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34 results about "Di-sec-octyl phthalate" patented technology

Continuous alcohol-removing device and alcohol-removing method of di-sec-octyl phthalate

InactiveCN102173991AContinuous dealcoholization achievedGood dealcoholization effectOrganic compound preparationCarboxylic acid esters preparationAlcoholRelative pressure
The invention discloses a continuous dealcoholizing device and dealcoholizing method of di-sec-octyl phthalate. The dealcoholizing device comprises an dealcoholizing tower and a stripping tower which are connected in series. The dealcoholizing method comprises the following steps: the material obtained through esterification enters the dealcoholizing tower first to re-dealcoholize under the conditions that the material temperature is 160-180 DEG C, the relative pressure is from -0.08MPa to -0.09 MPa, the top gas-phase temperature is more than 90 DEG C and the relative pressure is no more than -0.084MPa; the re-dealcoholized material enters the stripping tower to dealcoholize under the conditions that the material temperature is 160-180 DEG C, the relative pressure is from -0.083MPa to -0.09MPa, the top gas-phase temperature is 120-170 DEG C and the relative pressure is no more than -0.088MPa; and introducing saturated steam in a saturated steam distributor to perform stripping. In the invention, the continuous dealcoholizing production method is adopted; and the residence time of the material in the device is short, the energy consumption is low, the product purity is high, the quality is stable, and the quality and production efficiency of di-sec-octyl phthalate can be increased.
Owner:WEIFANG YUANLI CHEM

Preparation method of ethylene glycol gemini di-sec-octyl phthalate sodium sulfosuccinate

The invention discloses a preparation method of ethylene glycol gemini di-sec-octyl phthalate sodium sulfosuccinate. The preparation method of ethylene glycol gemini di-n-octyl phthalate sodium sulfosuccinate comprises the following steps: carrying out a mono-esterification reaction for combining maleic anhydride with two hydroxyls on ethylene glycol, so as to generate ethylene glycol di-maleic acid monoester, then carrying out a double-esterification reaction on ethylene glycol di-maleic acid monoester and sec-octyl alcohol to obtain ethylene glycol di-maleic anhydride di-sec-octyl phthalate, and finally carrying out a conjugate addition sulfonation reaction on ethylene glycol di-maleic anhydride di-sec-octyl phthalate and sodium hydrogen sulfite to obtain the ethylene glycol gemini di-sec-octyl phthalate sodium sulfosuccinate product, wherein a catalyst used in the mono-esterification reaction is carbon-based solid acid, and the carbon-based solid acid after the mono-esterification reaction is carried out is directly taken as a catalyst of the double-esterification reaction. The preparation method of ethylene glycol gemini di-sec-octyl phthalate sodium sulfosuccinate is simple, easy to operate and good in environmental protection property.
Owner:NANTONG UNIVERSITY

Plastic composition resistant to methanol fuel and gasoline and preparation method of composition

InactiveCN107828094AAnti-agingForm corrosion resistancePolyvinyl chlorideSolvent
The invention provides a plastic composition resistant to a methanol fuel and gasoline, and relates to the technical fields of vehicle material compositions and production. The composition includes abasic rubber variety, an additive and an anti-aging agent; and the composition concretely comprises the following materials in parts by weight: 50-80 parts of acrylonitrile-butadiene rubber, 20-40 parts of polyvinyl chloride (PVC), 3-6 parts of zinc oxide, 1-3 parts of stearic acid, 0.5-2 parts of sulphur, 1-3 parts of anti-ozone wax, 0.5 part of di-sec-octyl phthalate, 30-50 parts of carbon blackN774 (N774), 20-30 parts of carbon black N330 (N330), 20 parts of barium sulfate, 5-7 parts of liquid butyronitrile, and 3-8 parts of the anti-aging agent. The invention also provides a preparation method of the plastic composition. According to the method provided by the invention, the plastic composition is prepared by co-mixing of the acrylonitrile-butadiene rubber and the polyvinyl chloride,and has the advantages of excellent aging resistance, oil resistance, solvent resistance and chemical corrosion resistance, and additives such as the zinc oxide and the anti-aging agent are added, sothat the material can have corrosion resistance to methanol and gasoline after being shaped.
Owner:HUNAN GEELY AUTOMOBILE COMPONENTS +1

Rubber material for oil-resistant, high-temperature, and high-pressure gaskets and preparation method thereof

The invention discloses an oil-resistant and high temperature-resistant high-pressure washer rubber material and a preparation method thereof. The oil-resistant and high temperature-resistant high-pressure washer rubber material is prepared from the following raw materials in parts by weight: 70 to 90 parts of nitrile rubber, 20 to 30 parts of chloroprene rubber, 18 to 22 parts of vinylidene fluoride / chlorotrifluor ethylene copolymer, 5 to 8 parts of epoxidized fatty acid methyl ester, 6 to 8 parts of dicapryl phthalate, 4 to 5 parts of anilmomethyl triethoxy silane, 12 to 16 parts of asphalt oil and the like. The oil-resistant and high temperature-resistant high-pressure washer rubber material has the advantages that by using the nitrile rubber, the chloroprene rubber and the vinylidene fluoride / chlorotrifluor ethylene copolymer as base materials, the good oil-resistant and high temperature-resistant properties are realized; the added dicapryl phthalate and epoxidized soybean oil form a complex plasticizer, and the complex plasticizer is compounded with the epoxidized fatty acid methyl ester, so that the high temperature-resistant property and processing property are improved, and the elasticity and flexibility of the rubber are improved; by adding raw materials of aluminum phosphite, sodium antimonate, basic magnesium chloride whiskers and the like, the flame-retardant property is good; by adding raw materials of silicon boride, precipitated white carbon black, white jade powder and the like, the oil-resistant property of a product is improved, and the abrasion-resistant property of the product is enhanced.
Owner:潘赵翔

Elastic grouting water-stop glue

The invention relates to elastic grouting water-stop glue. The invention relates to a polyurethane hot melt adhesive which comprises the following components in percentage by weight: 40%-41% of polyether polyol, 7.3%-7.7% of polyphenyl polymethylene polyisocyanate, 26%-28.5% of plasticizer, 23.5%-24.5% of filler, 0.2%-0.4% of pigment and 0.2%-0.6% of antioxidant. The plasticizer is prepared by mixing four of dioctyl phthalate, diisooctyl terephthalate, dinonyl phthalate, butyl benzyl phthalate, di-sec-octyl phthalate, fatty acid methyl ester, acetyl tributyl citrate, tributyl citrate and chlorinated paraffin; the plasticizer is prepared by mixing four of dioctyl phthalate, diisooctyl terephthalate, dinonyl phthalate, butyl benzyl phthalate, di-sec-octyl phthalate, fatty acid methyl ester, acetyl tributyl citrate, tributyl citrate and chlorinated paraffin; the antioxidant is formed by mixing one or two of octadecanol propionate, bis (stearoyl) thiodipropionate, bis (cinnamoyl) thiodipropionate and polysiloxane; the antioxidant is formed by mixing one or two of octadecanol propionate, bis (stearoyl) thiodipropionate, bis (cinnamoyl) thiodipropionate and polysiloxane; the filler is formed by mixing one or two of calcium carbonate, diatomite, talcum powder and carbon fiber; the pigment is formed by mixing one or two of carbon black and graphite.
Owner:SHENYANG GUOJIAN XINTEC TECH DEV
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