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44results about How to "Moderate volatilization speed" patented technology

Preparation method of polystyrene sulfonic acid type ion exchange resin

The invention discloses a preparation method of polystyrene sulfonic acid type ion exchange resin. The preparation method comprises steps as follows: deionized water, polyvinyl alcohol, ethanol, sodium chloride and sodium persulfate are mixed uniformly, and an aqueous phase is obtained; styrene, divinylbenzene, n-heptane, cyclohexanone, methylbenzene and benzoyl peroxide are added to the aqueous phase to be uniformly mixed, react for 2.5-4 h at the temperature ranging from 70 DEG C to 80 DEG C, react for 5-8 h at the temperature ranging from 85 DEG C to 90 DEG C, react for 0.5-1 h at the temperature ranging from 91 DEG C to 95 DEG C and is washed, filtered, dried and screened, and then polystyrene microspheres are obtained; the polystyrene microspheres are added to dichloroethane to be swollen, a sulfonating agent is added, the mixture reacts for 4-5 h at the temperature ranging from 50 DEG C to 60 DEG C, and the polystyrene sulfonic acid type ion exchange resin is obtained. According to the preparation method of the polystyrene sulfonic acid type ion exchange resin, the operation is simple, conditions are mild, and the obtained polystyrene sulfonic acid type ion exchange resin has high mechanical strength, good heat resistance, a high ion exchange rate and a large specific surface area.
Owner:ANHUI WANDONG CHEM

Aerosol type precise instrument cleaning agent and preparation method thereof

The invention provides an aerosol type precise instrument cleaning agent and a preparation method. The formula of the aerosol type precise instrument cleaning agent comprises the following componentsin parts by weight: 75.0-90.0 parts of an environment-friendly solvent, 0.01-1.0 part of a surfactant, 1.0-10.0 parts of a cosolvent and 5.0-10.0 parts of a propellant. According to the invention, thecleaning agent for the precise instrument has the following beneficial effects that 1, the cleaning agent is excellent in performance, safe and reliable, and can quickly remove dust, oil stains, moisture and the like of the precise instrument under the condition of no power failure; 2, the construction operation is flexible, simple and convenient, and the product safety is high; 3, the cleaning agent product is safe to use, free of flash point, non-combustible, zero in ODP and low in GWP value, and meets the environmental protection requirement; and 4, the volatilization speed is moderate, the ice crystal effect and the condensation phenomenon are avoided in the cleaning process, the surface insulation value of the equipment is not obviously reduced, and the equipment is not corroded anddamaged. The invention further discloses a preparation method of the precise instrument cleaning agent.
Owner:GUANGDONG SANVO CHEM IND TECH

Method for rapidly preparing high-purity sodium thiosulfate crystals

The invention discloses a method for rapidly preparing high-purity sodium thiosulfate crystals. The method comprises the following steps: adding 6.3 g of sodium sulfite, 3.2 g of sulfur powder and 30mL of distilled water into a small beaker, covering the small beaker with a large beaker, carrying out a microwave heating reaction for 1 min, cooling the obtained reaction product to normal temperature, and carrying out suction filtration to recover the sulfur powder; adding 150 mL of acetone to the obtained filtrate, stirring the filtrate and the acetone for 5-6 min to make crystals appear, carrying out suction filtration, washing the obtained crystals with 10 mL of acetone to obtain sodium thiosulfate crystals, carrying out vacuum drying for 2 h, and weighing the dried sodium thiosulfate crystals; distilling the obtained filtrate to recover the acetone for reuse; and recovering the obtained remaining solution for next preparation. The method has the advantages of high substance utilization rate, less experiment devices, simplicity and convenience in operation, safety and simplicity in the experiment devices, short experiment time, high yield, high purity, good crystal precipitationspeed, omission of the evaporative concentration link in traditional experiments, reduction of requirements of the experiments for the devices, low experiment cost, less raw material waste, energy saving, environmental protection and no pollution.
Owner:王亚玲
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