9results about How to "Promotes sintering densification" patented technology

The invention belongs to the technical field of ceramic materials, and particularly discloses whisker toughened zirconium oxide-aluminum oxide composite ceramic and an additive manufacturing method thereof, the composite ceramic comprises the following components by mass: 94 parts of zirconium oxide toughened aluminum oxide ceramic and 5 parts of silicon carbide whisker; the zirconium oxide toughened aluminum oxide ceramic is prepared from the following components in parts by mass: 76 parts of aluminum oxide and 24 parts of zirconium oxide, and 3mol% of yttrium oxide is added into the zirconium oxide. According to the whisker toughened zirconium oxide-aluminum oxide composite ceramic and the additive manufacturing method thereof, the preparation method has unique design of components and process, and the preparation of a high-density and high-performance ceramic-based composite material part based on a fused deposition modeling technology is successfully realized. Further, the prepared silicon carbide whisker toughened zirconium oxide-aluminum oxide-based composite ceramic has relatively high density and excellent obdurability.

The application discloses a kind of core-shell structure nanometer powder toughened zirconia ceramics and preparation method thereof, belong to ceramic material technical field, the method includes using three-dimensional network gel to realize washing-free co-precipitation method to prepare high-activity, ZrO2@SiO2Core-shell structure nanometer zirconia raw material powder, and stable agent is mixed ball milling, drying, sieving, shaping, cold isostatic pressing and gets green body, green body is placed in vacuum furnace and sintering, annealing and obtains toughened zirconia ceramic target product, realizes the efficient preparation of jade quality feeling simulation ceramic tooth of integral penetration.The application avoids the repeated washing steps of precursor in the traditional co-precipitation preparation process, reduces the introduction of impurities, the sintering temperature is lower, the powder yield is high, the process is simple, the cost is low, and is suitable for the industrial production of toughened zirconia ceramics.

This invention discloses a high thermal conductivity semiconductor packaging substrate and its preparation method, relating to the field of electronic materials technology. The method includes the following steps: mixing composite aluminum nitride powder with a sintering aid, ball milling, drying, and pressing into shape; sintering under high temperature and high pressure in a nitrogen atmosphere to obtain an aluminum nitride ceramic substrate; washing and drying the aluminum nitride ceramic substrate; covering both sides of the aluminum nitride ceramic substrate with copper foil, laying active solder between the aluminum nitride ceramic substrate and the copper foil, and then connecting them by vacuum brazing to obtain the semiconductor packaging substrate; the composite aluminum nitride powder is composed of aluminum nitride powder and modified aluminum nitride powder in a mass ratio of (6~8):(2~4). The semiconductor packaging substrate prepared by this method has excellent interfacial compatibility, effectively reduces interfacial thermal stress, and has good thermal conductivity.

The application belongs to the field of ceramic powder preparation, and discloses a method for in-situ preparation of high-performance TiB2-B4C composite ceramic from sapphire fine grinding waste. The method uses the waste produced in the sapphire grinding process as raw material (B4C, Al2O3 and Fe), adds TiO2 and C after alkali washing and purification, and combines with the discharge plasma sintering to in-situ prepare TiB2-B4C composite ceramic. The method not only realizes the comprehensive recovery of B4C in the sapphire fine grinding waste slurry, reduces environmental pollution, but also provides a method for in-situ preparation of TiB2-B4C composite ceramic from waste, changes waste into treasure, and realizes the secondary use of resources. In addition, the raw material cost is low, and the method has obvious economic value and environmental protection significance. The method has the advantages of short process, small pollution, simplicity and the like, and can be used for industrial production.

The invention relates to the field of refractory materials, and discloses a high-purity alumina lightweight aggregate and a preparation method thereof. The aggregate is prepared from alumina micro powder with a specific particle size ratio: 50-60 wt% of micro powder with the particle size of 70-115 [mu] m, 20-30 wt% of micro powder with the particle size of 20-36 [mu] m and 10-20 wt% of micro powder with the particle size of 2.5-5 [mu] m, and each micro powder needs to meet the conditions that the content of alpha-Al2O3 is greater than or equal to 99.6% and the content of Na2O is less than or During preparation, water, the foaming agent, the foam stabilizer, the binding agent, the dispersing agent and the sintering aid are added in an external addition form, and the preparation method comprises the steps of mixing, pulping, foaming, foam stabilizing, pouring, drying, high-temperature sintering and the like. A foaming method is adopted to replace a traditional high-energy-consumption electric melting process, the sintering temperature is reduced to 1600-1700 DEG C, and the energy consumption is reduced by 30% or above. The obtained aggregate has high purity (Al2O3 is greater than 99.4 wt%), low volume density (1.5-2.0 g / cm < 3 >), high apparent porosity (50-70%), excellent normal-temperature compressive strength (20-30 MPa) and low thermal conductivity (0.3-0.7 W / (m.K) at 1000 DEG C), perfectly solves the problem that light weight, high strength and efficient thermal insulation performance are difficult to consider at the same time, and is suitable for producing working lining and thermal insulation layer products of high-temperature industrial kilns.

