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33results about How to "Guaranteed nitrogen content" patented technology

Flux-cored wire used for super duplex stainless steel gas shielded welding and preparation method thereof

The invention discloses a flux-cored wire used for super duplex stainless steel gas shielded welding and a preparation method thereof. The flux-cored wire is composed of an external use steel belt andflux powder, wherein the external use steel belt is made of an austenitic stainless steel belt with 17.0%-18.0% of chromium and 11.0%-12.5% of nickel; and the flux powder comprises the following components of, in percentage by weight, 36.0%-38.0% of chromium powder, 9.0%-13.0% of high-nitrogen chromium iron, 2.5%-3.0% of electrolytic manganese metal, 4.0%-5.0% of molybdenum powder, 0.5%-1.0% of ferrosilicon, 1.0%-1.5% of ferrotitanium, 0.5%-1.0% of aluminum-magnesium alloy, 18.0%-20.0% of rutile, 1.0%-2.0% of quartz, 5.0%-6.0% of zircon sand, 1.0%-1.5% of potassium feldspar, 3.0%-3.5% of albite, 1.0%-1.5% of fluorite, 0.5%-1.0% of sodium cryolite, 1.0%-1.5% of potassium titanate, 0.1%-0.3% of bismuth oxide and the balance iron powder. According to the flux-cored wire used for super duplexstainless steel gas shielded welding and the preparation method thereof, the components and the two-phase proportion of deposited metal can be balanced, thus obtaining a duplex stainless steel welding joint which is good in forming quality and excellent in corrosion resistance.
Owner:CENT RES INST OF BUILDING & CONSTR CO LTD MCC GRP

System and method for removing sulfur and mercury out of flue gas by adding organic catalyst to wet spraying absorption tower

The invention discloses a system for removing sulfur and mercury out of flue gas by adding an organic catalyst to a wet spraying absorption tower. The system comprises flue gas absorption equipment, ammonia water storage and supply equipment, dust separation and catalyst recycling equipment, evaporative crystallization equipment and process water equipment, wherein the ammonia water storage and supply equipment and the dust separation and catalyst recycling equipment are respectively communicated with the flue gas absorption equipment; the dust separation and catalyst recycling equipment is connected with the evaporative crystallization equipment; and the evaporative crystallization equipment is connected with the process water equipment. The invention simultaneously discloses a method for removing sulfur and mercury by utilizing the system. The mixture of the organic catalyst and emulsion comes into countercurrent contact with flue gas in the wet spraying absorption tower and purify and absorb the flue gas and then desulfurization saline solution is sent to a three-phase separator and the evaporative crystallization equipment to produce ammonium sulfate, thus reaching the aims of multi-effect control of the flue gas, energy conservation, consumption reduction and cost reduction.
Owner:光阳工程技术有限公司

Refrigerator

The invention provides a refrigerator. The refrigerator comprises a box body, a gas adjusting membrane assembly and a gas sucking pump assembly. A storing space and a compressor cabin are defined inside the box body. A storing container is arranged in the storing space, and a refreshment space is defined inside the storing container. The gas adjusting membrane assembly is arranged in the way that oxygen in airflow of a surrounding space of the gas adjusting membrane assembly can more penetrate through a gas adjusting membrane to enter an oxygen-enriched gas collecting cavity relative to nitrogen in the airflow. The inlet end of the gas sucking pump assembly communicates with the oxygen-enriched gas collecting cavity in a controlled mode through a pipeline and a pipeline switching mechanism, so that gas in the oxygen-enriched gas collecting cavity is pumped to the outside of the refreshment space, and the actual nitrogen content in the refreshment space is within the range of 81% to 98%. According to the refrigerator disclosed by the invention, the actual nitrogen content in the refreshment space is within a proper range, and aerobic respiration strength of a food material can be effectively lowered; and meanwhile, a basic respiration effect is guaranteed, anaerobic respiration of the food material is avoided, and therefore the storage effect of the food material is improved and the refreshing time of the food material is prolonged.
Owner:大连海尔电冰箱有限公司 +2

Smelting and casting process for smelting high-nitrogen non-magnetic stainless steel by using argon oxygen furnace

