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31results about How to "Reduced interfacial free energy" patented technology

Viscose containing natural antimicrobials and preparation method thereof

The invention provides viscose containing natural antimicrobials. The viscose containing the natural antimicrobials comprises the viscose and the antimicrobials contained in the viscose. The viscose containing the natural antimicrobials is characterized in that the antimicrobials is natural indigowoad leaf extract powder, a natural indigowoad leaf extract powder solution added with dispersing agent is added into a viscose filature stock solution, the additive amount of the natural indigowoad leaf extract powder is 1%-7% of the quality of the viscose filature stock solution, the additive amount of the dispersing agent in the natural indigowoad leaf extract powder solution is 0.1%-1.0% of the quality of water in the natural indigowoad leaf extract powder solution. The preparation method of the viscose comprises the steps of dissolving the indigowoad leaf extract powder into water and adding the dispersing agent to obtain the indigowoad leaf extract powder solution, adding the indigowoad leaf extract powder solution to the viscose filature stock solution according to a ratio of 10%-14% of the quality of the viscose filature stock solution, and then shaping a obtained solution according to conventional wet spinning jet process to obtain the viscose. The viscose has a durable antibacterial function and has no side effect on human bodies. The preparation method has reasonable and simple technology, and is suitable for industrialized production.
Owner:单修铎

Preparation method of high-refractive-index high-transparency friction type silicon dioxide

The invention provides a preparation method of high-refractive-index high-transparency friction type silicon dioxide. The preparation method comprises the following steps: (1) blending a sodium silicate solution, adding a surfactant, and stirring uniformly; (2) injecting sodium sulfate solution into a reaction tank, starting a stirring device, and heating to 80-90 DEG C; (3) adding the sodium silicate solution into the reaction tank, synchronously adding sulfuric acid solution after 0.5-1 minute, controlling a pH value to be 9.0-9.5, further adding the sulfuric acid solution after the sodium silicate solution is completely added, controlling the pH value of a reaction end point to be 4.4-4.8, then stopping adding the sulfuric acid solution, keeping temperature at 80-85 DEG C, and further stirring and precipitating for 10-15 minutes to obtain slurry; and (4) performing pressure filtration on the slurry obtained in the step (3) to obtain a filter cake, washing the filter cake by using deionized water, and drying and crushing the washed filter cake to obtain high-refractive-index high-transparency friction type silicon dioxide. Silicon dioxide prepared by using the method provided by the invention is high in refractive index and wide in range, ensures that the transparency can reach 99.0%, and also has good cleaning performance and fluorine compatibility.
Owner:GUANGZHOU FEIXUE MATERIAL TECH

Surface metallised ceramic and manufacturing method thereof

The invention discloses a surface metallised ceramic and a manufacturing method thereof. The method comprises the following operation steps of immersing a metallised surface of the ceramic in an aluminium or aluminium alloy melt, making the metallised surface move with respect to the melt such that the aluminium or aluminium alloy melt wets the metallised surface of the ceramic, taking out the metallised surface of the ceramic from the melt and freely cooling the aluminium or aluminium alloy film attached to the surface, so as to obtain the ceramic with the surface connected with the aluminium or aluminium alloy film. Compared with prior art, the interface between the ceramic and the aluminium or the aluminium alloy film in the invention does not contain amorphous oxide. The aluminium or aluminium alloy crystal grains and the ceramic crystal grains are grown together. The internal organisations of the formed film are compact and do not contain oxide. The formed aluminium or aluminium alloy film has a thickness in a range from several microns to more than ten microns, is firm, and cannot easily fall off. The chessboard division peeling strength between the aluminium or the aluminium alloy film and the ceramic is proved, by experiments, to be greater than or equal to 4.1N / cm. The invention has wide application prospect in the surface metallising field of ceramic.
Owner:TSINGHUA UNIV

