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54results about How to "Uniform surface coating" patented technology

Preparation method of alumina composite nickel-cobalt lithium manganate ternary material

The invention provides a preparation method of an alumina composite nickel-cobalt lithium manganate ternary material. The preparation method comprises the following steps: (1), preparing liquor A; (2), preparing liquor B; (3), installing and configuring a reaction flask; (4), adding the liquor A and the liquor B into the reaction flask to participate in hybrid reaction; (5), preparing liquor C, and adding into the flask for reaction; (6), obtaining a precursor by suction-filtering, washing and drying; and (7), mixing and roasting the precursor with a lithium source to prepare the alumina composite nickel-cobalt lithium manganate ternary material. The preparation method disclosed by the invention has the beneficial effects that firstly, liquid-phase coating is adopted, production preparation period is short, efficiency is high, and coating and dispersing are uniform; secondly, the coating layer alumina on the surface of the ternary material is a film with an amorphous structure, so that charging and discharging voltage difference is reduced, multiplying power performance and high-performance performance of the material are improved; and thirdly, characteristics of a solid-liquid phase interface among an anode material, electrolyte and a diaphragm are improved by alumina film-coating, so that velocity and efficiency of electrochemical reaction are improved.
Owner:博尔特新材料(银川)有限公司

Conducting-polymer dipped and coated lithium-ion battery composite-electrode material and preparation method thereof

The invention provides a conducting-polymer dipped and coated lithium-ion battery composite-electrode material and a preparation method thereof. A high-polymer conducting polymer is coated on the lithium-ion battery electrode material of the composite electrode material, the conducting polymer is the conducting polymer which is easily dispersed into an aqueous solution, and the aqueous solution of dispersants, such as polystyrolsulfon acid and the like is used as a dispersing medium. The composite electrode material is prepared through the following steps of: dipping a lithium-ion anode material or cathode material into the aqueous solution of the high-polymer conducting polymer, and obtaining the surface-coated lithium-ion battery composite-electrode material through dipping and coating processing. The composite electrode material has cheap preparation raw materials, the surface of the novel composite electrode material is uniformly coated, and the composite electrode material has the advantages of high specific capacity, high charging and discharging efficiency and long cycling life. Compared with the prior art, the preparation method of the composite electrode material has the advantages of simple process, low cost, good effect and green and environment-friendly production process, is easy for industrial popularization and is convenient for large-scale industrialized production.
Owner:GUANGZHOU INST OF ENERGY CONVERSION - CHINESE ACAD OF SCI

Coating method for improving electrochemical property of high-nickel ternary nickel cobalt manganese anode material

The invention discloses a coating method for improving electrochemical properties of a high-nickel ternary nickel cobalt manganese anode material. The coating method comprises the following steps: dissolving a titanium source into a solvent so as to obtain a solution, dissolving a lithium source, and further adding citric acid so as to obtain a mixed solution; uniformly dispersing a high-nickel ternary nickel cobalt manganese anode material into a solvent, adding the mixed solution, uniformly mixing, and performing a hydrothermal reaction or a solvent thermal reaction so as to obtain a reaction solution; evaporating the reaction solution to a gel state, and drying so as to obtain an anode material mixture; calcining the anode material mixture, thereby obtaining the high-nickel ternary nickel cobalt manganese anode material with a lithium titanate coating layer. The coating method for improving the electrochemical properties of the high-nickel ternary nickel cobalt manganese anode material, which is disclosed by the invention, is simple in process, low in cost and good in repeatability, the obtained coating layer is high in crystallization degree, small in particle size and good inuniformity, and the charge and discharge specific capacity, the circulation property and the multiplying power of the high-nickel ternary nickel cobalt manganese anode material can be improved.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY

Preparation method for improving interfacial properties of carbon fiber composite material