The invention relates to a smelting and casting process for smelting high-nitrogen non-magnetic stainless steel by using an argon oxygen furnace. The process comprises the following steps: firstly, melting 510-530kg/t of returned stub bars, 300-320kg/t of high-carbon ferrochrome, 8-40kg/t of ferromolybdenum, 14-30kg/t of electrolytic nickel and 5-10kg/t of carburant by using an intermediate frequency furnace, sampling the steel when the temperature is greater than or equal to 1560 DEG C, and then, putting the steel into the argon oxygen furnace; then, supplementing alloy into the argon oxygenfurnace according to the sampling result, performing decarburization to be less than 0.01%, adding 10-25kg/t of special ferrosilicon for reduction, adding 200-240 kg/t of electrolytic manganese, adding 5-10kg/t of aluminum, raising the temperature, and adding 20-30kg/t of ferromanganese nitride alloy in two batches; discharging the steel into a steel ladle; and transferring the steel to a pouringstation to be molded by pouring by adopting a top pouring method, and adding 0.5-1kg/t of protecting slag into the mold. The process provided by the invention is environment-friendly and low in cost and increases the utilization ratio of molten steel by 8%; and by adding the protecting slag into the mold, the surface quality of an electrode blank is ensured, and mold release is facilitated.
Owner:HENAN ZHONGYUAN SPECIAL STEEL EQUIP MFG CO LTD

Method for preparing nitrided ferrovanadium

InactiveCN107829018APrevent the reaction temperature from droppingShort processSlagNitrogen gas
The invention discloses a method for preparing nitrided ferrovanadium. The method comprises the following steps that (1), a sample fabricated by uniformly mixing and pressing vanadium oxide powder, iron powder and carbon powder is subjected to prereduction through the nitrogen gas in a heating furnace, in the prereduction process, the temperature in the heating furnace is 650 +/-20 DEG C, the nitrogen gas flow is 150-180 L/h, and the heat preservation time of the heating furnace is 3-5 hours; (2), after heat preservation in step (1) is finished, the temperature of the heating furnace is then increased to 1200-1500 DEG C to perform final reduction on the sample, in the final reduction process, the nitrogen gas flow in the heating furnace is 150-180 L/h, and the heat preservation time of theheating furnace is 2-3 hours; (3), after heat preservation in step (2) is finished, the sample is cooled along with the furnace in the atmosphere of the nitrogen gas, and an obtained product is the nitrided ferrovanadium. According to the method, the vanadium oxide powder serves as the raw material, the iron powder serves as the iron source, the carbon powder serves as a reducing agent, the nitrogen gas is introduced into the heating furnace for reaction, and the method has the advantages that the procedure is simple, no vanadium slag is generated, the vanadium utilization rate is high, resources are saved, the environment is protected, and the production cost can be lowered.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY

Water-soluble solid silicon fertilizer and production method and preparation device thereof

The invention belongs to the technical field of inorganic silicon and particularly relates to water-soluble solid silicon fertilizer and a production method and a preparation device thereof. The water-soluble silicon fertilizer is prepared from, by weight, 40-60% of quick-resolving sodium silicate, 10-20% of sodium humate, 10-20% of urea, 5-10% of magnesium sulfate, 5-10% of liquid sodium silicate and 0.1-0.2% of sodium carboxymethyl cellulose, wherein the modulus of the quick-resolving sodium silicate is 2.85-3.0, the content of water-soluble silicon elements in the quick-resolving sodium silicate is calculated as 50-75% according to the content of silicon dioxide, the modulus of the liquid sodium silicate is 3.2-3.3, and the content of water-soluble silicon elements in the liquid sodium silicate is calculated as 26-27% according to the content of silicon dioxide. The content of water-soluble silicon dioxide of the water-soluble silicon fertilizer is high, the fertilizer application amount is small, the cost performance is high, the water-soluble solid silicon fertilizer can be applied as base fertilizer for plants and can also be applied to topdressing of water flush fertilizer, and the water-soluble solid silicon fertilizer can be widely applied to all soil lacking silicon.
Owner:山东龙港硅业科技有限公司

Organic fertilizer prepared from recovered wastes of pig farm and preparation method thereof

