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37results about How to "Uniform particle size dispersion" patented technology

High-tap-density lithium iron manganese phosphate positive electrode material, preparation method and applications thereof

The invention belongs to the technical field of lithium ion batteries, and particularly relates to a high-tap-density lithium iron manganese phosphate positive electrode material, a preparation methodand applications thereof, wherein the positive electrode material is formed by mixing small particle lithium iron manganese phosphate with a particle size of 0.3-0.8 [mu]m and large particle lithiumiron manganese phosphate with a particle size of 3-5 [mu]m according to a mass ratio of 1-9:9-1. The preparation method comprises: (1) preparation of dense iron manganese phosphate; (2) preparation oflarge particle lithium iron manganese phosphate slurry and small particle lithium iron manganese phosphate slurry; (3) preparation of lithium iron manganese phosphate precursor powder; and (4) preparation of lithium iron manganese phosphate finished product, wherein the obtained material is used for lithium battery positive electrode materials. According to the present invention, the prepared lithium iron manganese phosphate has advantages of high tap density, high electrical capacity, good rate performance, high charge and discharge efficiency and large gram capacity, and the preparation method has advantages of simple preparation process, easy control, low energy consumption, low raw material cost and high production efficiency, and is suitable for large-scale industrial production.
Owner:江苏元景锂粉工业有限公司

Method for preparing organosilicone stripping agent by emulsion polymerizing

InactiveCN107739440AAdjust particle size distributionAdjust the degree of spreadPolymer sciencePtru catalyst
The invention relates to a method for preparing an organosilicone stripping agent, in particular to a method for preparing the organosilicone stripping agent by emulsion polymerizing. The method adopts the emulsion polymerizing technology to prepare the organosilicone stripping agent at one time. The method comprises the following steps of adding deionized water, a catalyst, an end capping agent and an organosilicone ring body into a reaction kettle according to a ratio, and stirring at the temperature of 40 to 60 DEG C, so as to obtain a prepolymer emulsion; adding an emulsifier, a surfactantand a structure control agent, and reacting for 4 to 6h at the temperature of 80 to 95 DEG C; adding a terminating agent, and adjusting the pH (potential of hydrogen) value of the emulsion to the neutral property, so as to obtain the neutral organosilicone stripping agent emulsion. The method has the advantages that the emulsion polymerizing method is adopted, the water is used as a dispersant and can be easily sprayed, and the particle size of the emulsified particle is small. The prepared organosilicone stripping agent has the advantages that the application range is broad, the preparationcost is low, the hazard to environment and health of human body is avoided, and the stripping force on a rubber and plastic product is greatly improved.
Owner:TANGSHAN SANYOU SILICON IND

Instant whole lotus root powder containing highly-resistant starch and preparation method of instant whole lotus root powder containing highly-resistant starch

The invention belongs to the technical field of food and particularly discloses instant whole lotus root powder containing highly-resistant starch and a preparation method of the instant whole lotus root powder containing the highly-resistant starch. The preparation method includes subjecting fresh lotus roots taken as a raw material to washing, peeling, slicing, color protection, pulping and cryogenic grinding so as to obtain fresh lotus root pulp; subjecting the fresh lotus root pulp to limited-enzyme hydrolysis-drum drying, crosslinking adsorption, complexing, vacuum drying, grinding, blending, extruding granulation, sieving and packaging so as to obtain the instant whole lotus root powder containing the highly-resistant starch. The instant whole lotus root powder containing highly-resistant starch and the preparation method have the advantages that since embedded crosslinking, complexing, enzymatic debranching treatment and drum drying are combined to be applied to a whole lotus root powder production process, reconstituability of the whole lotus root powder can be improved, liquidity and solubility of the whole lotus root powder can be increased, resistant starch content in the whole lotus root powder can be increased, and the whole lotus root powder can have a certain effect on intestinal microecological balance regulation and gastrointestinal function improvement; powder granules produced by extruding granulation are uniform, loose and porous and can swell and gelatinize within short time, and accordingly the whole lotus root powder is excellent in instant solubility and wettability.
Owner:FUJIAN AGRI & FORESTRY UNIV

Method for preparing nanometer ferroferric oxide through acid-regenerating desilicated mud cake

