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39results about How to "Good flow dispersion" patented technology

Ginkgolic acid grafted and modified polycarboxylate water-reducer and preparation method thereof

The invention provides a ginkgolic acid grafted and modified polycarboxylate water-reducer and a preparation method thereof. The polycarboxylate water-reducer is a random copolymer prepared by polymerizing ginkgolic acid, unsaturated polyether, unsaturated carboxylic acid or salt thereof. The preparation method comprises the following steps: dissolving ginkgolic acid and unsaturated polyether into water; heating the solution to reach the temperature of 20-80 DEG C; then correspondingly dropwise adding the aqueous solution of unsaturated carboxylic acid and the aqueous solution of an initiator and a chain transfer agent for 2-2.5 hours and 3-3.5 hours; continuously reacting for 1 hour under the temperature of 20-80 DEG C after dropwise adding; cooling; neutralizing the system with liquid caustic soda until the pH is 6-7, so as to obtain the ginkgolic acid grafted and modified polycarboxylate superplasticizer. According to the preparation method, unsaturated ginkgolic acid is extracted from waste ginkgo biloba exocarp; carboxyl, hydroxyl and side chain of ginkgolic acid are introduced into a water-reducer molecular structure, therefore, the wastes are treated into treasure on the premise that the performance of the water-reducer is maintained, and as a result, the environment is protected, and the cost of the polycarboxylate water-reducer is decreased.
Owner:WUHAN UNIV OF TECH

Novel polyaluminum chloride water purifying agent and preparation method thereof

The invention discloses a novel polyaluminum chloride water purifying agent and a preparation method thereof. Polyaluminum chloride contains 10wt%-12wt% of aluminum oxide, has basicity being 70 wt%-95wt%, contains lower than or equal to 0.1wt% of water insoluble substances and has pH (10g/L aqueous solution) being 4.5-5.0. The preparation method of the polyaluminum chloride water purifying agent comprises the following steps: preparing aluminum-containing mother liquor, and performing high-speed dispersion and homogenization to obtain homogenized mother liquor; adding an alkaline regulator under the condition of high-speed dispersion to adjust the polymerization degree, and performing continuous reaction to obtain the polyaluminium chloride water purifying agent. The novel polyaluminum chloride water purifying agent has the advantages of high aluminum, high basicity, high flow dispersibility, wider pH application range, better coagulation effect, COD removal rate up to 50% or higher and TP removal rate up to about 99%. In the preparation method, the high-speed dispersion technology is adopted to homogenize the aluminum-containing mother liquor and the polymerization degree and adjust reaction procedure, so that the defect of limited polymerization degree adjustment of the traditional alkali adjustment system is overcome, and complete slag-free continuous production of water purifying agent with high polymerization degree is achieved.
Owner:CHANGZHOU WUJIN YOUBANG WATER PURIFICATION MATERIALS

A kind of polycarboxylate water-reducer modified by gingkgolic acid grafting and preparation method thereof

The invention provides a ginkgolic acid grafted and modified polycarboxylate water-reducer and a preparation method thereof. The polycarboxylate water-reducer is a random copolymer prepared by polymerizing ginkgolic acid, unsaturated polyether, unsaturated carboxylic acid or salt thereof. The preparation method comprises the following steps: dissolving ginkgolic acid and unsaturated polyether into water; heating the solution to reach the temperature of 20-80 DEG C; then correspondingly dropwise adding the aqueous solution of unsaturated carboxylic acid and the aqueous solution of an initiator and a chain transfer agent for 2-2.5 hours and 3-3.5 hours; continuously reacting for 1 hour under the temperature of 20-80 DEG C after dropwise adding; cooling; neutralizing the system with liquid caustic soda until the pH is 6-7, so as to obtain the ginkgolic acid grafted and modified polycarboxylate superplasticizer. According to the preparation method, unsaturated ginkgolic acid is extracted from waste ginkgo biloba exocarp; carboxyl, hydroxyl and side chain of ginkgolic acid are introduced into a water-reducer molecular structure, therefore, the wastes are treated into treasure on the premise that the performance of the water-reducer is maintained, and as a result, the environment is protected, and the cost of the polycarboxylate water-reducer is decreased.
Owner:WUHAN UNIV OF TECH

