordinate system.
Owner:BEIJING UNIV OF CHEM TECH

Device and method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination

The invention discloses a device and a method for preparing polysulfonamide nanometer fiber nets by means of airflow-electrostatic combination. The device comprises a liquid storage tank, an air chamber, an electrostatic generator and a receiving device, a plurality of spinnerets are arranged at the bottom of the liquid storage tank, the air chamber is arranged outside the liquid storage tank, air outlets in the number equal to that of the spinnerets at the bottom of the liquid storage tank are arranged at the bottom of the air chamber, the spinnerets are arranged inside the air outlets, an electrode with multiple pins are led from the positive electrode of the electrostatic generator to be connected with the spinnerets, and a lead is led from the negative electrode of the electrostatic generator to be connected with the receiving device. The method includes steps of combining the airflow method and the electrostatic spinning method effectively to prepare the polysulfonamide nanometer fiber nets. By the device and the method for preparing the polysulfonamide nanometer fiber nets, the specific surface area of the polysulfonamide nanometer fibers is enlarged greatly, the problem of blockage of existing electrostatic spinning needles due to inflow of the airflow is alleviated greatly, and spinning efficiency is improved. Besides, nanometer fibers can be prepared at the normal temperature directly, so that production procedures are simplified and production cost is saved.
Owner:SHANGHAI UNIV OF ENG SCI

System for nanofluid minimal quantity lubrication electrostatic atomization controllable jet flow inner cooling technology

The invention relates to a system for the nanofluid minimal quantity lubrication electrostatic atomization controllable jet flow inner cooling technology. According to the system for the nanofluid minimal quantity lubrication electrostatic atomization controllable jet flow inner cooling technology, based on the electrostatic atomization principle, minimal quantity lubrication cutting fluid fog droplets can be controllably distributed during jetting, the evenness of a fog droplet spectrum can be improved, the deposition efficiency can be improved, the fluid effective utilization rate can be increased, the motion law of the fog droplets can be effectively controlled, in this way, pollution to the environment is reduced, and better health security is provided for workers. The system comprises an adjustable high-voltage direct-current power supply, an inner-cooled cutter converter, a high-voltage electricity converting device and an integrated spray nozzle. A minimal quantity lubrication system supplies minimal quantity lubrication cutting liquid to an inner-cooled drill bit through the inner-cooled cutter converter. The adjustable high-voltage direct-current power supply conducts positive electricity to a needle electrode of the integrated nozzle through the high-voltage electricity converting device, the adjustable high-voltage direct-current power supply makes negative electricity be grounded and transmits the negative electricity to a workpiece through an electromagnetic connector, and then a corona charging field is formed in the needle electrode-workpiece area; in this way, corona charging is conducted on the minimal quantity lubrication cutting fluid, and then electrostatic atomization function is achieved.
Owner:QINGDAO TECHNOLOGICAL UNIVERSITY

Liquid-phase circulating hydrogenation treatment method capable of reinforcing gas-liquid mass transfer

The invention discloses a liquid-phase circulating hydrogenation treatment method capable of reinforcing gas-liquid mass transfer. The process flow adopted by the method comprises: part of hydrogenation circulating oil and a fresh raw material are mixed to form a liquid-phase mixed material to be filled into supergravity gas-liquid hydrogen dissolution equipment together with hydrogen; through the drive of the high-speed rotation of a feeding rotor, gas-liquid countercurrent full contact is formed; the mixed liquid-phase material in which hydrogen is dissolved is discharge out from the bottom of the supergravity gas-liquid hydrogen dissolution equipment and contacted with a catalyst to undergo a hydrogenation reaction, and part of a liquid phase obtained after reaction is circulated. Compared with the prior art, the method has the advantages that: the rotation of the feeding rotor in the gas-liquid hydrogen dissolution equipment forms a supergravity field, so the gas-liquid mass transfer efficiency is increased greatly, and the liquid phase material can fully dissolve hydrogen; meanwhile, gas impurities such as H2S and NH3 in a reaction system can be removed efficiently, so that the hydrodesulfurization, denitrification, aromatic saturation, cracking and other reactions are promoted.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method for silicon powder

InactiveCN103043665AReduce contentMeet the requirements of pickling and impurity removal processSilicon compoundsSlagAtmospheric pressure
The invention discloses a preparation method for silicon powder, relates to a process of removing boron by industrial silicon and a preparation method for high-purity superfine silicon powder. The invention provides the preparation method for the silicon powder capable of remarkably reducing the content of the boron. The silicon powder can be used as an ideal low-boron material for a later process, namely pickling and impurity-removing process of purifying solar polycrystalline silicon by a metallurgy method. The preparation method comprises the following steps of: (1), adopting a metallurgical-grade silicon material as the material, putting the material silicon to a crucible, electromagnetically heating up the silicon material to melt the silicon material by an inductive coil; (2), adding a slag former to control the heating power when the silicon material is molten, so that the temperature of the molten silicon is kept to 1550 DEG C to 1850 DEG C in a reaction process, stewing the molten silicon to remove the slag former on the upper layer of the molten silicon after slagging and refining; and (3), controlling the temperature of the molten silicon to 1500 DEG C to 1700 DEG C, and then opening the valve and starting an atomizer; guiding the molten silicon to the atomizer by a guide tube, adjusting the air pressure of the air outlet of the atomizer so that the molten silicon is sprayed out of the atomizer in the forms of mists to enter an atomizing chamber; and collecting the silicon powder by a supporting rotary plate.
Owner:XIAMEN UNIV