The invention discloses a method for preparing nanometer ferroferric oxide through acid-regenerating desilicated mud cake. The method comprises the steps as follows: adding water to desilicated mud cake, heating and pulping to obtain desilicated slurry which has good dispersibility; and then adding acid for regeneration to the obtained desilicated slurry; heating and uniformly agitating; then adding thin iron rim charge after reacting for 2 hours; heating to 80 to 90 DEG C so as to achieve acid dissolution and reduction to the desilicated mud cake; filtering, washing with water, and adjusting pH to 4 through ammonia water to obtain filtrate which is ferrous chloride turbid solution; further adding fatty acid to carry out oxidization; centrifuging, washing and drying to obtain nanometer ferroferric oxide rough product; finally ultrasonically dispersing the nanometer ferroferric oxide rough product into the water; magnetically attracting and separating; and then drying in a vacuum drying box at 60 to 90 DEG C so as to obtain nanometer ferroferric oxide. According to the method for preparing nanometer ferroferric oxide through acid-regenerating desilicated mud cake disclosed by the invention, the recycling and reusing of industrial waste desilicated mud cake is achieved, and the environmental pollution can be reduced.
Owner:SHANGHAI APPLIED TECHNOLOGIES COLLEGE

Method for preparing Crisaborole soluble film preparations and application thereof

The invention discloses a method for locally releasing Crisaborole in a sustained manner. The method includes a method for preparing Crisaborole soluble film preparations. The method for preparing theCrisaborole soluble film preparations is characterized by comprising steps of S1, selecting ionic active agents with (-CH2-) and the chain lengths of 3-15 to be used as raw materials for dispersing agents, and selecting alcohol substances to be used as stabilizers for the corresponding dispersing agents; S2, carrying out gas dispersion on Crisaborole original medicines in the ultrasonic intensityranges of 60-80 W/m<2>, then adding the raw materials for the dispersing agents, carrying out treatment in room-temperature keeping environments for 20-40 minutes, adding the stabilizers, and carrying out ultrasonic treatment under identical intensity conditions for 20-30 minutes to form wide distribution stock solution; S3, continuously filtering the stock solution by the aid of filter paper with the filter hole specifications of 0.22 micrometer by 2-3 times and collecting filter liquor to obtain the single-distribution Crisaborole soluble film preparations with the sizes of 0.10-0.15 micrometer. According to the technical scheme, the method has the advantages that the ionic active agents with the appropriate lengths are selected, the ultrasonic intensity is controlled, accordingly, finished medicine products with uniformly dispersed particle sizes and stable and controllable release curves can be obtained, and the practicality can be improved.
Owner:SUZHOU ZHIYU BIOTECH CO LTD

Positive electrode material of lithium-sulfur battery and preparation method thereof

The invention provides a positive electrode material of a lithium-sulfur battery and a preparation method thereof, and aims at improving the electronic and electric conductivity so as to improve the capacity of a positive electrode of the lithium-sulfur battery and prolong the circle life of the lithium-sulfur battery, and solving the problem that the capacity of the positive electrode of the lithium-sulfur battery rapidly decreases, resulting in short circle life of the battery. The positive electrode material is characterized in that a BaTiO3 material is introduced, so that the electronic and electric conductivity of the positive electrode material can be improved, and the capacity and the circulating performance of the electrode can be effectively improved; the introduced porous carbonmaterial is high in specific area and high pore distribution performance, and a large number of elemental sulfur can be stored, so that high sulfur content in a composition is ensured; sulfur is uniformly distributed in porous carbon, so that the utilization rate of active substances of the sulfur can be increased; the pore channel structure of the porous carbon relieves the dissolution loss of anintermediate product which is polysulfide lithium, thus the shuttling effect is reduced; the service life of the battery is prolonged, and the coulombic efficiency is improved. The preparation methodis simple in processes, simple in equipment, short in manufacturing period, easy to operate, low in energy consumption, environmentally friendly, and easy for industrial production.
Owner:吉林省东驰新能源科技有限公司

A high tap density lithium manganese iron phosphate positive electrode material and its preparation method and application