Preparation method of foamed polypropylene beads

ActiveCN106543559ALow costPowerful deliveryPolymer sciencePlastic packaging
The invention discloses a preparation method of foamed polypropylene beads. The method comprises the following steps that 1, polypropylene resin, an active filler and auxiliaries are added into a high-speed mixing machine and mixed to be uniform at the temperature of 10-20 DEG C, and a polypropylene foaming material is obtained; 2, the polypropylene foaming material is added into a triple-screw extruder, plastification and mixing are conducted, a supercritical fluid is injected, the mouth mold pressure is controlled to be 5-25 MPa, the mouth mold temperature is 110-160 DEG C, instant pressure release is conducted through a mouth mold, foaming is conducted, and super-fine hole foamed polypropylene is obtained; 3, super-fine hole foamed polypropylene is subjected to mold surface water-ring hot-cutting granulation, drying and sieving, and the foamed polypropylene beads are obtained. The method is low in production cost, high in capacity, safe and environmentally friendly, no foaming agent decomposed residue exists in the prepared foamed polypropylene beads, secondary foaming can be conducted, the foaming ratio can be adjusted, the rebound resilience of a finished product is high, decomposing and recycling are easy, and the foamed polypropylene beads can be widely used in the fields of plastic packaging, transportation industry, military aerospace, office supplies and the like.
Owner:湖北聚石新材料科技有限公司

Atorvastatin calcium tablet and preparation method thereof

The invention provides an atorvastatin calcium tablet which comprises the following components of raw materials in parts by weight: 1-20 parts of atorvastatin calcium, 10-80 parts of a filling agent,20-40 parts of a disintegrant, 5-40 parts of an adhesive, 1-15 parts of a lubricant and 1-20 parts of a calcium enhancing agent. The atorvastatin calcium tablet provided by the invention has the advantages of being high in stability, good in dissolubility, high in bioavailability, and the like, and is good in clinical application prospect.
Owner:NUOWEIDE TIANJIN PHARMA

Blood pretreatment liquor

The invention discloses blood pretreatment liquor which includes the following components: sodium chloride, monopotassium phosphate, dibasic sodium phosphate, bovine serium albumin, an ionic detergent, a protein protectant, Proclin-300 and water; the interfacial free energy can be reduced by the ionic detergent, and the interfacial properties of to-be-removed objects and the matrix can be changed, glycerol, active polysaccharides and the biological activity of bovine serium albumin can be fused for function enhancement through like charges repelling, filtering or magnetic adsorption of an adsorption layer. With the utilization of the blood pretreatment liquor provided by the invention, after centrifuging blood, white blood cells, infected factors and target cells and the like are concentrated and purified, and the surface bioactivity of the cells cannot be damaged.
Owner:NINGBO MEIJING MEDICAL TECH

Amphiphobic fluorine-containing nanofluid as well as preparation method and application thereof

The invention relates to an amphiphobic fluorine-containing nanofluid as well as a preparation method and application thereof. The amphiphobic fluorine-containing nanofluid is composed of a nano core material and a polymer shell layer material, the surface of the nano core material is grafted with a coupling agent with double bonds, the polymer shell material is a fluorine-containing polymer, and the invention further provides a preparation method and application of the amphiphobic fluorine-containing nano fluid. The amphiphobic fluorine-containing nanofluid disclosed by the invention has extremely strong wetting reversal capability, can be used for transforming oil reservoirs, can convert the wettability of hydrophilic and oleophylic reservoirs into remarkable amphiphobic property, and effectively solves the liquid lock effect and Jamin effect caused by the wettability of the reservoirs.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)

Oil-in-water type menthol ointment and preparation method thereof

The invention discloses oil-in-water type menthol ointment and a preparation method thereof. The oil-in-water type menthol ointment comprises glycerol, camphor, menthol, eucalyptus globulus leaf oil, a liquorice extract, vitamin E, allantoin, citronella oil and the like. The oil-in-water type menthol ointment has the effects of cooling and refreshing, diminishing inflammation, relieving itching and repelling mosquitoes, and has the advantages of being high in stability, low in irritation and small in oily feeling.
Owner:GUANGDONG SHUNFENG PHARMA