The invention discloses an organic fertilizer prepared from recovered wastes of a pig farm and a preparation method thereof. The method comprises the following steps: preparing lichens, mellea armillaria sporophore, stillage, yeast powder, cake pulp, brown sugar, honey and a proper amount of water; after mixing and stirring the raw materials, putting the raw materials in a culture barrel and placing the barrel in a darkroom in a semi-hermetical manner, wherein the culture temperature is 20-30 DEG C, and after 15 days when suspended solids immerse to water, the liquid is brown and the pH value is bellow 3.8; adding pig manure, pig urine, pig bone, pig hair, pig blood, horseshit, straws, wheat straws, beanstalks, peanut stalks, copperas and magnesium sulfate into the liquid; after uniformly smashing and stirring, carrying out anaerobic fermentation at an environmental temperature of 20-30 DEG C for 10-20 days in summer and 15-30 days in winter; and smashing, prilling and drying. The organic fertilizer prepared from recovered wastes of the pig farm disclosed by the invention solves the problem of environmental pollution caused by the wastes, soil hardening caused by chemical fertilizers used on soil and unabiding fertilizer efficiency.
Owner:ZHEJIANG MAOYANGGANG AGRI DEV CO LTD

Urea sulfate coated urea slow-release granular fertilizer and preparation method therefor

ActiveCN105001023ARealize double-membrane double-controlling effectLow costUrea compound fertilisersFertilizer mixturesCoated ureaMetasilicate
The invention discloses a urea sulfate coated urea slow-release granular fertilizer. The urea sulfate coated urea slow-release granular fertilizer is prepared through the following steps of: adding 100kg of urea granules of which the diameters are 2-4.5mm to a rotary drum type coating machine, preheating the urea granules to 40-45 DEG C, spraying 1-10kg of a binder namely urea sulfate, uniformly mixing the preheated urea granules and the urea sulfate so as to obtain a mixture, spraying 1-20kg of metasilicate powder, cooling the mixture and the metasilicate powder, spraying 1-10kg of mounting addition agents (a mixture of solid paraffin and liquid paraffin) of which the temperature is 50-60 DEG C, cooling the mixture, the metasilicate powder and the mounting addition agents to a room temperature, and repeating the coating operation 2-3 times. The binder namely the urea sulfate is prepared through the steps of slowly adding1-2kg of concentrated sulfuric acid of 90-98wt% to every 1-10kg of urea and performing a reaction in a reaction tank. The urea sulfate coated urea slow-release granular fertilizer disclosed by the invention adopts a urea sulfate metasilicate slow-release film, tests prove that the urea sulfate metasilicate slow release film has a favorable slow-release effect, and in the slow-release process, the slow-release film is not liable to collapse and is easy to degrade. The urea sulfate has subacidity, so that the application range of the urea sulfate is wider than that of sulfur coating urea. The urea sulfate coating film realizes double-film double-control effects, and has the advantages of high efficiency, environmental protection, low cost and the like.
Owner:JILIN YUNTIANHUA AGRI DEV CO LTD

Rural domestic wastewater treatment device and method based on MBBR coupling anaerobic-aerobic process integration

The invention discloses a rural domestic wastewater treatment device based on MBBR coupling anaerobic-aerobic process integration. The device comprises an MBBR anaerobic chamber, an MBBR anoxic chamber and an MBBR aerobic chamber, a large amount of anaerobic bacteria are enriched in the MBBR anaerobic chamber for anaerobic hydrolysis, wastewater enters the device, a large amount of sulfur autotrophic denitrifying bacteria are enriched in the MBBR anoxic chamber for denitrification, and a large amount of nitrifying bacteria and phosphorus phagocytosis bacteria are enriched in the MBBR aerobic chamber. Gravity curved screens and sedimentation tanks are additionally arranged at the water outlet tail ends of the anaerobic tank and the aerobic tank, so that the flow of MBBR filler and activated sludge is ensured, the defect that the biological population ecology is influenced by drifting of suspended filler in different stages in the MBBR is overcome, and the nitrogen and phosphorus removal efficiency is improved. The system not only retains the advantages of large specific surface area and high efficiency of the MBBR, but also can greatly reduce the generation of excess sludge, and can realize regulation and control of nitrogen and phosphorus indexes of rural domestic wastewater.
Owner:ZHEJIANG UNIV

ArHeN2CO2 protective gas for consumable electrode gas shielded nickel-based welding wire