Device and method for magnesium process flue gas desulfurization

InactiveCN108187478AEnhanced mass transfer processImprove reaction rate and desulfurization rateDispersed particle separationFilling materialsGas pipeline
The invention discloses a device and method for magnesium process flue gas desulfurization. The device comprises a multi-stage cross flow-reverse flow rotating filling bed absorption device, wherein an exhaust pipe is arranged on the top of the rotating filling bed absorption device; a liquid discharge pipe is arranged at the bottom; a liquid inlet pipe is connected with the side surface of the upper side; an air inlet pipe is connected with the side surface of the lower side; a rotating shaft is arranged inside the rotating filling bed absorption device; two filling material rotors or more are arranged on the rotating shaft; a filling material stator is arranged between the two adjacent rotors; a liquid distributor is arranged in the center of the filling material rotor and is connected with the liquid inlet pipe; the lower end of the rotating shaft extends to the outside of an absorption device to be connected with a frequency modulation motor; the gas inlet pipe of the rotating filling bed absorption device is connected with a SO2-containing smoke gas pipeline; a liquid inlet pipe of the rotating filling bed absorption device is connected with a magnesium hydrate storage groove;the liquid discharge pipe is connected with a magnesium bisulfite storage groove. The method has the advantages that a magnesium hydroxide desulfurizer is used for wet process desulfurization; the purification degree, and the speed in the desulfurization process and the desulfurization efficiency are improved; the smoke gas ultra-low discharge standard can be reached by single piece of equipment.
Owner:ZHONGBEI UNIV

Method for preparing lithium iron manganese phosphate precursor and method for preparing lithium iron manganese phosphate

The invention relates to a method for preparing a lithium iron manganese phosphate precursor and a method for preparing lithium iron manganese phosphate. The method for preparing the lithium iron manganese phosphate precursor comprises the following steps: (1) preparing a liquid material A and a liquid material B, wherein the liquid material A is a mixed solution of a manganese salt and an iron salt, and the liquid material B is an oxalic acid or phosphoric acid solution; (2) carrying out a coprecipitation reaction on the liquid material A and the liquid material B in a supergravity rotating bed to obtain a first slurry; (3) washing and filtering the first slurry to obtain a filter cake; (4) mixing the filter cake with water, adding a carbon source, and uniformly stirring to obtain a second slurry; (5) homogenizing the second slurry; and (6) drying the homogenized second slurry to obtain the lithium iron manganese phosphate precursor. The particle size of the lithium iron manganese phosphate precursor prepared by the method is smaller and more uniform than that of a precursor prepared by a traditional method using a reaction kettle, the preparation speed is increased, and carbon coating is uniform.
Owner:JIANGSU LITHITECH CO LTD

Novel method and device for preparing polymer particles

The invention relates to a novel method and device for preparing polymer particles. The method includes the following steps that, a conductive organic solvent is pumped into an insulated capillary tube through an injection pump, the capillary tube is sealed and penetrate through a shuttle-shaped pneumatic conveying container which can be sealed, the outlet end of the capillary tube is communicatedwith a nozzle, under the strong electric field effect generated by a high voltage source, the organic solvent is dispersed to form charged droplets, under the traction force effect of electric fieldforce, gravity and flowing gas in the container, the charged droplets are uniformly spread on a grounded collection plate in the shuttle-shaped pneumatic conveying container, and the charged dropletsare grounded through the collection plate so as to remove static electricity, and solid polymer particles are formed. The novel method for preparing the polymer particles is convenient to operate, thedevice for preparing the polymer particles is simple in structure, and the particle size and shape of the obtained products, namely the polymer particles, are uniform, the performance is stable, andthe method and the device are conducive to application and popularization.
Owner:CHINA UNIV OF PETROLEUM (BEIJING)

Super-centrifugal and swirl high viscosity spinning method and device for producing nano-fibers

The invention discloses a super-centrifugal and swirl high viscosity spinning method and device for producing nano-fibers. The device comprises a storage tank, a fiber receiver, a rotating drive mechanism and a conveying mechanism; the fiber receiver is arranged below the storage tank; the rotating drive mechanism is disposed around the storage tank; the conveying mechanism is arranged outside the storage tank; a plunger rod is disposed in the storage tank; a retaining plate is disposed at the bottom of the storage tank; a feed plate is arranged above the retaining plate; a nozzle plate is disposed between the feed plate and the retaining plate; a spout of the nozzle plate is arranged within the fiber receiver. The method includes the steps: material is conveyed to the nozzle plate by forced extraction; under the coupled action of strong extrusion and super-centrifugal force, the material overcomes capillary pressure and spouts out from the spout to primarily form fiber; under further action of the super-centrifugal force and swirl air pressure, the fiber is urged to continuously decrease in diameter until arriving the fiber receiver to form nano-fiber. The nano-fibers produced by the method and device are good in performance and uniform in diameter.
Owner:SOUTH CHINA UNIV OF TECH

