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31results about How to "Reduce solid waste generation" patented technology

Coproduction method of methylbenzoic acid, methyl benzoate and benzenedicarboxylic acid diester

The invention discloses a coproduction method of methylbenzoic acid, methyl benzoate and benzenedicarboxylic acid diester. The method comprises the following steps: (1) continuously introducing xylene, a catalyst and oxygen-containing gas into an oxidation reactor for a reaction, and controlling oxygenic concentration in the tail gas to not exceed 5% by controlling introduction amount of the oxygen-containing gas to obtain an oxidation reaction liquid; (2) feeding the obtained oxidation reaction liquid into a predistillation tower for distillation separation to obtain a low-boiling-point component and a predistillation tower bottom liquid; (3) feeding the predistillation tower bottom liquid into a distillation tower for distillation to obtain a methylbenzoic acid product and a distillationtower bottom liquid; (4) mixing the distillation tower bottom liquid and alcohol for an esterification reaction, and controlling the reaction endpoint to be lower than 0.5wt% of the content of methylbenzoic acid to obtain an esterification reaction liquid; (5) performing distillation separation on the obtained esterification reaction liquid to obtain methyl benzoate and benzenedicarboxylic acid diester products. The method has the advantages that the process is simple, equipment investment is low, and the method is environmentally friendly and has good comprehensive economic benefits.
Owner:JIANGXI KEYUAN BIOPHARM

Waste emulsion demulsification processing method

The invention belongs to the field of industrial waste water treatment, and relates to a waste emulsion demulsification processing method. The method employs at least one of bentonite, diatomite and activated clay as an adsorbent, employs at least one of polymeric aluminium, polymerization ferric chloride, polyferric sulfate and polyacrylamide as a flocculating agent, and performs demulsification processing on waste emulsion, wherein grease adsorption is carried out by an adsorbent, flocculation settlement is carried out by a flocculating agent, and solid-liquid separation is carried out. The method has the advantages of simple process, low operation cost, low energy consumption and high processing efficiency. the used agent has the advantages of nontoxicity and innocuousness, low cost and easy acquisition, has obvious maneuverability, and can be widely used for processing the waste emulsion, waste cutting fluid and waste saponification liquor for metal product, machining and other industries. According to the invention, more than 90% of chemical oxygen demand (COD) in the waste emulsion can be removed by a one step, and favorable condition can be provided for subsequent deep treatment such as chemical oxidation and biodegradation.
Owner:ZHANGJIAGANG GREEN TECH ENVIRONMENTAL PROTECTION EQUIP

Sodium chloride-containing pesticide production wastewater resource treatment system and method

The invention discloses a sodium chloride-containing pesticide production wastewater resource treatment system and method, and belongs to the field of a sewage treatment method. The system comprises asalt-tolerant bacterium biochemical system, a nanofiltration membrane device, an electrodialysis device and an electrocatalytic oxidation device, wherein the salt-tolerant bacterium biochemical system comprises a first salt-tolerant bacterium aerobic device, a salt-tolerant bacterium anaerobic device and a second salt-tolerant bacterium aerobic device; the second salt-tolerant bacterium aerobic device comprises a salt-tolerant bacterium MBR device; the treatment system also comprises a reverse osmosis device. The invention also discloses a wastewater treatment method. The flow process of themethod of the salt-tolerant bacterium biochemical treatment, MBR treatment, nanofiltration membrane treatment, electrodialysis treatment and electrocatalytic treatment is used; after the pesticide production wastewater is subjected to treatment, the water quality of produced water is high; when the system and the method are applied to enterprise production, water resources in the waste water are recovered; the general organic carbon content in the obtained sodium chloride salt wastewater is low; the system and the method can be used for chlor-alkali production; sodium chloride salt in the wastewater is recovered.
Owner:JIANGSU LASON CHEM ENVIRONMENTAL PROTECTION

A method for co-producing methylbenzoic acid, methylbenzoic acid ester and phthalic acid diester

