The invention relates to a preparation method for a 
zirconium-contained rare-earth 
composite oxide. At a certain ratio, 
rare earth (
cerium, 
yttrium, 
praseodymium or 
terbium) is mixed with 
zirconium to burden, or 
rare earth (
cerium, 
yttrium, 
praseodymium or 
terbium) and 
zirconium are mixed with at least one of other 
metal ions (aluminum, 
barium, 
magnesium, 
strontium, 
titanium, 
manganese, ferrum, 
copper and 
hafnium) to burden. A 
magnesium bicarbonate or /  and 
calcium bicarbonate aqueous solution prepared from raw materials of 
magnesium or /  and 
calcium minerals or oxides and hydroxides by at least one working procedure of 
roasting, digesting, mixing size, carbonizing and the like can serve as a precipitator to carry out 
precipitation so as to obtain at least one of 
rare earth and zirconium composite 
carbonate and subcarbonate, and the at least one of rare earth and zirconium composite 
carbonate and subcarbonate is further roasted to obtain a zirconium-contained rare-earth 
composite oxide product. In the preparation method, cheap 
calcium or /  and magnesium minerals or low-purity oxides and hydroxides can serve as initial raw materials to replace common 
chemical industry precipitators, such as 
ammonia water, 
ammonium bicarbonate, 
sodium carbonate, 
sodium hydroxide and the like, substances, such as magnesium, calcium, 
carbon dioxide and the like can be effectively circulated and utilized so as to greatly lower the production cost of the zirconium-contained rare-earth 
composite oxide, such as ceria-zirconia, 
yttrium zirconium, 
praseodymium zirconium, 
terbium zirconium and the like. In addition, in the production technology disclosed by the invention, no 
ammonia nitrogen wastewater, high-
salinity wastewater and the like are generated, 
carbon dioxide greenhouse gas emission amount is reduced, the preparation technology is environmentally-friendly, and environment 
pollution is avoided.