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31results about How to "Reduce purification load" patented technology

Preprocessing method suitable for analyzing estrogen and bisphenol A in complex matrix solid sample

The invention discloses a preprocessing method suitable for analyzing estrogen and bisphenol A in a complex matrix solid sample, which is a method for detecting the estrogen and the bisphenol A based on accelerated solvent extraction-liquid-liquid extraction-Florisil column purification-alkaline solution extraction-HLB (Hydrophile Lipophile Balance) column enrichment purification-liquid chromatogram / tandem mass spectrometry (ASE-LLE-Florisil-AS-HLB-LC / MS / MS). The method comprises the following steps of: taking acetone and methanol in a volume ratio of 1 : 1 (v / v) as extracting agents for the accelerated solvent extraction of the estrogen and the bisphenol A in sludge and deposit; taking acetonitrile-normal hexane system for the liquid-liquid extraction to remove non-polar impurities such as grease and polycyclic aromatic hydrocarbon and the like; taking the Florisil column for purifying most of pigments; extracting the estrogen and the bisphenol A from residue by using 0.1mol / L of sodium hydroxide; filtering by a filter membrane of 0.22 um[m]; and enriching and purifying by using an HLB column. According to the method, the recovery rate of the estrogen and the bisphenol A is 75-100%, the detection limit is lower than 0.4ng / g, the purification effect is good and the detection requirement for the estrogen in the complex matrix solid sample is satisfied. According to the research result, the estrogens and the bisphenol A in the sludge, the deposit and the livestock and poultry manure sample can be quickly and effectively separated and purified, the accuracy and stability of the method can be favorably improved and the damage of the complex sample on the instrument also can be reduced.
Owner:BEIJING NORMAL UNIVERSITY

Method for preparing lithium carbonate by extracting lithium from lepidolite by adopting two-stage chloridizing roasting and alkali liquor leaching method

The invention discloses a method for preparing lithium carbonate by extracting lithium from lepidolite by adopting two-stage chloridizing roasting and an alkali liquor leaching method. The method disclosed by the invention comprises the following steps: (1) levigating the lepidolite and calcium chloride, adding the levigated lepidolite and calcium chloride into ammonium chloride solution, uniformly blending and pelletizing, so as to obtain green balls; (2) performing first-stage roasting on the green balls obtained in step (1) at the temperature of 150-300 DEG C and performing second-stage roasting on the green balls at the temperature of 500-800 DEG C, so as to obtain clinkers; (3) leaching the clinkers obtained in step (2) with water, and filtering to obtain leaching solution; (4) addingcarbonate solution into the leaching solution obtained in step (3), stirring and filtering to obtain mother solution and filter residues, and collecting the filter residues, so as to obtain the lithium carbonate. In the method disclosed by the invention, all the steps are cooperated, and a process of preparing the lithium carbonate by extracting the lithium from the lepidolite is environmentallyfriendly, low in energy consumption, low in cost and high in extracting efficiency. Therefore, the method disclosed by the invention has a broad industrial application prospect.
Owner:CENT SOUTH UNIV

Method and device for continuously rinsing chemical activated carbon

The invention discloses a method and device for continuously rinsing chemical activated carbon. The rinsing device is a combination of a conveying chain plate, a long-strip-shaped rinsing water tank and an activated tail gas heating facility and comprises a feeding pipe, material partition plates, the conveying chain plate, a rinsing water tank bottom plate, an activated tail gas flow guide partition plate, an activated tail gas jacket, a chain wheel, an activated tail gas inlet, an activated tail gas connecting pipe, an activated tail gas outlet, a device supporting column, a spraying nozzle,an activated tail gas condensate discharge port, a rinsed carbon guide groove and side face material baffles. The rinsing water tank has the length of 10-15 m and the width of 0.6-1 m. The activatedtail gas jacket is arranged at the bottom of the water tank. The annular conveying chain plate is arranged on the inner side and the two ends of the water tank and the outer side of the activated tailgas jacket. The material partition plates perpendicularly welded to the chain plate at the interval of 0.4-0.6 m are arranged on the chain plate. The side face material baffles parallel to the side faces are arranged on the upper sides, on the two sides of the interior of the water tank, of the chain plate. A driving motor drives the chain wheel and the chain plate through a reduction gear to circularly run around the water tank in the upward, downward, leftward and rightward directions.
Owner:ZHEJIANG FORESTRY ACAD

Ecological restoration system suitable for hard revetments of high-flow-rate polluted rivers