The invention discloses a method for co-producing methyl benzoic acid, methyl benzoate and phthalic acid diester, comprising: (1) continuously feeding xylene, a catalyst and an oxygen-containing gas into an oxidation reactor to carry out reaction, by controlling the amount of oxygen-containing gas to control the tail oxygen concentration to be no more than 5%, to obtain an oxidation reaction liquid; (2) enter the obtained oxidation reaction liquid into an initial distillation tower for rectification separation, to obtain low boiling point components and initial (3) enter the rectifying tower still liquid into the rectifying tower for rectification to obtain toluic acid product and rectifying tower still liquid; (4) mix the rectifying tower tower liquid with alcohol , carry out the esterification reaction, control the reaction end point to be that the content of toluic acid<0.5wt%, obtain the esterification reaction solution; (5) carry out rectification separation with the esterification reaction solution obtained, obtain methyl benzoic acid ester respectively and diester phthalate products. The invention has the advantages of simple process, less equipment investment, environmental protection and good comprehensive economic benefits.
Owner:JIANGXI KEYUAN BIOPHARM

Filtering device and filtering method for reducing nuclear power filtering solid waste quantity

The invention discloses a filtering device and a filtering method for reducing nuclear power filtering solid waste quantity. The filtering device comprises a filter shell, a filter element assembly, a water inlet pipe, a water outlet pipe, a water inlet valve, a water outlet valve and a filter element cleaning structure, wherein the filter element assembly is arranged inside the filter shell, a water inlet and a water outlet are formed in the filter shell, a water inlet pipe is arranged at the water inlet, and a water inlet valve is arranged on the water inlet pipe; the water outlet pipe is arranged at the water outlet and is provided with a water outlet valve; and the water inlet is positioned below the water outlet. According to the filtering device, the filter element cleaning structure is arranged, the filter element assembly can be cleaned and regenerated, the problem that an original filter element cannot be recycled is solved, the filtering device is adopted for filtering, long-term operation can be achieved, the filter element does not need to be frequently replaced, and the filtering device has the advantages of reducing the maintenance frequency, reducing the solid waste output of the filter element and reducing filter element solid waste quantity. And the device is suitable for radioactive water filtration of the nuclear power station.
Owner:AT&M ENVIRONMENTAL ENG TECH CO LTD

Method for reducing residue output in sodium hydrosulfite production process

The invention discloses a method for reducing residue output in a sodium hydrosulfite production process, the method comprises the following steps: S1, pumping sodium hydrosulfite rectification residual liquid into a first-effect evaporator, heating with steam, evaporating, and concentrating in a second-effect evaporator to obtain concentrated liquid and condensate; s2, feeding the concentrated solution into a curing kettle B, heating and concentrating with steam, discharging to a centrifugal head tank, feeding into a centrifugal machine, and centrifuging to obtain sodium formate and centrifugal mother liquor; s3, pumping the centrifugal mother liquor into a curing kettle A, continuously heating and concentrating with steam, adding methanol for extraction after concentration, removing supernatant liquid, connecting other materials with a metal hose, putting the other materials into a dryer, carrying out pressure filtration with nitrogen to obtain pressure filtration mother liquor, and treating the pressure filtration mother liquor to obtain sodium formate; s4, after the four-in-one mother liquor tank reaches a second preset liquid level, pumping liquid in the four-in-one mother liquor tank into an evaporation kettle, gasifying methanol, condensing and recycling so that a kettle bottom concentrated solution is sodium hydrosulfite residues. The method has the beneficial effect of reducing the generation amount of residues.
Owner:HUBEI YIHUA CHEMICAL INDUSTRY CO LTD