Cement composite dispersant

InactiveCN110015861AImprove surface activityGood amphiphilic surface activityChemical industryHydrolysis
The invention discloses a cement composite dispersant, and belongs to the technical field of chemical industry. The problems that a current commonly used cement dispersant has a poor dispersion effectand influences on the internal mechanical properties are solved. A low critical micelle concentration can be maintained, the lipophilic groups of the dispersant can be adsorbed on the surface of thecement, and the hydrophilic groups can be combined with water, so that the dispersion effect of the cement is improved better. Hydrogen bonds are formed by silicon hydoxyl groups generated through hydrolysis and hydroxyl group contained in a composite dispersing material B, so that the stability of dispersion is enhanced, and the internal bonding force is improved; high-polarity reactive carboxylgroups in acrylic acid are introduced into humic acid molecules of the dispersant, and the influence of steric hindrance is brought through cooperation with acrylic acid grafting, so that the viscosity-reducing effect of the prepared silicon-containing material is improved, the dispersibility inside the obtained blended material is improved, and generation of sedimentation and uneven dispersion isreduced; and furthermore, the cement cohesion strength is improved, and the internal mechanical properties is further improved after blending of the cement is performed.
Owner:刘国荣

Preparation method of starch microspheres with small particle sizes

The invention discloses a preparation method of starch microspheres with small particle sizes. The preparation method comprises steps as follows: (1) preparation of a starch solution; (2) preparation of a polyvinylpyrrolidone solution; (3) forming of an aqueous two-phase emulsion through high-speed shearing and emulsification performed after the polyvinylpyrrolidone solution is added to the starch solution; (4) balling through retrogradation and solidification, separation and washing: the emulsified aqueous two-phase emulsion is put in an environment at the temperature of 4-30 DEG C to be retrograded for 24 h, then taken out and subjected to centrifugal separation for 10-15 min, a substrate in a centrifuge tube is washed and then dried for 12 h, and the starch microspheres with the average particle sizes smaller than 10 mu m are obtained. The prepared starch microspheres have the characteristic of being small in particle size, the phenomenon that starch microspheres aggregate due to the fact that the interfacial area between the two phases of the aqueous two-phase emulsion is substantially increased, the interfacial free energy is substantially increased and liquid drops aggregate to reduce the interfacial free energy in the preparation process of the starch microspheres can be avoided, and the preparation method has great application value.
Owner:GUANGXI ACAD OF SCI

Nano-foam oil-displacing agent and preparation method thereof

The invention belongs to the technical field of oil extraction in oil fields, and particularly relates to a nano-foam oil-displacing agent and a preparation method thereof. The oil-displacing agent comprises the following components in percentage by weight: 10-45% of an anionic surfactant, 7-15% of a zwitterionic surfactant, 6-12% of oily nanoparticles, 5-10% of a stabilizer, 1-2% of a dispersingagent and the balance of water. The preparation method of the oil-displacing agent comprises the following steps: preparing oily nanoparticles from solid paraffin and isocaprylic acid, dispersing theoily nanoparticles in water, conducting uniform mixing with a surfactant, and adding a stabilizer and water to prepare the nano-foam oil-displacing agent. The nano-foam oil-displacing agent can effectively inhibit gas diffusion, enhance the mechanical stability and viscosity of a liquid film, effectively prevent external heat from being transferred to the inside, reduce the molecular thermal motion rate, greatly reduce the liquid separation rate of a foam liquid film, enhance the stability of foam and further improve the oil-displacing efficiency.
Owner:滨州市广友石油科技有限公司

A kind of preparation method of expanded polypropylene beads

ActiveCN106543559BLow costPowerful deliveryPolymer sciencePlastic packaging
The invention discloses a preparation method of foamed polypropylene beads. The method comprises the following steps that 1, polypropylene resin, an active filler and auxiliaries are added into a high-speed mixing machine and mixed to be uniform at the temperature of 10-20 DEG C, and a polypropylene foaming material is obtained; 2, the polypropylene foaming material is added into a triple-screw extruder, plastification and mixing are conducted, a supercritical fluid is injected, the mouth mold pressure is controlled to be 5-25 MPa, the mouth mold temperature is 110-160 DEG C, instant pressure release is conducted through a mouth mold, foaming is conducted, and super-fine hole foamed polypropylene is obtained; 3, super-fine hole foamed polypropylene is subjected to mold surface water-ring hot-cutting granulation, drying and sieving, and the foamed polypropylene beads are obtained. The method is low in production cost, high in capacity, safe and environmentally friendly, no foaming agent decomposed residue exists in the prepared foamed polypropylene beads, secondary foaming can be conducted, the foaming ratio can be adjusted, the rebound resilience of a finished product is high, decomposing and recycling are easy, and the foamed polypropylene beads can be widely used in the fields of plastic packaging, transportation industry, military aerospace, office supplies and the like.
Owner:湖北聚石新材料科技有限公司