The invention provides an ecological restoration system suitable for hard revetments of high-flow-rate polluted rivers. The system comprises an upstream permeable wall, a plant area and a downstream permeable wall, wherein the upstream permeable wall is connected with the plant area through an iron wire net, the plant area is connected with the downstream permeable wall through the iron wire net,bio-balls are arranged in the downstream permeable wall, and microorganisms are attached to the bio-balls; incoming water flows into the plant area at a lower flow rate after being dissipated and adsorbed by the upstream permeable wall, is purified by plants, then flows into the downstream permeable wall, is degraded by the microorganisms attached to the bio-balls and arranged in the downstream permeable wall and flows out of the system. The system has the advantages as follows: 1) energy dissipation can be effectively performed on high-flow-rate water, and impurities can be filtered and adsorbed; 3) sustainable ecological restoration can be performed on water; 4) the bio-balls are arranged in the downstream permeable wall, and the purification capacity is improved; 5) the erosion effect of the water on the revetments is weakened; 6) the overall process device of the system is made of an environment-friendly lightweight material, and the whole device is convenient to install, replace and maintain.
Owner:南京市长江河道管理处 +1

Method and device for recycling waste circuit boards through ion liquid

InactiveCN109967487AOvercome the disadvantages of high energy consumptionWide electrochemical windowTransportation and packagingSolid waste disposalParticulatesCatalytic pyrolysis
The invention discloses a method and a device for recycling waste circuit boards through ion liquid, and belongs to the technical field of solid waste resource development and utilization. The methodcomprises the steps of prilling the waste circuit boards, then mixing the waste circuit board particles and the magnetic ion liquid, heating the mixture, meanwhile, applying voltage on the mixture through an inert electrode or/and applying a magnetic field on the mixture through a magnetic induction loop, carrying out catalytic pyrolysis on the mixture at 200 to 500 DEG C, collecting a gas-phase product, and condensation recycling; and separating solid-phase and liquid-phase products, recycling a liquid phase, and magnetically separating a solid phase. According to the method and the device for recycling the waste circuit boards through the ion liquid provided by the invention, the ion liquid with a high catalytic performance is utilized, electricity or/and magnetism is/are additionally added for producing an electromagnetic coupling liquid phase catalysis effect on an organic matter base plate, the pyrolysis temperature is low, the micromolecule substance yield is high, a catalyst canbe recycled, and a pyrolysis three-phase product is high-value utilized.
Owner:KUNMING UNIV OF SCI & TECH

Anti-haze heat dissipation type solar street lamp

The invention discloses an anti-haze heat dissipation type solar street lamp, and relates to the technical field of street lamps, the anti-haze heat dissipation type solar street lamp comprises a lamppost, a lamp post is arranged at the upper part of the lamp post, an LED lamp is mounted on the lamp post, an inner cavity of the lamp post naturally forms an air outlet area, a purification area, anair inlet area and a pollution discharge area from top to bottom, a plurality of air outlet holes are formed in the side wall of the air outlet area, a fan, a filtering assembly, a spraying assemblyand a steel wire mesh layer are sequentially arranged in the purification area from top to bottom, the filtering assembly comprises an activated carbon layer and two grating plates arranged on the upper face and the lower face of the activated carbon layer respectively, the spraying assembly comprises a spraying pipe and a plurality of spraying heads installed on the lower side face of the spraying pipe, the two ends of the spraying pipe penetrate through the lamp pole wall, one end of the spraying pipe is connected with a circulating water tank through a first water pump, and the other end penetrates through a heat dissipation area of the lamp and then is connected to the circulating water tank, a plurality of air inlet holes are formed in the side wall of the air inlet area, and the bottom end of the blowdown area is connected with a water outlet pipe. The street lamp can be cooled, and haze can be removed at the same time.
Owner:江苏丰登光电科技有限公司

System and method for treating radioactive waste through plasma high-temperature pyrolysis melting

The invention belongs to the technical field of radioactive waste treatment, and particularly discloses a system and method for treating radioactive waste through plasma high-temperature pyrolysis melting, and the system comprises a plasma high-temperature melting furnace, a plasma torch communicated with the melting furnace, a feeding device and a combustible gas supplementary combustion device. The air pump and the two-stage dust removal device are communicated with the combustion device, the nitric oxide removal device is communicated with the combustion device and the two-stage dust removal device, the heat exchange cooling device is communicated with the dust removal device, and the induced draft fan and the chimney are communicated with the heat exchange cooling device. The method comprises the steps that after radioactive waste is fed, the plasma torch heats and melts the waste in the melting furnace to generate radioactive waste gas and a glass melting solidified body, tail gas generated by combustion is subjected to nitrogen oxide removal, two-stage dust removal, heat exchange cooling, deacidification, demisting, cooling and purification, and then the tail gas is discharged. The pyrolysis efficiency of radioactive waste can be improved, the tail gas purification treatment load is reduced, the tail gas emission quality is improved, and a stable glass melting solidified body is generated.
Owner:SOUTHWESTERN INST OF PHYSICS +1