The invention provides an ArHeN2CO2 protective gas for a consumable electrode gas shielded nickel-based welding wire. The consumable electrode gas shielded welding adopts the nickel-based welding wireand an ArHeN2CO2 quaternary protective gas, the mixing using amount of the nickel-based welding wire and the ArHeN2CO2 quaternary protective gas comprises the following components of, by mass, 45-50%of Ar, 45-50% of He, 2.5-3.5% of N2, and 2.5-3.5% of CO2; the use amount of the ArHeN2CO2 quaternary protective gas is mixed through different proportions, so that the content of nitrogen elements ina weld joint of a large-thickness plate is ensured, and excellent arc stiffness and strong directivity are achieved; and excellent welding of the nitrogen element without burning loss improves the compactness degree of the weld joint, and the technical problems that the nitrogen element losses and the mechanical property of weld joint is not stable in the welding process are solved. Due to the fact that the method adopting the ArHeN2CO2 quaternary gas to be mixed according to the proportions to serve as the protective gas in NiCrMo-3 nickel-based melting electrode gas shielded welding, the excellent arc stiffness is achieved, the welding efficiency is improved, the construction period is shortened, and the production cost is reduced; and the compactness degree of the weld joint is improved, and the welding difficulty is reduced, and the gas is suitable for being used as the protective gas in application for a consumable electrode gas shielded nickel-based welding wire.
Owner:中国船舶集团渤海造船有限公司

ArHeN2H2 protective gas for consumable electrode gas shielded nickel-based welding wire

The invention provides an ArHeN2H2 protective gas for a consumable electrode gas shielded nickel-based welding wire. The melting electrode gas shielded welding adopts a nickel-based welding wire and an ArHeN2H2 protective gas, and the mass ratio of the mixed use amount of the nickel-based welding wire and the ARHN2h2 protective gas is as follows, 45-50% of Ar, 45-50% of He, 2.5-3.5% of N2, and 1.0-1.5% of H2. The use amount of the ArHeN2H2 quaternary protection gas is mixed through different proportions, the content of nitrogen elements in the weld joint of the large-thickness plate is guaranteed, excellent arc stiffness is achieved, the directivity is high, free of burning loss of nitrogen elements is achieved, the compactness degree of the welding seam is improved, and the technical problem that the mechanical property of a nitrogen element lost weld joint is not stable in the welding process is solved. In the NiCrMo-3 nickel-based melting electrode gas shielded welding, ArHeN2H2 quaternary gases are mixed according to a ratio to serve as protective gas, excellent arc stiffness is achieved, the welding efficiency is improved, the construction period is shortened, and the production cost is reduced; the compactness degree of the welding seam is improved, and the welding difficulty is reduced; and the ArHeN2H2 protective gas is suitable for being used as a protective gas for aconsumable electrode gas shielded nickel-based welding wire.
Owner:渤海造船厂集团有限公司

Repeated filling type packaging bag nitrogen filling device

The invention discloses a repeated filling type packaging bag nitrogen filling device. The nitrogen filling device comprises a machine frame and an air inflation sub-clamp mechanism, wherein an air inflation pipe (13) is arranged at the position, between a left sub-clamp and a right sub-clamp of the air inflation sub-clamp mechanism, on the machine frame; rollers (12) are arranged at the upper endpart of the air inflation pipe; a rolling plate (4) is arranged at the position, above the air inflation pipe, of the machine frame, the rollers can roll on the rolling plate, and air inflation pipelifting mechanisms (5) and bag opening packaging mechanisms (15) are arranged on the side edges of the end parts of the rolling plates; and a feeding rotating disc (1) is arranged on the side edge ofthe machine frame, and a packaging bag conveying mechanism (3) is arranged at the position between the machine frame and the feeding rotating disc. According to the nitrogen filling device, the packaging bag conveying mechanism is used for conveying loaded packaging bags to a nitrogen filling station, and the air inflation pipe is used for carrying out continuous and repeated nitrogen filling andpumping on the packaging bags so as to guarantee the nitrogen content and concentration in the bags, so that the shelf life of the materials is properly prolonged, waste caused by the expiration of the materials is effectively avoided, and the material packaging quality is obviously improved.
Owner:浙江简正机械有限公司

ArHeN2 protective gas for consumable electrode gas shielded nickel-based welding wire