Preparation technology of painting mist coagulant

The invention discloses a preparation technology of a painting mist coagulant. The technology comprises the following steps of (1) preparation of an adhesive elimination agent, and preparation includes the hydroxymethylation stage and the condensation stage, wherein at the hydroxymethylation stage, deionized water is added to a 500-mL beaker, then melamine and formaldehyde are added in sequence, the pH value is adjusted to 8-9 with triethylamine, and a stirring reaction is conducted for 30-60 min at 60-80 DEG C; at the condensation stage, the pH value of the solution is adjusted to 3-5 with 50% sulfuric acid, a stirring reaction is conducted for 1-3 h at 60-80 DEG C, and transparent liquid, namely the adhesive elimination agent is prepared; (2) preparation of the painting mist coagulant, wherein 300 mL of water is added to the 500-mL beaker, cationic polyacrylamide is added under high-speed stirring, after stirring and dissolution are conducted for certain time, a modification agent and the adhesive elimination agent are added, stirring continues for 0.5 h, and a sticky transparent solution, namely the painting mist coagulant is obtained. According to the preparation technology ofthe painting mist coagulant, through the cooperation effect of all the components, the flocculation performance and paint residue separation effect of the painting mist coagulant are obviously improved, and the aim of removing over-sprayed oil paint in oil paint wastewater is achieved.
Owner:江苏二九建筑装饰工程有限公司

Polylactic acid composition containing carboxylate nucleating agent and preparation method thereof

The invention relates to a polylactic acid composition containing a carboxylate nucleating agent and a preparation method thereof, and belongs to the technical field of polylactic acid processing, the raw materials comprise the carboxylate nucleating agent, an antioxidant, an anti-hydrolysis agent and L-polylactic acid, and the polylactic acid composition is prepared by mixing the raw materials through a high-speed mixer and carrying out twin-screw extrusion granulation. In the preparation process, by using anhydride substances and potassium hydroxide as raw materials and reacting in an aprotic solvent, the anhydride substances are synthesized into a carboxylate nucleating agent containing four carboxylate groups, the carboxylate nucleating agent is uniformly dispersed in a polylactic acid melt in the form of extremely tiny solid particles to serve as heterogeneous crystal nucleuses, the interface free energy required by polylactic acid nucleation crystallization is reduced, so that polylactic acid chain segments are promoted to crystallize simultaneously by taking the crystal nucleus as the center, and the aim of improving the crystallization rate and crystallinity of polylactic acid is fulfilled.
Owner:湖南玥昇杰科技有限责任公司

Polylactic acid composition containing phosphate nucleating agent and preparation method thereof

The invention relates to a polylactic acid composition containing a phosphate nucleating agent and a preparation method thereof, and belongs to the technical field of polylactic acid processing. The raw materials comprise a phosphate nucleating agent, an antioxidant, an anti-hydrolysis agent and L-polylactic acid. The polylactic acid composition is prepared by mixing the raw materials through a high-speed mixer and carrying out twin-screw extrusion granulation. In the preparation process, 2, 2'-methylene bis (4, 6-di-tert-butylphenyl) phosphate is used as a raw material and is subjected to a substitution reaction with an ionic compound under the condition that methanol is used as a solvent to obtain the phosphate nucleating agent containing two symmetrical benzene rings. When a polylactic acid melt is cooled, the phosphate nucleating agent is uniformly dispersed in the polylactic acid melt in the form of extremely tiny solid particles to serve as a heterogeneous crystal nucleus, so that the interface free energy required by polylactic acid nucleation crystallization is reduced, polylactic acid chain segments are promoted to be simultaneously crystallized by taking the crystal nucleus as the center, and the purpose of improving the crystallization rate and crystallinity of polylactic acid is achieved.
Owner:湖南玥昇杰科技有限责任公司

Preparation method with high yield, low cost and environmental protection for polypropylene beads

InactiveCN107602903ALow costPowerful deliveryPolypropyleneCaprolactam
The invention provided a preparation method with high yield, low cost and environmental protection for polypropylene beads. The preparation method is characterized by comprising the following steps: adding polypropylene resin, an active filling material, caprolactam and an auxiliary agent into a high-speed mixer, and carrying out uniform mixing at 10 to 20 DEG C so as to obtain a polypropylene foamed material.
Owner:绵阳旺通科技有限公司

