30 results about "Mercury nitrate" patented technology

The invention belongs to the field of semiconductor nanomaterial preparation, in particular to a method for rapidly preparing spherical mercury sulfide nanoparticles, aiming at the existing problem of not being able to save energy and time, and synthesizing mercury sulfide nanoparticles with uniform shape and size and good dispersibility. Propose the following scheme, which includes the following steps: S1: Preparation of reaction mixture: at room temperature, add 0.5mmol of mercury nitrate, 0.5mmol of sulfur powder, and 0.15g of polyvinylpyrrolidone to 500g of ethylene glycol to prepare a mixture; S2: Synthesis of mercury sulfide nanoparticles: transfer the mixed solution into an oil bath filled with dimethyl silicone oil, and perform magnetic stirring to make the mixed solution react for 2 hours; S3: Separation of mercury sulfide nanoparticles: transfer the mixed solution from the bath Take it out from the pot, add an equal volume of ultrapure water and centrifuge for 15 minutes, remove the supernatant to retain the precipitate, and wash the precipitate with ultrapure water, and the precipitate will be spherical mercury sulfide nanoparticles after freeze-drying. The solvothermal synthesis system of the present invention can be used to prepare spherical nano-mercuric sulfide; the obtained spherical nano-mercuric sulfide particles have a single crystal form, good dispersibility, uniform shape and high stability; the method and process are simple, time-consuming, and the reaction temperature Low energy consumption, low cost of raw materials, easy to obtain, and conducive to industrial production.

The invention provides a human urine detection reagent for monohydroxyphenyl metabolites. The human urine detection reagent for the monohydroxyphenyl metabolites comprises mercury sulfate solution, mercury nitrate solution, nickel sulfate solution, silicotungstic acid solution, trichloroacetic acid solution and mercury ion (i) mesoporous silica. The concentration of the mercury sulfate solution is 0.7-3 mol / L; the concentration of the mercury nitrate solution is 0.1-0.6 mol / L; the concentration of the nickel sulfate solution is 0.01-0.05 mol / L; the concentration of the silicotungstic acid solution is 1.0-4.0 mmol / L; the concentration of the trichloroacetic acid solution is 0.6-5.0 mmol / L; the mass fraction of the mercury ion (i) mesoporous silica is 3-10%.