The invention discloses a method for preparing a 3
omega electrode of a surface conductive or rough sample, which comprises the following steps of: cleaning a sample to be detected, spin-
coating liquid BCB resin and curing, tightly attaching a hollow
mask plate to the sample to be detected so as to transfer a pattern on the
mask plate to the sample to be detected, fixing the attached hollow
mask plate to the sample to be detected, and carrying out surface conductive treatment on the sample to be detected, so as to obtain the 3
omega electrode of the surface conductive or rough sample. And putting the sample into a
metal evaporation furnace to evaporate
metal, and finally separating the sample to be detected from the hollow mask plate to complete the preparation of the 3
omega electrode. According to the scheme, the characteristic that the liquid BCB resin can be cured after
spin coating is utilized, a flat insulating layer can be formed on the surface of a conductive or rough sample, the subsequently prepared 3 omega electrode can be used for testing, meanwhile, the hollow mask and the
evaporation clamp
system designed in the scheme can avoid using
photoresist to photoetch the
evaporation electrode, and the
test efficiency is improved. The possible electrode falling condition is avoided, and the evaporated
metal electrode and the sample can be connected more firmly in the mode that the metal is directly evaporated through the hollowed-out mask.