Power plant industrial wastewater treatment device

The invention relates to a power plant industrial wastewater treatment device, which comprises an anaerobic tank, a water inlet pipe is arranged on the outer surface, close to the upper portion of theleft side, of the anaerobic tank, an anoxic tank is arranged on the outer surface, close to the right side, of the water inlet pipe, and an oxygen discharging pipeline is arranged in the middle, close to the upper side, of the outer surface of the anoxic tank; an aerobic tank is arranged on the outer surface, close to the right side, of the anoxic tank, and a secondary sedimentation tank is arranged on the outer surface, close to the right side, of the aerobic tank. According to the wastewater treatment device, an activated carbon plate and a biological nano-membrane plate can be convenientlycleaned, internal components of the device can be flushed without disassembly, the cleaning process of the internal components of the device is simplified, convenience is brought to a user, the purification effect of the device in the secondary sedimentation process is kept in the optimal state, the sewage is subjected to double purification processes of nitrogen and phosphorus removal, so that the operation steps of subsequent sewage treatment procedures are reduced.
Owner:フアネングチンメイルイジンパワージェネレーションカンパニーリミテッド

A method and a sintering machine for recycling flue gas to form a multi-stage secondary combustion chamber for incinerating solid waste flue gas

The invention provides a method for circulating flue gas on a sintering machine to form a multi-stage secondary combustion chamber for incineration disposal of solid waste flue gas. The sintering machine is utilized as main equipment for disposing solid waste, flue gas generated in the incineration process is circularly disposed, and the multi-stage secondary combustion chamber is formed through a next-stage combustion material layer. Specifically, a plurality of independent flue gas hoods are sequentially arranged above an incineration section of the sintering machine, and materials of the incineration section are isolated from external air; each flue gas hood corresponds to one or more draught hoods below the incineration section of the sintering machine, a flue gas inlet is formed in each flue gas hood, and each flue gas inlet is connected with a negative-pressure air draft pipeline of the previous draught hood below the incineration section; all flue gas generated by combustion of the preceding stage is collected to an air inlet position of the next stage to be mixed with distributed fresh air to be used as a combustion gas source of this stage, the flue gas passes through a high-temperature combustion zone in the incineration process to be subjected to secondary combustion, and full-amount circulating combustion of the flue gas is achieved; and combustible substances existing in the flue gas are thoroughly combusted, and the construction investment and operating cost of a flue gas purification system project are reduced.
Owner:CHONGQING ANGRUIYUE SCI & TECH

Preprocessing method suitable for analyzing estrogen and bisphenol A in complex matrix solid sample

The invention discloses a preprocessing method suitable for analyzing estrogen and bisphenol A in a complex matrix solid sample, which is a method for detecting the estrogen and the bisphenol A based on accelerated solvent extraction-liquid-liquid extraction-Florisil column purification-alkaline solution extraction-HLB (Hydrophile Lipophile Balance) column enrichment purification-liquid chromatogram / tandem mass spectrometry (ASE-LLE-Florisil-AS-HLB-LC / MS / MS). The method comprises the following steps of: taking acetone and methanol in a volume ratio of 1 : 1 (v / v) as extracting agents for the accelerated solvent extraction of the estrogen and the bisphenol A in sludge and deposit; taking acetonitrile-normal hexane system for the liquid-liquid extraction to remove non-polar impurities such as grease and polycyclic aromatic hydrocarbon and the like; taking the Florisil column for purifying most of pigments; extracting the estrogen and the bisphenol A from residue by using 0.1mol / L of sodium hydroxide; filtering by a filter membrane of 0.22 um[m]; and enriching and purifying by using an HLB column. According to the method, the recovery rate of the estrogen and the bisphenol A is 75-100%, the detection limit is lower than 0.4ng / g, the purification effect is good and the detection requirement for the estrogen in the complex matrix solid sample is satisfied. According to the research result, the estrogens and the bisphenol A in the sludge, the deposit and the livestock and poultry manure sample can be quickly and effectively separated and purified, the accuracy and stability of the method can be favorably improved and the damage of the complex sample on the instrument also can be reduced.
Owner:BEIJING NORMAL UNIVERSITY

Leakage-free coaling and coke pushing combined smoke purifying and recycling system and technology for coke oven

The invention discloses a leakage-free coaling and coke pushing combined smoke purifying and recycling system and a technology for a coke oven, which comprises the coke oven (1), a coke pushing device (2) and a coke guide (3), wherein a double-U-shaped water sealing smoke guide car (6) and a high-pressure ammonia water system (7) are connected with a furnace top gas collecting tube (4) through which the coke oven is led to a chemical product recycling and purifying system (5); a smoke collecting hood (8) is equipped on an oven side furnace end of the coke oven; the smoke collecting hood is connected with a U-shaped water sealing dust-removal dry tube (10) through a leakage-free seal connecting device (9) equipped on the double-U-shaped water sealing smoke guide car; an automatic ignition burning device (11), a Venturi dust-removal device (12), a desulfurization system (13) and a fan (14) are connected in sequence behind the U-shaped water sealing dust-removal dry tube; and a discharge pipe of the fan is led to a quenching tower. The leakage-free coaling and coke pushing combined smoke purifying and recycling system and the technology for the coke oven are low in power consumption, low in investment and good in dust removal effect, and fit for all coke ovens.
Owner:冯书辉
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