The invention belongs to the technical field of lithium ion batteries, and in particular relates to a high tap density lithium manganese iron phosphate positive electrode material and a preparation method and application thereof. The positive electrode material is prepared by mixing small particles of lithium manganese iron phosphate with a particle size of 0.3-0.8um and large particles of lithium manganese iron phosphate with a particle size of 3-5um in a mass ratio of 1-9:9-1, and the preparation method includes : (1) Preparation of dense ferromanganese phosphate; (2) Preparation of large and small particles of lithium iron manganese phosphate slurry; (3) Preparation of lithium iron manganese phosphate precursor powder; (4) Preparation of finished product of lithium iron manganese phosphate ; The obtained material is applied to the positive electrode material of lithium battery. The lithium manganese iron phosphate prepared by the invention has high tap density, high electrical capacity, good rate performance, high charge and discharge efficiency, large gram capacity, simple preparation process and easy control, low energy consumption and raw material cost, high production efficiency, It can be applied to large-scale industrial production.
Owner:江苏元景锂粉工业有限公司

A kind of jicama dietary fiber powder with prebiotic function and preparation method thereof

The invention discloses yam bean dietary fiber powder with a prebiotic function and a preparation method thereof.The yam bean powder is prepared by taking fresh yam bean tuberous roots as raw materials through the steps of cleaning, peeling, slicing, color protecting, first-time grinding, freezing grinding, limited enzymolysis performing and drum drying, crosslinking adsorbing, complexing, secondary grinding, mixing, extrusion granulating, sieving and packaging, the prepared yam bean powder retains all dietary fibers of the yam beans and the original flavor of the yam beans, contains high-resistance starch and has the instant solubility and the prebiotic function.According to the yam bean dietary fiber powder with the prebiotic function and the preparation method thereof, embedding crosslinking, complexing, enzymatic debranching treating and drum drying are combined to be applied to the production process of the yam bean dietary fiber powder, the dissolving ability of the yam bean powder can be effectively improved, the fluidity and solubility are improved, the content of the resistance starch in the product is increased, and the significant effects on regulating the intestinal microecological balance and improving the gastrointestinal function are achieved; in addition, powder granules produced through extrusion granulating are uniform in granule size, loosened and porous and can be swelled and gelatinized in a short time, and therefore the good instant solubility and wet permeability are achieved.
Owner:FUJIAN AGRI & FORESTRY UNIV

A preparation method of la0.7ca0.25sr0.05mno3 ferromagnetic film

InactiveCN103833358BConcentration adjustableNo vacuum requiredMANGANESE ACETATEFilm material
The invention relates to a preparation method of a thin film material, and more specifically relates to a preparation method of a La0.7Ca0.25Sr0.05MnO3 ferromagnetic thin film. The preparation method comprises following steps: 1, lanthanum nitrate is added into a mixed solution of glacial acetic acid and ethylene glycol monomethyl ether so as to obtain a solution A; 2, a mixture of calcium acetate and strontium nitrate is added into the mixed solution of glacial acetic acid and ethylene glycol monomethyl ether so as to obtain a solution B; 3, manganese acetate is added into the solution B so as to obtain a solution C; 4, the solution A is mixed with the solution C, and 1 to 10ml of acetic acid is added so as to obtain a La0.7Ca0.25Sr0.05MnO3 solution; 5, a substrate is subjected to ultrasonic processing in acetone and absolute ethyl alcohol successively; 6, the La0.7Ca0.25Sr0.05MnO3 solution is added onto the processed substrate dropwise for spin coating so as to obtain a thin film D; 7, the thin film D is subjected to presintering so as to obtain a thin film E; 8, the thin film E is delivered into a rapid heat treatment furnace for roasting, and is cooled with the rapid heat treatment furnace to room temperature so as to obtain the La0.7Ca0.25Sr0.05MnO3 ferromagnetic thin film. The preparation method is capable of solving problems of existing technology used for preparing the La0.7Ca0.25Sr0.05MnO3 (LCSMO) ferromagnetic thin film that performance is poor, purity is low, density is low, and sintering temperature is too high in preparation processes. The LCSMO ferromagnetic thin film with uniform film thickness and excellent magnetocaloric effects is prepared via modified sol-gel method.
Owner:JILIN NORMAL UNIV

A kind of blue fluorescent powder for white light LED and preparation method thereof

