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37results about How to "Simple production process and equipment" patented technology

Preparation method for high-purity magnesium oxide

The invention discloses a preparation method for high-purity magnesium oxide. The preparation method for high-purity magnesium oxide comprises the following steps of: calcining magnesite to generate caustic calcined magnesite; heating the caustic calcined magnesite and ammonium salt mother liquor to boil, and distilling; absorbing the distilled mixture of ammonia gas and water by carbonated aqueous ammonia I to form carbonated aqueous ammonia II; carbonizing the carbonated aqueous ammonia II by CO2 from a calcining furnace or flue gas from a washing-cooling tower in a carbonization tower to generate the carbonated aqueous ammonia I, and conveying the carbonated aqueous ammonia I in a storage tank I; conveying a part of the carbonated aqueous ammonia I entering in the storage tank I in an ammonia absorption tower for recycling; mixing the other part of the carbonated aqueous ammonia I with the magnesium salt solution formed by distillation in a reaction kettle, so as to generate basic magnesium carbonate and ammonium salt; filtering and conveying the ammonium salt in the reaction kettle for recycling; and calcining basic magnesium carbonate to prepare high-purity magnesium oxide. According to the preparation method for high-purity magnesium oxide disclosed by the invention, by recycling CO2 and ammonia gas generated during the reaction process, the problem of high raw material consumption due to massive use for ammonium bicarbonate during the production process is solved, and the production cost is reduced; and moreover, the product is high in purity, and the production process is simple in equipment and capable of being used for industrial production for high-purity magnesium oxide.
Owner:SHAANXI NORMAL UNIV

Preparation method for 2-phenylpropionic acid

The invention discloses a preparation method for 2-phenylpropionic acid. The preparation method is characterized by comprising a 2-phenyl-2-cyano methyl propionate preparation stage, a 2-phenyl propionitrile preparation stage and a 2-phenylpropionic acid preparation stage, wherein the 2-phenyl-2-cyano methyl propionate preparation stage comprises: mixing benzyl cyanide, dimethyl carbonate, methylbenzene and sodium methoxide to obtain a mixture, heating the mixture to 20-100 DEG C, controlling the pressure to 0.5-6MPa and carrying out thermal-insulation reaction for 1-10 hours; after the reaction is ended, steaming out a byproduct methanol under the normal pressure, cooling the mixture to 35 DEG C, dropwise adding dimethyl sulfate DMS at constant speed by controlling the temperature to 35-85 DEG C, and carrying out the thermal-insulation reaction for 1-10 hours at 45-105 DEG C after the dropwise-adding is ended; cooling to 35 DEG C, adding water, stirring, dissolving, and layering; desolventizing to recycle toluene, thereby obtaining compound ester; and carrying out basic hydrolysis reaction and acidification reaction to finally prepare a finished product, wherein the purity of the finished product is high, and the yield of the finished product is higher than 92%. Besides, the production process disclosed by the invention adopts simple equipment and is low in production cost.
Owner:ZHEJIANG BOJU NEW MATERIALS CO LTD

Intrinsically safe latex matrix ground station

ActiveCN104387214ASimple production process and equipmentEliminates the possibility of thermal explosionsExplosive working-up apparatusTruckThermal explosion
The invention belongs to the technical fields of latex matrix preparation technologies and apparatuses for mobile ground assisting facilities in the civil explosive industry, and relates to an intrinsically safe latex matrix ground station. The intrinsically safe latex matrix ground station includes a water phase tank, an oil phase tank, a water phase pump, an oil phase pump and a static emulsifier, the inlet and the outlet of the water phase pump are respectively connected with the outlet of the water phase tank and the water phase inlet of the static emulsifier through pipelines, and the inlet and the outlet of the oil phase pump are respectively with the outlet of the oil phase tank and the oil phase inlet of the static emulsifier through pipelines. The station uses the fully static emulsifier as an emulsifying device, and is a latex matrix preparation and conveying apparatus without stirring, mechanical shearing or matrix pump conveying of colloid in the matrix emulsifying process, the static emulsifier designed by using a jet eddy current emulsifying principle, and a latex matrix prepared in the invention is directly added into a colloid tank in an emulsifying mixing truck from the outlet of the static emulsifier through a flexible tube, so the thermal explosion possibility of mechanical friction is eliminated, and the total energy consumption of a whole production line is reduced.
Owner:SHIJIAZHUANG SUCCESS MACHINERY ELECTRICAL