Special automobile exterior trim part material added with waste mask melt-blown material

The invention discloses a special automobile exterior trim part material added with a waste mask melt-blown material. The special automobile exterior trim part material is prepared from the followingraw materials in parts by weight: 80-100 parts of PC resin, 50-60 parts of waste mask reclaimed material, 10-20 parts of flame-retardant filler, 10-15 parts of modified montmorillonite, 5-10 parts ofbasalt fiber, 1-5 parts of flexibilizer, 1-3 parts of light stabilizer and 1-3 parts of coupling agent. The flame-retardant filler is added to endow the composite material with excellent flame retardancy and heat resistance, the modified montmorillonite and the flexibilizer endow the composite material with excellent toughness and impact resistance in inorganic and organic aspects, and the titanium dioxide can scatter and absorb ultraviolet rays, thereby enhancing the aging resistance of the composite material. The melt-blown material in waste masks is utilized to implement secondary high-efficiency utilization of the waste and reduce pollution, so that the special material for the automobile exterior trim part has the characteristics of impact resistance, high-temperature resistance, flame retardancy, low cost, environment friendliness, health and the like.
Owner:ANHUI GUANHONG PLASTIC IND

A kind of preparation method of high-refractive-index high-transparency frictional silica

The invention provides a method for preparing high-refractive-index and high-transparency friction-type silica, comprising the following steps: (1) preparing a sodium silicate solution, adding a surfactant, and stirring evenly; (2) injecting a sodium sulfate solution into a reaction tank , turn on the stirring device and heat to 80-90°C; (3) Add sodium silicate solution to the reaction tank, add sulfuric acid solution at the same time after 0.5-1min, control the pH value at 9.0-9.5, continue to Add sulfuric acid solution to control the pH value at the end of the reaction to 4.4-4.8, stop adding sulfuric acid solution, keep the temperature at 80-85°C, continue stirring and sinking for 10-15min to obtain slurry; (4) The slurry in step (3) Press filtration to obtain a filter cake, wash the filter cake with deionized water, dry and pulverize the washed filter cake to obtain high-refractive index and high-transparency frictional silica. The silicon dioxide prepared by the invention has high refractive index, wide range, transparency up to 99.0%, good cleaning performance and fluorine compatibility.
Owner:GUANGZHOU FEIXUE MATERIAL TECH

A kind of environment-friendly water-soluble cathode electron emission slurry and preparation method thereof

InactiveCN102856154BHigh densityExhaust decomposition is goodGas discharge lampsSlurryDefoaming Agents
The invention relates to environment-friendly water-soluble cathode electron emission slurry, and also simultaneously relates to a preparation method of the environment-friendly water-soluble cathode electron emission slurry. The environment-friendly water-soluble cathode electron emission slurry is prepared from the materials by weight: 50-60% of electronic powders; 20-30% of water, 5-8% of water-soluble binder, 1-2% of hydrophilc agent, 1-2% of defoamer, 3-5% of activating agent, 0-2% of wetting agent, 0-2% of dispersing agent and 0-2% of curing agent. The environment-friendly water-soluble cathode electron emission slurry has the beneficial effects that the environment-friendly water-soluble cathode electron emission slurry is good in stability performance, economical and environment-friendly, excellent in performance, less in impurity and suitable for large-scale production and use; and the emission property of electron and the quality of a lamp tube are improved, and the service life of the lamp tube is prolonged.
Owner:南京双鹿电光源材料有限公司

Preparation method of surface metallized ceramic

The invention discloses surface metallized ceramic as well as a preparation method thereof. The method comprises the following steps: dipping a metallized treatment face of ceramic into aluminum or aluminum alloy melt, wherein the metallized treatment face moves relative to the melt, so that the aluminum or aluminum alloy melt wets the metallized treatment face of the ceramic; and then, moving the metallized treatment face of the ceramic out of the melt for freely cooling an aluminum or aluminum alloy liquid film attached to the surface to obtain the ceramic connected with the aluminum or aluminum alloy thin film on the surface. Compared with the prior art, no amorphous oxide impurities are available on the interface between the ceramic and the aluminum or aluminum alloy thin film, and grains of aluminum or aluminum alloy and ceramic grains directly grow together. The thin film formed is compact in internal tissue and free from oxide impurities. The aluminum or aluminum alloy thin film formed is several microns to dozens of microns in thickness, and the thin film is firm and not easy to fall. Experiments show that the chessboard partitioning and peeling strength of the aluminum or aluminum alloy thin film and the ceramic is greater than or equal to 4.1N / cm. The preparation method disclosed by the invention has a wide application prospect in the field of surface metallization of ceramic.
Owner:TSINGHUA UNIV