Preparation method of royal jelly microcapsule

The invention discloses a preparation method of a royal jelly microcapsule. The method comprises the following steps: preparing a water solution of sodium alginate with a concentration of 0.015 to 0.025 g/mL and a water solution of loyal jelly with a concentration of 0.15 g/mL, taking the two water solutions as the raw material solution; preparing a mixed solution containing CaCl2 (5-15 mg/mL), chitosan (2.5-7.5 mg/mL), and royal jelly (0.15 g/mL), wherein the pH value of the mixed solution is 4.5 to 6.0, subjecting the mixed solution to a centrifugation treatment, taking the supernate as the gel bath; transporting the raw material solution to the positive pole of a nozzle through a peristaltic pump, arranging a round disc, which is made of stainless steel and is provided with a hole in the center, right under the nozzle and above the gel bath, taking the round disc as the negative pole, spraying the raw material solution into the gel bath from the nozzle to form calcium alginate micro beads in the gel bath, and then subjecting the micro beads to processes of suction filtration, water washing, and freeze-drying so as to obtain the royal jelly microcapsule. The preparation method has the advantages of low temperature and short time. The moisture absorbing property of the freeze-dried powder in the royal jelly microcapsule is reduced, the pungent smell is prominently reduced at the same time, and the microcapsule can tolerate the stomach environment and finally releases freeze-dried powder in the small intestines.
Owner:ZHEJIANG UNIV OF TECH

Composite lining paper coating, printing processing technology

The invention discloses a composite lining paper coating, printing and processing technology. The technology comprises the following specific steps of: (1) unwinding: respectively inserting an aluminum foil roll and lining paper into two unwinding devices, simultaneously unwinding the aluminum foil and lining paper, enabling the unwound aluminum foil and lining paper to be parallel to each other,enabling the aluminum foil to be positioned right above the lining paper, and (2) compounding: coating the opposite surfaces of the aluminum foil and the lining paper with an adhesive through an adhesive coating roller, and then simultaneously pressing and forming the aluminum foil and the lining paper coated with the adhesive through a composite pressing roller to obtain the composite lining paper. The printing roller is set to be a micro-concave screen roller; the paper feeding direction of the composite lining paper is opposite to the rotating direction of the micro-concave screen roller; the composite lining paper and the micro-concave screen roller are coated reversely, certain relative friction is generated, so that uniform spreading of coating liquid on the composite lining paper isfacilitated; the liquid transfer amount of the micro-concave screen roller is further large, ink can fully fill fiber gaps and subsurface concave-convex areas of the composite lining paper, and the coating effect of the composite lining paper is guaranteed.
Owner:YUXI DAYING STREET ALUMINUM FOIL PAPER

Hollow microsphere composite modified thermosetting polyimide material and preparation method thereof

The invention relates to a hollow microsphere composite modified thermosetting polyimide material and a preparation method thereof. The material is prepared by the following steps: carrying out mechanical blending on the hollow microsphere and a thermosetting polyimide prepolymer according to the mass fraction ratio of (1 to 20 percent) to (99 to 80 percent) and uniformly mixing all parts to obtain a hollow microsphere / thermosetting polyimide prepolymer mixture; carrying out melting and crosslinking treatment on the mixture under high-temperature condition to prepare products such as high temperature resisting parts, adhesives and advanced composite materials. The invention aims at reducing the expensive cost of existing blocked thermosetting polyimide and further improving the comprehensive performance of the material at the same time, in particular to the melting processability of the thermosetting polyimide prepolymer and temperature resistance of cured resin. The hollow microsphere / thermosetting polyimide prepolymer obtained by modifying provided by the invention has the advantages that the cost is reduced; in addition, the melt viscosity can be greatly reduced and the meltingprocessing capacity is enhanced; the temperature resistance of the cured resin is also effectively improved.
Owner:SHANGHAI JIAOTONG UNIV