The invention provides an ArHeN2 protective gas for a consumable electrode gas shielded nickel-based welding wire. The consumable electrode gas shielded welding adopts the nickel-based welding wire and an ArHeN2 protective gas, the mixing using amount of the mass ratio of the nickel-based welding wire and the ArHeN2 protective gas comprises the following components of, 45-50% of Ar, 45-50% of He,and 2.5-3.5% of N2; the use amount of the ArHeN2 protective gas is mixed through different proportions, so that the content of nitrogen elements in a weld joint of a thin plate is ensured, and excellent arc stiffness and strong directivity are achieved; and excellent welding of the nitrogen element without burning loss improves the compactness degree of the weld joint, and the technical problems that the nitrogen element losses and the mechanical property of weld joint is not stable in the welding process are solved. Due to the fact that the method adopting the ArHeN2 ternary gas to be mixed according to the proportions to serve as the protective gas in NiCrMo-3 nickel-based melting electrode gas shielded welding, the excellent arc stiffness is achieved, the welding efficiency is improved,the construction period is shortened, and the production cost is reduced; and the compactness degree of the weld joint is improved, and the welding difficulty is reduced, and the gas is suitable forbeing used as the protective gas in application for a consumable electrode gas shielded nickel-based welding wire.
Owner:中国船舶集团渤海造船有限公司

Urea sulfate-coated urea slow-release granular fertilizer and preparation method thereof

ActiveCN105001023BRealize double-membrane double-controlling effectLow costUrea compound fertilisersFertilizer mixturesWaxMetasilicate
The invention discloses a urea sulfate coated urea slow-release granular fertilizer. The urea sulfate coated urea slow-release granular fertilizer is prepared through the following steps of: adding 100kg of urea granules of which the diameters are 2-4.5mm to a rotary drum type coating machine, preheating the urea granules to 40-45 DEG C, spraying 1-10kg of a binder namely urea sulfate, uniformly mixing the preheated urea granules and the urea sulfate so as to obtain a mixture, spraying 1-20kg of metasilicate powder, cooling the mixture and the metasilicate powder, spraying 1-10kg of mounting addition agents (a mixture of solid paraffin and liquid paraffin) of which the temperature is 50-60 DEG C, cooling the mixture, the metasilicate powder and the mounting addition agents to a room temperature, and repeating the coating operation 2-3 times. The binder namely the urea sulfate is prepared through the steps of slowly adding1-2kg of concentrated sulfuric acid of 90-98wt% to every 1-10kg of urea and performing a reaction in a reaction tank. The urea sulfate coated urea slow-release granular fertilizer disclosed by the invention adopts a urea sulfate metasilicate slow-release film, tests prove that the urea sulfate metasilicate slow release film has a favorable slow-release effect, and in the slow-release process, the slow-release film is not liable to collapse and is easy to degrade. The urea sulfate has subacidity, so that the application range of the urea sulfate is wider than that of sulfur coating urea. The urea sulfate coating film realizes double-film double-control effects, and has the advantages of high efficiency, environmental protection, low cost and the like.
Owner:JILIN YUNTIANHUA AGRI DEV CO LTD

Nitrogen system and glass hot bending machine

The invention discloses a nitrogen system and a glass hot bending machine. The nitrogen system comprises a gas storage tank, a main pipeline, a first separate pipeline, a second separate pipeline, a first branch pipeline, a second branch pipeline, a third branch pipeline, a fourth branch pipeline, a fifth branch pipeline, a sixth branch pipeline and a seventh branch pipeline, wherein the main pipeline is connected with the gas storage tank; the first separate pipeline and the second separate pipeline are connected with the main pipeline; the first branch pipeline and the second branch pipelineare connected with the first separate pipeline; the third branch pipeline, the fourth branch pipeline, the fifth branch pipeline, the sixth branch pipeline and the seventh branch pipeline are connected with the second separate pipeline; the first branch pipeline is communicated with a material charging box; the second branch pipeline is communicated with a material fetching box; the third branchpipeline is communicated with the material charging box; the fourth branch pipeline is communicated with the material fetching box; the fifth branch pipeline, the sixth branch pipeline and the seventhbranch pipeline are communicated with a forming box; a straight-through ball valve and a filtering pressure-relief valve are arranged on the main pipeline; a pressure gauge is arranged on the filtering pressure-relief valve and is used for displaying air pressure.
Owner:SHENZHEN CREATE CENTURY MACHINERY

Flux-cored wire for gas shielded welding of super duplex stainless steel and preparation method thereof