The invention relates to a blue fluorescent powder for white-light LED and a preparation method thereof. The chemical formula of the powder is Sc<4-4x>Al6Si3O21:4xCe<3+>; wherein in the formula, x represents the mole doping amount of rare earth activated ions (Ce3+), which are doped on the Sc3+ positions, 0.001<=x<=0.700. The prepared fluorescent powder can be well activated by the ultraviolet lights with a wavelength of 300 to 400 nanometers. The fluorescent powder can emit blue lights having a main peak at 425 nanometers, and thus the fluorescent powder can be well matched with an ultraviolet LED. The fluorescent is prepared by mixing compounds containing the required elements through a high-temperature solid-phase method or chemical synthesis method. The technology is simple and flexible, the repeatability is good, the operation is easy, the sources of the raw materials are wide, the chemical stability and thermal stability of the obtained products are both very good, crystallizing property of the synthesized fluorescent powder is good, the morphology is regular, the particle size is uniform, the luminescent efficiency is high, and thus the fluorescent powder is suitable for the preparation of LEDs excited by ultraviolet lights or near ultraviolet lights.
Owner:徐州博创建设发展集团有限公司

A kind of positive electrode material of lithium-sulfur battery and preparation method thereof

The invention provides a positive electrode material of a lithium-sulfur battery and a preparation method thereof, and aims at improving the electronic and electric conductivity so as to improve the capacity of a positive electrode of the lithium-sulfur battery and prolong the circle life of the lithium-sulfur battery, and solving the problem that the capacity of the positive electrode of the lithium-sulfur battery rapidly decreases, resulting in short circle life of the battery. The positive electrode material is characterized in that a BaTiO3 material is introduced, so that the electronic and electric conductivity of the positive electrode material can be improved, and the capacity and the circulating performance of the electrode can be effectively improved; the introduced porous carbonmaterial is high in specific area and high pore distribution performance, and a large number of elemental sulfur can be stored, so that high sulfur content in a composition is ensured; sulfur is uniformly distributed in porous carbon, so that the utilization rate of active substances of the sulfur can be increased; the pore channel structure of the porous carbon relieves the dissolution loss of anintermediate product which is polysulfide lithium, thus the shuttling effect is reduced; the service life of the battery is prolonged, and the coulombic efficiency is improved. The preparation methodis simple in processes, simple in equipment, short in manufacturing period, easy to operate, low in energy consumption, environmentally friendly, and easy for industrial production.
Owner:吉林省东驰新能源科技有限公司

A kind of high resistant starch instant whole lotus root powder and its preparation method

The invention belongs to the technical field of food and particularly discloses instant whole lotus root powder containing highly-resistant starch and a preparation method of the instant whole lotus root powder containing the highly-resistant starch. The preparation method includes subjecting fresh lotus roots taken as a raw material to washing, peeling, slicing, color protection, pulping and cryogenic grinding so as to obtain fresh lotus root pulp; subjecting the fresh lotus root pulp to limited-enzyme hydrolysis-drum drying, crosslinking adsorption, complexing, vacuum drying, grinding, blending, extruding granulation, sieving and packaging so as to obtain the instant whole lotus root powder containing the highly-resistant starch. The instant whole lotus root powder containing highly-resistant starch and the preparation method have the advantages that since embedded crosslinking, complexing, enzymatic debranching treatment and drum drying are combined to be applied to a whole lotus root powder production process, reconstituability of the whole lotus root powder can be improved, liquidity and solubility of the whole lotus root powder can be increased, resistant starch content in the whole lotus root powder can be increased, and the whole lotus root powder can have a certain effect on intestinal microecological balance regulation and gastrointestinal function improvement; powder granules produced by extruding granulation are uniform, loose and porous and can swell and gelatinize within short time, and accordingly the whole lotus root powder is excellent in instant solubility and wettability.
Owner:FUJIAN AGRI & FORESTRY UNIV

A multi-purpose polylysine fluorescent self-assembled nano-microsphere carrier and its preparation method and application

The invention discloses a multipurpose polylysine fluorescence self-assembly nano microsphere carrier and a preparation method and application thereof. By nano self-assembly technique, rhodamine marked polylysine fluorescence self-assembly nano microspheres can be prepared, azide group side chains with disulfide bonds can be modified, and by use of a click chemistry method, an alkynyl modified drug is connected with the fluorescent nano microspheres. The polylysine self-assembly nano microspheres linked with the drug can be used for tracing imaging analysis of the modified drug in animal and cell level. At the same time, the polylysine self-assembly nano microspheres can also be used to capture binding proteins of the modified drug, can release target binding proteins and associated proteins by cleavage of the disulfide bonds, and can be used for the study of drug effect targets. The invention provides a simple and fast tool and method for the study of the drug effect targets, and the method integrates drug tracing, target positioning and target protein capture and separation functions, is simple and practical, and has good application prospect in the study of drug action mechanisms and target discovery.
Owner:NANKAI UNIV
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