A kind of foam cement board and preparation method thereof

The invention relates to the technical field of cements, and concretely relates to a foaming cement slab and a preparation method thereof. The foaming cement slab is mainly prepared from the raw materials: 60 to 70 parts of cement, 10 to 15 parts of tetrasodium iminodisuccinate, 10 to 15 parts of ethylene diamine tetraacetic acid dipotassium ethylene dinitrilotetra-acetic acid, 10 to 15 parts of potassium chromate, 5 to 10 parts of tetrahydro-iso-humulone, 5 to 10 parts of 4,4-diphenylhydrazine diphenyl ether4,4-disulfonylhydrazide diphenyl ether, 5 to 10 parts of 4,4'-p-sulfonylhydrazide diphenyl ether 4,4'-oxybis(benzenesulfonyl hydrazide), 2 to 4 parts of sodium alkyl sulfate, 2 to 4 parts of heavy sodium alkyl benzene sulfonate, 0.3 to 0.5 part of sodium polymethacrylate, 0.3 to 0.5 part of sodium amine sulfonate, 0.5 to 0.7 part of 2,3-dihydrobutanedioic acid, 0.5 to 0.7 part of sodium hexametaphosphate, and the like. The preparation method comprises the steps of mixing the raw materials, injection molding, maintaining, demoulding and the like, and is simple in process and easy to operate. The foaming cement slab provided by the invention is low in heat conductivity coefficient, light in weight, less in water consumption, prolonged in initial setting time, sufficient in foaming, waterproof, and better in heat insulation and sound insulation effects.
Owner:陕西九龙保温工程有限公司

A kind of preparation method of small particle size starch microsphere

The invention discloses a preparation method of starch microspheres with small particle sizes. The preparation method comprises steps as follows: (1) preparation of a starch solution; (2) preparation of a polyvinylpyrrolidone solution; (3) forming of an aqueous two-phase emulsion through high-speed shearing and emulsification performed after the polyvinylpyrrolidone solution is added to the starch solution; (4) balling through retrogradation and solidification, separation and washing: the emulsified aqueous two-phase emulsion is put in an environment at the temperature of 4-30 DEG C to be retrograded for 24 h, then taken out and subjected to centrifugal separation for 10-15 min, a substrate in a centrifuge tube is washed and then dried for 12 h, and the starch microspheres with the average particle sizes smaller than 10 mu m are obtained. The prepared starch microspheres have the characteristic of being small in particle size, the phenomenon that starch microspheres aggregate due to the fact that the interfacial area between the two phases of the aqueous two-phase emulsion is substantially increased, the interfacial free energy is substantially increased and liquid drops aggregate to reduce the interfacial free energy in the preparation process of the starch microspheres can be avoided, and the preparation method has great application value.
Owner:GUANGXI ACAD OF SCI

A kind of nano foam oil displacement agent and preparation method thereof

The invention belongs to the field of oil recovery technology, and in particular relates to a nano-foam oil displacement agent and a preparation method thereof. The oil displacement agent comprises the following components in weight percentage: 10-45% of anionic surfactant, 7-15% of zwitterionic surfactant, 6-12% of oily nanoparticles, 5-10% of stabilizer, and 1-10% of dispersant 2%, the balance is water. The preparation method of the oil-displacing agent is as follows: prepare oily nanoparticles through solid paraffin and isooctanoic acid, then disperse the oily nanoparticles in water and mix them with a surfactant, then add a stabilizer and water to make a nano-foam oil-displacing agent . The nano-foam oil displacement agent can effectively inhibit gas diffusion, enhance the mechanical stability and viscosity of the liquid film, effectively isolate the transfer of external heat to the interior, reduce the thermal movement rate of molecules, greatly slow down the liquid separation rate of the foam liquid film, and enhance the foam's stability. stability, thereby improving the oil displacement efficiency.
Owner:滨州市广友石油科技有限公司