A trapping device and process for the production of 3,4-dichlorobenzonitrile

The invention discloses a trapping device and process for production of 3,4-dichlorobenzonitrile. The device is simple and reasonable in structural design; the implementation feasibility is high, thepracticability is high, more than 90% of ammonium chloride and more than 8% of 3,4-dichlorobenzonitrile are captured by a first-stage catcher through a dry capture method, more than 76% of 3,4-dichlorobenzonitrile is captured by a second-stage catcher through a dry capture method, latent heat of vaporization of water is fully utilized by the first-stage catcher, and the usage amount of spray liquid-water is small; besides, about 15% of the 3,4-dichlorobenzonitrile crude product collected by a third-stage catcher and a bath tower is dissolved by hot water, dehydrated, rectified and purified toobtain a liquid pure product of 3,4-dichlorobenzonitrile. The generation amount of coke oil and solid waste during the rectification process is low. Compared with a traditional multi-stage wet capturemethod, the consumption of 3,4-dichlorobenzonitrile is reduced, the investment cost of rectification equipment is reduced by more than half, the rectification energy consumption is equivalent to 15%of that of the traditional method, and the economic benefit is good.
Owner:常州新日催化剂股份有限公司

Device and method used for cobalt source storage source well water processing

The invention discloses a device and a method used for cobalt source storage source well water processing. The device comprises a pump, an active carbon filter, a membrane processing system, and a two-stage multi-medium mixed ion exchange column. Compared with the prior art, the advantages are that: the membrane processing system is adopted for condensation of extremely low concentration radionuclide or other ionic state impurities in well water, and an obtained concentrated solution is delivered through the two-stage multi-medium mixed ion exchange column, so that resin adsorption rate on radionuclide and impurities in unit time is accelerated, efficiency is increased, solid waste generation amount is reduced, and a problem in the prior art that only pure physical separation can be realized using the membrane processing system. Design of the distribution position of inlet water, reflux water, produced water, and concentrated water in well water is capable of realizing well water automatic circulation, and solving a problem that effective purifying of bottom precipitate is impossible to realize; and the device and the method can be both used for routine source well water purifyingand source well water pre-decommissioning fine processing, and the target of the invention is achieved.
Owner:SHANGHAI NUCLEAR ENG RES & DESIGN INST CO LTD

Method for directly smelting ferrovanadium nitride or ferrovanadium with high-temperature vanadium slag without chemical process

The invention provides a method for directly smelting ferrovanadium nitride or ferrovanadium with high-temperature vanadium slag without chemical process, which includes blowing vanadium-containing molten iron from the bottom or side of the furnace when it is close to the end point of vanadium extraction in the process of blowing vanadium in the converter Reductant, iron oxide in the reduction slag; after the semi-steel is produced, add the reducing agent from the top of the vanadium extraction furnace to continue reducing the iron oxide in the vanadium slag, and pour the high-temperature vanadium slag directly into the intermediate frequency induction furnace or electric arc furnace or through the heat preservation slag The tank is poured into the intermediate frequency induction furnace or electric arc furnace, and the vanadium and beneficial metal elements in the vanadium slag are deeply reduced by controlling the reduction temperature in the intermediate frequency induction furnace or electric arc furnace, and ferrovanadium nitride or ferrovanadium is obtained by controlling the amount of nitrogen blown at the bottom . The present invention uses high-temperature vanadium slag as raw material to directly produce ferrovanadium nitride, and can also produce ferrovanadium alloys of different grades, without the need for chemical land, and the production process is green and environmentally friendly, does not produce chemical waste water, and the energy consumption is significantly lower than that of traditional vanadium chemical processes. The process is short.
Owner:张计辉

A kind of catalytic hydrolysis pretreatment method for industrial park wastewater

A catalytic hydrolysis pretreatment method for industrial park wastewater relates to the technical field of industrial wastewater treatment. In order to solve the problems of traditional industrial park wastewater pretreatment, the invention has poor pretreatment effect, cumbersome acid-base adjustment, large amount of oxidative pretreatment, large amount of sludge and unstable operation. Method: 1. Add packing and pretreated industrial wastewater into the catalytic reduction biological hydrolysis tank, add ozone catalytic packing and hydrogen peroxide into the ozone catalytic reaction tank, and pump the upper layer liquid of the industrial wastewater in the catalytic reduction biological hydrolysis tank to the ozone catalytic reaction Catalytic oxidation is carried out in the tank, and the industrial wastewater in the ozone catalytic reaction tank is returned to the catalytic reduction biological hydrolysis tank; the industrial wastewater flows into the flocculation sedimentation tank through the water outlet, the pH is adjusted to 7-8.5, polyacrylamide is added, and precipitation is completed to complete the industrial wastewater. Catalytic hydrolysis pretreatment. The invention can obtain a method for catalytic hydrolysis pretreatment of industrial park wastewater.
Owner:工大环境股份有限公司

