A preparation method of a
zinc cobaltate nanometer material doped with
zinc oxide comprises the following steps: dispersing the
zinc oxide and cobaltic
oxide in deionized water according to a certain
molar ratio, so as to obtain a first solution; heating the first solution for a certain time at a first constant temperature, so as to obtain a second solution; cooling the second solution until the temperature of the second solution to be the
room temperature, and performing rinsing and low-temperature
drying, so as to obtain the zinc cobaltate nanometer material; wherein the certain
molar ratio is (1:2)-(2:1), the first constant temperature is 120-180 DEG C, and the certain time is 12-48 hours. The preparation method adopts a hydro-thermal
synthesis system, and directly takes the oxide (i.e. the zinc oxide) as the reactant to prepare the zinc cobaltate nanometer material; the reaction time,
reaction temperature and reactant
concentration ratio are regulated; the variety and using amount of additive are changed. Therefore, the morphology and grain sizes of the particles are controlled. The preparation method has the advantages of low
raw material and equipment costs, simple process, easiness in operation, relatively-low
reaction temperature and low environment
pollution.