A kind of microsphere graphene reinforced masterbatch and preparation method

ActiveCN107151364BMake use of interface characteristicsAvoid reunionMasterbatchMicrosphere
Theinvention discloses a microsphere graphene reinforced master batch and a preparation method. In a glass microsphere forming process, graphene adheres to the surface of the glass microsphere, so as to form microsphere graphene with graphene as a wrapping layer and glass microsphere as a core after condensation. The graphene fulfills a higher potential in interface characteristic, further, the graphene and the glass microsphere are combined tightly, so that the microsphere graphene is easy to flow and scatter. The graphene scatters in a sphere state, thereby being prevented from gathering effectively. The microsphere graphene reinforced master batch with a reinforcing function can be obtained by assisting pelletizing of high-molecular polymer. When the microsphere graphene reinforced master batch is used for reinforcing materials like plastics and rubber, the graphene is tightly combined with the glass microsphere so as to scatter in the microsphere state in the system, so that the scattering function is improved substantially; in addition, the graphene fulfills a higher potential in interface characteristic, that is, the graphene can be better wound the plastics and rubber. The preparation method disclosed in the invention is simple, a wide range of raw materials can be used, and the preparation method is contamination-free, is low in cost, and is easy to realize large-scale industrial production.
Owner:台州施特自动化有限公司

Degradable antibacterial functional master batch special for polylactic acid and preparation method of degradable antibacterial functional master batch

The invention relates to the technical field of plastic modification processing, in particular to a special degradable antibacterial functional master batch for polylactic acid and a preparation method of the special degradable antibacterial functional master batch, and the antibacterial functional master batch comprises the following components in percentage by mass: 75.0-85.0% of low-molecular-weight polylactic acid; 10.0 to 20.0 wt.% of an inorganic antibacterial agent; 1.0 to 3.0 wt.% of nano cerium dioxide; 1.0 to 3.0 wt.% of mesoporous zirconium hydrogen phosphate; 0.1 to 0.3 wt.% of a thermo-oxidative aging resistant auxiliary agent; and 2.5-3.0 wt.% of a dispersing aid. According to the antibacterial functional master batch provided by the invention, a powder antibacterial agent of a silver-zinc ion inorganic substance carrier is adopted, and mesoporous zirconium hydrogen phosphate is introduced into the antibacterial functional master batch, so that the antibacterial performance of a modified polylactic acid special material adopting the antibacterial functional master batch can be remarkably improved, and the action period of the antibacterial function of modified biodegradable plastic is prolonged; the processing efficiency is improved.
Owner:江苏万纳普新材料科技有限公司

Novel polyaluminum chloride water purifier and preparation method thereof

ActiveCN109678232BSolve the defect of limited adjustment of polymerization degreeGood flow dispersionWater/sewage treatment by flocculation/precipitationAluminium chlorideAluminium chlorohydrate
The invention discloses a novel polyaluminum chloride water purifying agent and a preparation method thereof. The aluminum oxide of the polyaluminum chloride is 10-12wt%, the basicity is 70-95wt%, the water-insoluble matter is ≤0.1wt%, and the pH (10g / L aqueous solution) value is 4.5-5.0, and its preparation method includes the following Steps: preparing aluminum-containing mother liquor, high-speed dispersion and homogenization to obtain a homogenized mother liquor, adding an alkaline regulator under high-speed dispersion conditions to adjust the degree of polymerization, and continuing the reaction to obtain a polyaluminum chloride water purifying agent. The new polyaluminum chloride water purifying agent of the present invention has high aluminum, high basicity, high flow dispersibility, wider pH application range, better coagulation effect, COD removal rate can reach more than 50%, and TP removal rate can reach About 99%, in the preparation method of the present invention, the high-speed dispersion technology is used to homogenize the aluminum-containing mother liquor and the polymerization degree adjustment reaction process, which overcomes the limitation of the polymerization degree adjustment of the traditional alkali adjustment system and realizes the high polymerization degree water purifier Completely slag-free continuous production.
Owner:CHANGZHOU WUJIN YOUBANG WATER PURIFICATION MATERIALS
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