Asphalt pavement permeable diversion road flat stone and diversion road structure

PendingCN110761142AIncrease runoffPlay a retention roleIn situ pavingsSingle unit pavingsCompressive resistanceIn vehicle
The invention discloses an asphalt pavement permeable diversion road flat stone and a diversion road structure. The asphalt pavement permeable diversion road flat stone includes a diversion road flatstone body, a tamped soil layer, a pavement, a permeable road edge stone and an asphalt road surface layer. The pavement, the permeable road edge stone and the asphalt road surface layer and the diversion road flat stone are arranged above the tamped soil layer, the permeable road edge stone is arranged on one side of the pavement, one side of diversion road flat stone is close to the permeable road edge stone, the other side of the diversion road flat stone is connected with an asphalt road surface, and the diversion road flat stone is arranged above a sewage disposal well ditch. The size ofthe prepared diversion road flat stone can be changed according to the specific requirements of road traffic design, the thickness is no less than 60MM, diabase and the like or the other broken stonesare arranged on the bottom layer, permeable cement is of a porous structure, and the surface layer is arranged to be of a cement-based or polymer-silica sand fine hole structure. The compressive strength of the prepared diversion road flat stone is more than and equal to 45 MPa, the flexural strength is more than and equal to 4.0 MPa, the city vehicle-mounted load capacity can be completely met,and the surface layer is fine in holes and abrasion-resistant and attractive. All-directional seepage drainage is achieved, and the runoff volume is much higher than that of general flat stones.
Owner:江西亘森生态材料有限公司

Aliphatic-series high-efficiency water reducing agent and preparation method thereof

The invention discloses an aliphatic-series high-efficiency water reducing agent and a preparation method thereof. The preparation method comprises the following steps: adding formaldehyde and sodiumpyrosulfite into one container and performing sulfonation reaction for 30 to 40 minutes under the reflux condensation condition; then adding acetone to keep reflux reaction for 20 to 40 minutes under30 DEG C to 50 DEG C to obtain a pre-melted material A; adding water and sodium sulfite into another container, evenly stirring and dissolving and obtaining a material B; dropwise adding the pre-melted material A into the material B, warming to 75 DEG C to 80 DEG C within 20 to 40 minutes of dropwise adding to performing condensation constant-temperature reaction and finishing reaction, wherein dropwise adding time is totally 2 to 3 hours; adding water to dilute, reducing temperature to 55 DEG C or below, adding acid to neutralize, adjusting a PH value to 11 to 13.5 and adding an activating agent. The preparation method has the advantages of no heat source, stable and quick production, large productivity, small investment, reduced material cost, good environmental friendliness and reducedcost; the prepared high-efficiency water reducing agent has excellent performance; furthermore, the prepared high-efficiency water reducing agent has little harmful impurities, and effects to reinforced concrete durability are reduced.
Owner:JIANGSU BAIRUIJI NEW MATERIAL

Intrinsically safe latex-based ground station

The invention belongs to the technical fields of latex matrix preparation technologies and apparatuses for mobile ground assisting facilities in the civil explosive industry, and relates to an intrinsically safe latex matrix ground station. The intrinsically safe latex matrix ground station includes a water phase tank, an oil phase tank, a water phase pump, an oil phase pump and a static emulsifier, the inlet and the outlet of the water phase pump are respectively connected with the outlet of the water phase tank and the water phase inlet of the static emulsifier through pipelines, and the inlet and the outlet of the oil phase pump are respectively with the outlet of the oil phase tank and the oil phase inlet of the static emulsifier through pipelines. The station uses the fully static emulsifier as an emulsifying device, and is a latex matrix preparation and conveying apparatus without stirring, mechanical shearing or matrix pump conveying of colloid in the matrix emulsifying process, the static emulsifier designed by using a jet eddy current emulsifying principle, and a latex matrix prepared in the invention is directly added into a colloid tank in an emulsifying mixing truck from the outlet of the static emulsifier through a flexible tube, so the thermal explosion possibility of mechanical friction is eliminated, and the total energy consumption of a whole production line is reduced.
Owner:SHIJIAZHUANG SUCCESS MACHINERY ELECTRICAL