The invention discloses a carbon ceramic closing resistor for a high-voltage circuit breaker and a preparation method of the carbon ceramic closing resistor, and belongs to the technical field of power elements. The problems of poor resistor compactness, non-uniform performance, insufficient mechanical property and the like caused by high pressing and sintering difficulty, process instability and high and non-uniform resistor porosity of the carbon ceramic resistor are solved. The preparation process of the resistor comprises the following steps: by taking aluminum oxide and quartz as ceramic phases, presintered kaolin, mullite and potassium feldspar as clay phases and carbon black or graphite as conductive phases, pre-coating the ceramic phases with the clay phases, carrying out vacuum calcination on pre-coated powder, mixing the pre-coated powder with the secondarily added clay phases and the conductive phases, carrying out spray granulation, pressing a green body, sintering and spraying. And obtaining the carbon ceramic closing resistor. According to the invention, the kaolin is pre-sintered, and the clay phase is pre-coated with the ceramic phase, so that the subsequent blank pressing uniformity and density are increased, the structural defects of the carbon ceramic resistor are reduced, and in combination with the spark plasma sintering technology, the batch rapid production of the resistor can be realized.

The application belongs to the technical field of silicon carbide ceramic preparation, and particularly relates to a silicon carbide ceramic slurry based on DIW-3D printing, a silicon carbide ceramic product and a preparation method. The silicon carbide ceramic slurry is prepared from raw materials including the following components and weight contents: silicon carbide mixed powder 60-100 parts, thermosetting resin 10-40 parts, dispersing agent 5-15 parts and thermal initiator 0.01-1 part. The application realizes the application of DIW-3D printing in the preparation of silicon carbide ceramic through the synergistic effect of double-particle-size SiC grading, introduction of B4C sintering aid, special resin and dispersant system, thermal initiation and solidification, DIW rheological design and gas pressure sintering, saves the material cost in the manufacturing process, prepares a silicon carbide sample with excellent mechanical properties, and further widens the development of silicon carbide ceramic.

The application discloses a preparation method of a high-temperature alloy, which comprises the following steps: (1) mixing high-temperature alloy raw material powder with a granulating agent to perform granulation to obtain granulated raw material; and (2) under vacuum conditions, the granulated raw material is sintered by using oscillation hot pressing, and during sintering, an alternating load is adopted to control the grain growth process, so that the high-temperature alloy is obtained. The preparation method of the high-temperature alloy first performs granulation on alloy powder, and then controls the grain growth process of the product by controlling the alternating load of the oscillation hot sintering process, so that the grain refinement is facilitated, the fine-grain strengthening effect is generated, and the mechanical properties of the high-temperature alloy product are greatly improved. In addition, through the mutual synergistic effect of the granulation and the alternating load, the compactness of the product can be improved.

This invention discloses a method for preparing yttrium-magnesium oxide (YMO) multiphase transparent ceramics using non-aqueous gel casting, belonging to the field of ceramic preparation technology. To overcome the problems associated with water-based gel casting, this invention provides a method for preparing YMO multiphase transparent ceramics using non-aqueous gel casting, comprising: ball milling Y2O3, MgO, a dispersant, and a non-aqueous solvent; then adding epoxy resin and a curing agent and ball milling again; the resulting ceramic slurry is defoamed, cured, and dried; then subjected to debinding, sintering densification, cooling, hot isostatic pressing, annealing, and polishing to obtain the YMO multiphase transparent ceramic. This invention overcomes the difficulties in preparing large-size Y2O3-MgO nano-multiphase infrared transparent ceramics and the problem of component inhomogeneity by designing a non-aqueous solvent system and selecting a suitable gel system, and can produce complex-shaped / large-size, uniformly composed YMO nano-multiphase ceramics.