Surface metallised ceramic and manufacturing method thereof

The invention discloses a surface metallised ceramic and a manufacturing method thereof. The method comprises the following operation steps of immersing a metallised surface of the ceramic in an aluminium or aluminium alloy melt, making the metallised surface move with respect to the melt such that the aluminium or aluminium alloy melt wets the metallised surface of the ceramic, taking out the metallised surface of the ceramic from the melt and freely cooling the aluminium or aluminium alloy film attached to the surface, so as to obtain the ceramic with the surface connected with the aluminium or aluminium alloy film. Compared with prior art, the interface between the ceramic and the aluminium or the aluminium alloy film in the invention does not contain amorphous oxide. The aluminium or aluminium alloy crystal grains and the ceramic crystal grains are grown together. The internal organisations of the formed film are compact and do not contain oxide. The formed aluminium or aluminium alloy film has a thickness in a range from several microns to more than ten microns, is firm, and cannot easily fall off. The chessboard division peeling strength between the aluminium or the aluminium alloy film and the ceramic is proved, by experiments, to be greater than or equal to 4.1N / cm. The invention has wide application prospect in the surface metallising field of ceramic.
Owner:TSINGHUA UNIV

Preparation method of silibinin nano-cage type nanocrystalline injection

The invention discloses a preparation method of a silibinin nano-cage type nanocrystalline injection and belongs to the technical field of medicines. The nano-cage type nanocrystalline injection is prepared from ingredients as follows: an active ingredient, namely, silibinin, a nano-cage type nanocrystalline drug release system and an organic solvent used for dissolving the active ingredient, namely, silibinin, wherein the nano-cage type nanocrystalline drug release system is formed by PEG-PCL (polyethylene glycol-polycaprolactone) and PEG-CS (polyethylene glycol-chitosan). The prepared silibinin nano-cage type nanocrystalline injection has good physical stability, the blood circulation time of the drug can be prolonged after drug administration, the relative bioavailability is improved, the average retention time in vivo is prolonged, and the silibinin nano-cage type nanocrystalline injection has long cyclicity and passive targeting property.
Owner:QILU UNIV OF TECH

A kind of modified natural zeolite warm mixing agent and preparation method thereof

The invention belongs to the field of road construction materials, in particular relates to a modified natural zeolite warm mixing agent and a preparation method of the modified natural zeolite warm mixing agent. The modified natural zeolite warm mixing agent is prepared by carrying out alkaline solution treatment and fatty amine modification on natural zeolite. According to the modified natural zeolite warm mixing agent disclosed by the invention, the water content of the modified natural zeolite warm mixing agent is higher, so that the mixing and paving temperature of an asphalt mixture can be effectively reduced; a non-polar group of fatty amine in the modified natural zeolite warm mixing agent has very strong affinity with asphalt, and a polar group has very strong affinity with aggregate surfaces (particularly, acidic aggregates such as basalt), so that the interfacial free energy of the aggregates and the asphalt can be effectively reduced, the adhesion of the asphalt and the aggregates is improved, the water stability of the asphalt mixture is increased, and a water damage phenomenon of an asphalt pavement is effectively prevented from happening; raw materials of the modified natural zeolite warm mixing agent prepared by the invention are easy to obtain and low in cost, and the modified natural zeolite warm mixing agent is capable of obviously reducing the cost of a warm mixing asphalt mixture, and is beneficial for being widely applied.
Owner:WUHAN UNIV OF TECH

A binary fluoropolymer wetting reversal agent and its preparation method and application

The invention relates to a binary fluorine-containing polymer wet reversal agent, a preparation method and application thereof. Use dodecafluoroheptyl methacrylate and 2-(perfluorohexyl) ethyl methacrylate binary monomer to polymerize with acrylic monomer in the presence of an initiator to obtain a binary fluoropolymer microemulsion wet inversion agent. The binary fluorine-containing polymer emulsion prepared by the present invention is used as a wetting reversal agent, which is stably dispersed in a water-based system. After use, the contact angle between the formation and water can reach 142°, which significantly improves the wettability of the formation and reduces the The interfacial free energy of the reservoir is improved, and the oil and gas recovery is enhanced.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
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