The invention provides a hydro-thermal synthesis method for a TS-1
molecular sieve. The hydro-thermal synthesis method includes the steps that 1, a
silicon source and a template agent are mixed to obtain
silicon source
hydrolysate, a
titanium source and polyhydric
alcohol are mixed to be added into the
silicon source
hydrolysate, and then water is added; 2, a product obtained through step1 is subjected to pre-
crystallization for 5-24 hours; 3, a silicon source is added again and heated to 60 DEG C-90 DEG C, and then polyhydric
alcohol is removed; 4, a product obtained through step3 is crystallized, after the
crystallization reaction, a reaction mixture is subjected to
solid-liquid separation, and a
solid is taken to be dried and calcined. In the hydro-thermal synthesis method, after the silicon source and the
titanium source are gelatinized,
alcohol is not removed, namely,
crystallization is performed for 5-24 hours at 90 DEG C-100 DEG C under the presence of alcohol, in this way, forming of non-framework
titanium can be effectively reduced, and the content of framework titanium can be increased. In the process of constructing a multi-
level structure in the TS-1
molecular sieve, no mesporous template agent, organosilane and other organic additives are needed, in the whole synthesis process, operation is easy, the cost is low, an expected amplification effect is small, and large-scale industrial production and popularization are easy.