Trapping device and process for production of 3,4-dichlorobenzonitrile

The invention discloses a trapping device and process for production of 3,4-dichlorobenzonitrile. The device is simple and reasonable in structural design; the implementation feasibility is high, thepracticability is high, more than 90% of ammonium chloride and more than 8% of 3,4-dichlorobenzonitrile are captured by a first-stage catcher through a dry capture method, more than 76% of 3,4-dichlorobenzonitrile is captured by a second-stage catcher through a dry capture method, latent heat of vaporization of water is fully utilized by the first-stage catcher, and the usage amount of spray liquid-water is small; besides, about 15% of the 3,4-dichlorobenzonitrile crude product collected by a third-stage catcher and a bath tower is dissolved by hot water, dehydrated, rectified and purified toobtain a liquid pure product of 3,4-dichlorobenzonitrile. The generation amount of coke oil and solid waste during the rectification process is low. Compared with a traditional multi-stage wet capturemethod, the consumption of 3,4-dichlorobenzonitrile is reduced, the investment cost of rectification equipment is reduced by more than half, the rectification energy consumption is equivalent to 15%of that of the traditional method, and the economic benefit is good.
Owner:常州新日催化剂股份有限公司

System and method for recovering acid and alkali from high-salt-content deacidification wastewater

The invention discloses a system for recovering acid and alkali from high-salt-content deacidification wastewater. The system is characterized by comprising a homogenizing tank, a first reaction tank, a second reaction tank, a sedimentation tank, a concentration tank, an ultrafiltration device, an ultrafiltration water producing tank, a nanofiltration device, a nanofiltration water producing tank, a reverse osmosis device, a reverse osmosis concentrated water tank and a bipolar membrane electrodialysis device which are connected in sequence, a CaCl2 dosing device is arranged over the first reaction tank, a Na2CO3 dosing device is arranged over the second reaction tank, and a hydrochloric acid dosing device is arranged above the ultrafiltration water producing tank. According to the method, NaCl in the deacidification wastewater can be effectively separated through cooperation of chemical reaction and membrane treatment devices with different levels of precision, and NaOH and HCl are prepared through electrodialysis, so that acid and alkali can be recycled from the deacidification wastewater, the resource utilization of the deacidification wastewater is realized, the solid waste output is reduced, and the energy conservation and emission reduction degree is improved.
Owner:浙江省环保集团有限公司

Composite sponge material and preparation method thereof, and application of composite sponge material in treatment of high-salt high-calorific-value wastewater

The invention relates to a composite sponge material and a preparation method thereof, and application of the composite sponge material in treatment of high-salt high-calorific-value wastewater. The composite sponge material is formed by mixing an inorganic drying agent and an organic curing coagulant, can efficiently cure wastewater, and overcomes the problems that special wastewater is difficult to treat, treatment cost is high and secondary pollution is caused. A using method of the composite sponge material comprises the following steps: uniformly mixing wastewater and the composite sponge material to a semi-solid state, and conducting drying to obtain solid waste; and incinerating the solid waste. The composite sponge material is suitable for treatment of the high-salt high-calorific-value wastewater, good in effect, mild in incineration conditions and short in incineration time, and the solid waste obtained after incineration is powdery, so the problem that incineration equipment is damaged by molten salt in a direct incineration process of the high-calorific-value wastewater can be effectively solved; and a drying agent in the material can be recycled, and treatment cost is low.
Owner:南京乐透思高新材料科技有限公司