The invention discloses a flux-cored wire used for super duplex stainless steel gas shielded welding and a preparation method thereof. The flux-cored wire is composed of an external use steel belt andflux powder, wherein the external use steel belt is made of an austenitic stainless steel belt with 17.0%-18.0% of chromium and 11.0%-12.5% of nickel; and the flux powder comprises the following components of, in percentage by weight, 36.0%-38.0% of chromium powder, 9.0%-13.0% of high-nitrogen chromium iron, 2.5%-3.0% of electrolytic manganese metal, 4.0%-5.0% of molybdenum powder, 0.5%-1.0% of ferrosilicon, 1.0%-1.5% of ferrotitanium, 0.5%-1.0% of aluminum-magnesium alloy, 18.0%-20.0% of rutile, 1.0%-2.0% of quartz, 5.0%-6.0% of zircon sand, 1.0%-1.5% of potassium feldspar, 3.0%-3.5% of albite, 1.0%-1.5% of fluorite, 0.5%-1.0% of sodium cryolite, 1.0%-1.5% of potassium titanate, 0.1%-0.3% of bismuth oxide and the balance iron powder. According to the flux-cored wire used for super duplexstainless steel gas shielded welding and the preparation method thereof, the components and the two-phase proportion of deposited metal can be balanced, thus obtaining a duplex stainless steel welding joint which is good in forming quality and excellent in corrosion resistance.
Owner:CENT RES INST OF BUILDING & CONSTR CO LTD MCC GRP

A nitrogen-containing high-entropy alloy composite material and its preparation method

The invention belongs to the field of alloys, in particular to a nitrogen-containing high-entropy alloy composite material and a preparation method thereof. The nitrogen-containing high-entropy alloy composite material has a mixed crystal structure in which one layer of coarse grains and one layer of fine grains are alternately distributed. The preparation method includes: step 1, preparing nitrogen-containing high-entropy pre-alloyed powder; in the nitrogen-containing high-entropy pre-alloyed powder, metal elements are selected from at least three of Fe, Co, Cr, Ni, and Mn; In step 2, the nitrogen-containing high-entropy pre-alloyed powder obtained in step 1 is formed by using a selective laser melting technology; and a nitrogen-containing high-entropy alloy is obtained. The preparation process of the present invention is simple and controllable; the structure of the product is fine and uniform, the nitrogen element distribution inside the blank is uniform, the overall nitrogen element distribution is also relatively uniform, the mechanical properties are good, and the corrosion resistance is good; this is to realize the nitrogen-containing high-entropy alloy. Engineering applications provide the necessary conditions.
Owner:CENT SOUTH UNIV

Method for eliminating warped skin on surface of hot alloy steel

The invention relates to the technical field of steelmaking processes, in particular to a method for eliminating surface warping of hot alloy steel. The method comprises the following steps: smelting molten iron in a converter to obtain molten steel after the converter; refining and smelting the molten steel after the furnace to obtain refined molten steel; the refined molten steel is sequentially subjected to continuous casting and stack cooling, and a plate blank is obtained; the nitrogen content of the molten steel after the furnace is less than or equal to 28ppm by mass concentration; the nitrogen increasing amount of the refined molten steel is smaller than or equal to 6 ppm by mass concentration; in the continuous casting process, the nitrogen increasing amount is smaller than or equal to 3 ppm by mass concentration, and the nitrogen content of the plate blank is smaller than or equal to 40 ppm by mass concentration; in the plate blank, a metallographic structure comprises, by volume fraction, 100% of ferrite; and through a low-temperature hot delivery process of nitrogen production content and stack cooling, precipitation of second-phase particles is reduced, austenite is ensured to be completely converted into ferrite, and the defect of warping of a hot-rolled coil is eliminated.
Owner:SHOUGANG JINGTANG IRON & STEEL CO LTD

A kind of method for preparing vanadium nitride

The invention discloses a method for preparing vanadium nitride, which comprises the following steps: step 1, carrying out pre-reduction on a test specimen prepared from ammonium metavanadate powder and carbon powder in a heating furnace by nitrogen, wherein in the pre-reduction process, a temperature in the heating furnace is 650 to 670 DEG C, nitrogen flow is 210 to 270mL / min, and heat preservation time of the heating furnace is 2 to 4 hours; step 2, after ending heat preservation in the step S1, warming the heating furnace to a temperature of 1,300 to 1,500 DEG C and carrying out final reduction on the test specimen, wherein the final reduction process, nitrogen flow in the heating furnace is 210 to 270mL / min, and heat preservation time of the heating furnace is 4 to 5 hours; step 3, after ending heat preservation in the step S2, carrying out furnace cooling on the test specimen in nitrogen atmosphere, so that the obtained test specimen is the vanadium nitride. According to the method disclosed by the invention, the vanadium nitride is prepared by the ammonium metavanadate, so that a calcination section can be omitted, and the aims of simplifying a production process, reducing production cost of an enterprise and reducing pollution are fulfilled.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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