Nano composite solder with high retention rate and preparation method thereof

The invention discloses a nano composite solder with high retention rate and a preparation method thereof. The preparation method comprises the steps of providing a solder matrix, a nano-reinforcing phase and a cavity; cleaning the solder matrix, the nano-reinforcing phase and the cavity, and then performing surface treatment; mixing the obtained solder matrix with the nano-reinforcing phase to obtain a mixture, and placing the obtained mixture into the cavity to make the mixture into the a bulk material or a preformed sheet; and closing the cavity containing the bulk material or the preformedsheet, and melting and solidifying the bulk material or the preformed sheet under the external high-energy auxiliary action to obtain the nano composite solder with high retention rate. The compositesolder has a uniform and stable material structure, and has greatly improved strength, elongation, thermal conductivity and electrical conductivity, moreover can control a treatment process to promote the oriented alignment of the nano-reinforced phase to achieve targeted anisotropic strengthening of the composite solder, and has high material utilization rate and simple process, and the increaserange can reach 40-100% compared with the solder matrix.
Owner:HOERSON ELECTRONICS TECH +1

Droplet Generation Method Based on Microchannel

The invention provides a micro-pipeline-based liquid droplet generation method which comprises the following steps: firstly, providing a micro-pipeline with an opening in one end, wherein the micro-pipeline is full of a first liquid; providing an opened container with a second liquid; positioning the micro-pipeline above the liquid level of the opened container; enabling the micro-pipeline to move downwards from the part above the liquid level of the opened container, thereby enabling the opening of the micro-pipeline to contact and be fed into the second liquid, and positioning the first liquid at the opening of the micro-pipeline; subsequently enabling the micro-pipeline of which the opening enters the second liquid to move upwards to leave off the liquid level of the opened container, thereby dissociating the opening of the micro-pipeline from the second liquid, dissociating the first liquid at the opening of the micro-pipeline from the micro-pipeline, and forming liquid droplets in the second liquid, wherein the first liquid and the second liquid are two liquids which are not compatible with each other or two liquids with interface reaction. The liquid droplet generation method is simple and convenient, liquid droplets with controllable sizes can be formed, and the precision and the efficiency in generating large-scale liquid droplets are improved.
Owner:MACCURA MEDICAL INSTR CO LTD

Device and method for removing sulfur dioxide in waste gas

The invention belongs to the field of waste gas desulfurization, and particularly relates to a device and a method for removing sulfur dioxide contained in a waste gas. The device and the method can be used for solving the problems of the traditional waste gas desulfurization technology. The device for removing the sulfur dioxide contained in the waste gas comprises an inverse shearing rotation packed bed, a barren solution storage tank, a pregnant solution storage tank, a barren solution circulation pump and a pregnant solution circulation pump, wherein an inverse rotation packed bed absorber is in a parallel flow structure; a gas and a liquid which are positioned in the inverse shearing rotation packed bed contact in a parallel flow way. The method for removing the sulfur dioxide contained in the waste gas comprises the following step: fast transferring SO2 contained in the waste gas to a desulfurization absorbing agent by carrying out multistage parallel flow contact on the desulfurization absorbing agent and the SO2-containing waste gas through multilayer inverse rotation packings and body resistance parts. The device disclosed by the invention has the advantages of small size, width treatment tolerance range, simple structure and easiness for operation. Compared with the traditional tower, the process disclosed by the invention has the advantages of high desulfurization rate, less gas-phase pressure drop, low energy consumption, low investment and operation cost, stability in operation, convenience for start and stop, and the like.
Owner:JIANGSU ZEYU ENVIRONMENTAL ENG

Microcapsule manufacturing system driven by machinery to generate high pressure

The invention provides a microcapsule manufacturing system driven by machinery to generate high pressure, and belongs to the technical field of micro-nano manufacturing. The system comprises a mechanical energy input device, a friction nano-generator, a rectifying / boosting circuit and a microcapsule generator which are connected in sequence, wherein the mechanical energy input device drives the friction nano-generator to generate kV-level voltage and mA-level current, and the generated voltage is adjusted to be stable kV-level voltage after passing through the rectifying / boosting circuit and input into the microcapsule generator. According to the microcapsule manufacturing system driven by the machinery to generate the high pressure, the friction nano-generator and biological microcapsulemanufacturing are combined, and a high-voltage electrostatic field is generated through mechanical motion friction, so that the diameters of droplets ejected by a needle are greatly reduced; while thefriction nano-generator generates high voltage, the current in the circuit is very small, so that the system is very safe for operators and does not threaten biological cells, thereby providing a safe, controllable, concise and low-cost manufacturing platform for biological microcapsules.
Owner:TSINGHUA UNIV
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