Arsenic removal device with monitoring and regenerating functions and use method thereof

The invention belongs to the technical field of water treatment and particularly provides an arsenic removal device with monitoring and regenerating functions and a use method thereof. The arsenic removal device consists of a main body, a regenerating device, a monitoring system and a power control system, wherein the main body is a fixed bed processor equipped with an inner core made from a cloth-shaped arsenic adsorption fiber material. The arsenic removal device is characterized in that the cloth-shaped arsenic adsorption fiber material is adopted to manufacture the arsenic removal inner core, the arsenic removal inner core is formed by rolling the cloth-shaped arsenic adsorption fiber material around a central shaft, the arsenic removal inner core is cylindrical, is tight in interlayer lamination and is vertically mounted in a housing, and no gap exists between the layers of the cloth-shaped arsenic adsorption fiber material or between the arsenic removal inner core and the inner wall of the housing; the regenerating system consists of a regenerated liquid tank, a pump valve and a pipeline; and the monitoring system consists of a quartz column with a rapid arsenic detection reagent and comparison columns. The arsenic removal device has the advantages of excellent water permeability, high arsenic removal efficiency, easy desorption regeneration and the like, can monitor the arsenic concentration of water in real time and provides instructions for desorption regeneration while ensuring that the effluent meets the discharge standard.
Owner:江阴和悦鑫环保科技有限公司

A steel slag treatment method using oxidation desulfurization and reduction dephosphorization two-step method

The invention relates to a steel slag treatment method using a two-step method of oxidation desulfurization and reduction dephosphorization, belongs to the technical field of iron and steel metallurgy and resource utilization, and solves the problem of enrichment of sulfur and phosphorus in the existing steel slag recycling technology. The steel slag treatment method using the two-step method of oxidation desulfurization and reduction dephosphorization includes S1. Oxidative desulfurization of steel slag; passing Ar and O into molten steel slag 2 The mixed gas, the SO obtained by oxidation 2 Overflow and remove from the slag phase, the removal rate of S is 82-97%; S2. The desulfurized steel slag obtained in step S1 is subjected to gas-based reduction dephosphorization; the reducing gas is CO and CO 2 The mixed gas, the removal rate of phosphorus reaches more than 80%, and the P obtained by reduction 2 Spilled and removed from the slag. The invention can completely solve the problem of removing sulfur and phosphorus in steel slag, greatly improve the recycling rate of steel slag, realize the full utilization of steel slag, S and P, reduce the cost of steelmaking, increase the utilization value of sulfur and phosphorus, and have broad application prospects.
Owner:钢研晟华科技股份有限公司

An arsenic removal device with monitoring and regeneration functions and its application method

The invention belongs to the technical field of water treatment and particularly provides an arsenic removal device with monitoring and regenerating functions and a use method thereof. The arsenic removal device consists of a main body, a regenerating device, a monitoring system and a power control system, wherein the main body is a fixed bed processor equipped with an inner core made from a cloth-shaped arsenic adsorption fiber material. The arsenic removal device is characterized in that the cloth-shaped arsenic adsorption fiber material is adopted to manufacture the arsenic removal inner core, the arsenic removal inner core is formed by rolling the cloth-shaped arsenic adsorption fiber material around a central shaft, the arsenic removal inner core is cylindrical, is tight in interlayer lamination and is vertically mounted in a housing, and no gap exists between the layers of the cloth-shaped arsenic adsorption fiber material or between the arsenic removal inner core and the inner wall of the housing; the regenerating system consists of a regenerated liquid tank, a pump valve and a pipeline; and the monitoring system consists of a quartz column with a rapid arsenic detection reagent and comparison columns. The arsenic removal device has the advantages of excellent water permeability, high arsenic removal efficiency, easy desorption regeneration and the like, can monitor the arsenic concentration of water in real time and provides instructions for desorption regeneration while ensuring that the effluent meets the discharge standard.
Owner:江阴和悦鑫环保科技有限公司
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