The utility model discloses a rectification device in an
isobutanol production process, which comprises a rectification tank, a condenser and a
reboiler, the condenser is arranged at the top of the rectification tank and is used for circularly condensing gaseous materials, the
reboiler is arranged at the bottom of the rectification tank and is used for circularly gasifying liquid materials, a feeding
pipe is arranged on the outer side of the rectification tank, and the feeding
pipe is communicated with the
reboiler. Flow guide partition plates which are vertically arranged are fixedly mounted in the rectification tank. Recondensed liquid gathers on the flow guide partition plate, the liquid level exceeds the overflow plate and flows downwards, steam at the bottom flows upwards along the air holes in the flow guide partition plate under the action of pressure, gas-liquid two-phase contact is achieved, and meanwhile due to the fact that the flow equalizing cover on the flow guide partition plate is completely immersed by
stock solution, the flow equalizing cover is completely immersed by the
stock solution. The
stock solution at the bottom is heated by the reboiler to form steam, and the steam rises and is dispersed by the flow equalizing cover, so that more efficient contact efficiency with the stock solution is realized, and the device has the advantages of high gas-liquid double-phase contact efficiency, improvement of rectification efficiency and reduction of equipment
energy consumption.