Novel atenolol slow-release drop pill and preparation method thereof

Hypertension is recognized by the medical community at home and abroad as the "most ferocious killer" that threatens the human life, the mortality rate of hypertension is higher than that of any otherdisease, and hypertension seriously affects the human health. Atenolol tablets are administered twice per day, and the blood concentration fluctuates greatly, thereby being necessary to prepare the atenolol tablets into a slow-release preparation. The invention relates to an atenolol slow-release drop pill capable of quickly taking effect and slowly releasing drugs and used for treating hypertension and angina, performing maintenance treatment of myocardial infarction and treating arrhythmia, hyperthyroidism and the like, and a preparation method of the atenolol slow-release drop pill. In order to make up for the deficiencies of the prior art, the invention provides an atenolol slow-release drop pill preparation. The atenolol slow-release drop pill provided by the invention is characterized in that a hydrophobic skeleton capable of slowly releasing drugs and Tween-80 with a solubilizing effect are added on the basis of the existing drop pill technology, the deficiencies of the prior art are effectively overcome, and the atenolol slow-release drop pill has the advantages of uniform drug dispersion, sufficient drug release, long drug release time, reduced patient medication frequency and high bioavailability.
Owner:ZHENGZHOU TAIFENG PHARMA CO LTD

A kind of preparation method of 2-phenylpropionic acid

The invention discloses a preparation method for 2-phenylpropionic acid. The preparation method is characterized by comprising a 2-phenyl-2-cyano methyl propionate preparation stage, a 2-phenyl propionitrile preparation stage and a 2-phenylpropionic acid preparation stage, wherein the 2-phenyl-2-cyano methyl propionate preparation stage comprises: mixing benzyl cyanide, dimethyl carbonate, methylbenzene and sodium methoxide to obtain a mixture, heating the mixture to 20-100 DEG C, controlling the pressure to 0.5-6MPa and carrying out thermal-insulation reaction for 1-10 hours; after the reaction is ended, steaming out a byproduct methanol under the normal pressure, cooling the mixture to 35 DEG C, dropwise adding dimethyl sulfate DMS at constant speed by controlling the temperature to 35-85 DEG C, and carrying out the thermal-insulation reaction for 1-10 hours at 45-105 DEG C after the dropwise-adding is ended; cooling to 35 DEG C, adding water, stirring, dissolving, and layering; desolventizing to recycle toluene, thereby obtaining compound ester; and carrying out basic hydrolysis reaction and acidification reaction to finally prepare a finished product, wherein the purity of the finished product is high, and the yield of the finished product is higher than 92%. Besides, the production process disclosed by the invention adopts simple equipment and is low in production cost.
Owner:ZHEJIANG BOJU NEW MATERIALS CO LTD

Preparation method of nanoscale zirconia ceramic powder for spraying

The invention provides a preparation method of nanoscale zirconia ceramic powder for spraying. The preparation method provided by the invention comprises the following steps of ingredient ball milling, atomization drying, sieving gradation, dry-pressing molding, sintering compaction, crushing polishing, autogenous grinding trimming, and screening detection. The preparation method provided by the invention has the advantages that nanoscale yttria-stabilized zirconia ceramic powder for spraying is directly prepared by high temperature ceramic preparation and crushing and through high-temperature sintering at a temperature of 1500 to 1600 DEG C in preparation, ZrO2 has a yttria-stabilized zirconia (YSZ) crystal structure or a yttria-partially stabilised zirconia (PYSZ) crystal structure at ahigh temperature, in other word, ZrO2 comprises monoclinic crystals and cubic crystals; the YSZ crystal structure or the PYSZ crystal structure has high strength, high toughness, good wear resistance, good high temperature resistance, good corrosion resistance, high rigidity, no magnetic conductivity and an electrical insulating property; the nanoscale zirconia ceramic powder obtained by the preparation method has density of 6.00g / cm<3>, Moh's hardness of 9, compressive strength of 1170Mpa and good thermal shock resistance; and through granulator-based autogenous grinding trimming, the nanoscale zirconia ceramic powder obtained by the preparation method has volume density of 1.15 to 1.45g / m<2> (min)% and good fluidity.
Owner:重庆利特高新技术有限公司
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