The invention provides a preparation method for improving interfacial properties of a carbon fiber composite material. The method is characterized by comprising the steps of firstly, preparing plasma activated carbon fiber; secondly, preparing a maleic anhydride dimethylbenzene solution; thirdly, subjecting the activated carbon fiber to ultrasonic infiltration; fourthly, performing grafting of maleic anhydride; and fifthly, purifying a crude product of the plasma activated carbon fiber which the maleic anhydride is grafted to. The method has the advantages that the free radicals formed on the surface of carbon fiber are processed through plasmas of argon-oxygen mixed gas, so that the polymerization reaction speed of the free radicals and the maleic anhydride is accelerated and the degree us improved; the reaction speed is accelerated through a high temperature, and the grafting reaction time is only 3 min to 7 min, so that grafting carbon fiber which is uniform in surface coating and high in grafting rate and has certain quantities of anhydride groups is obtained, the grafting carbon fiber and epoxy resin are subjected to reaction well, and the interfacial properties of the composite material is improved; and the method is energy-saving, environment-friendly and convenient to process.
Owner:DONGHUA UNIV

Porous lithium iron phosphate/carbon composite microspheres and preparation method thereof

The invention provides porous lithium iron phosphate / carbon composite microspheres and a preparation method thereof. The porous lithium iron phosphate / carbon composite microspheres and the preparation method thereof are characterized in that iron phosphate oxalate is used as a precursor and the preparation method comprises the following steps: (1) dispersing solution of iron salt and phosphate solution into a precipitating agent ethanol, adding lithium salt, carrying out ultrasonic stirring to enable the solution of iron salt, the phosphate solution and the lithium salt to be totally dissolved, and adding a certain quantity of oxalic ethanol solution into the obtained solution; (2) placing the obtained mixture into an oven to dry at a certain temperature so as to obtain a yellow jelly iron phosphate oxalate precursor; and (3) after mixing a carbon source and the iron phosphate oxalate precursor, calcining to obtain the porous lithium iron phosphate / carbon composite microspheres. The preparation method provided by the invention is low in cost and is simple and easy to operate; the pH does not need to be regulated; the products have high purity, high tap density and good repeatability; the products are spherical particles formed by self-assembling disk nano-scale particles, and thus, the specific surface area is large; and moreover, the diffusion path of lithium ions is greatly shortened, so that the porous lithium iron phosphate / carbon composite microspheres have excellent electrochemical property and are suitable for large-scale production.
Owner:QINGDAO UNIV OF SCI & TECH

A kind of preparation method of aluminum oxide composite nickel cobalt lithium manganese oxide ternary material

The invention provides a preparation method of an alumina composite nickel-cobalt lithium manganate ternary material. The preparation method comprises the following steps: (1), preparing liquor A; (2), preparing liquor B; (3), installing and configuring a reaction flask; (4), adding the liquor A and the liquor B into the reaction flask to participate in hybrid reaction; (5), preparing liquor C, and adding into the flask for reaction; (6), obtaining a precursor by suction-filtering, washing and drying; and (7), mixing and roasting the precursor with a lithium source to prepare the alumina composite nickel-cobalt lithium manganate ternary material. The preparation method disclosed by the invention has the beneficial effects that firstly, liquid-phase coating is adopted, production preparation period is short, efficiency is high, and coating and dispersing are uniform; secondly, the coating layer alumina on the surface of the ternary material is a film with an amorphous structure, so that charging and discharging voltage difference is reduced, multiplying power performance and high-performance performance of the material are improved; and thirdly, characteristics of a solid-liquid phase interface among an anode material, electrolyte and a diaphragm are improved by alumina film-coating, so that velocity and efficiency of electrochemical reaction are improved.
Owner:博尔特新材料(银川)有限公司

Wet surface treatment process for calcium carbonate

The invention discloses a wet surface treatment process for calcium carbonate, which relates to the technical field of surface treatment for calcium carbonate. The wet surface treatment process for calcium carbonate comprises choice of material, agitation, addition of modifier and washing and drying. The steps are as follows: choice of material: the average grain size of chosen calcium carbonate is about 30nm to 70nm, and the crystal form structure is the form of calcite; agitation: the calcium carbonate powder is put into a reaction kettle, so that a calcium carbonate suspension is prepared,the temperature of the calcium carbonate suspension is kept within a range from 70 to 80 DEG C, and the agitation speed of agitating blades is controlled; addition of modifier: the temperature of thecalcium carbonate suspension and the agitation speed in step 2 are kept unchanged, the ratio of the dosage of added modifier to the dosage of the calcium carbonate is 1-4/100g, and reaction time is within a range from 20 to 30 minutes; and washing and drying: the hot slurry is filtered, the filter cake is washed to remove the unreacted modifier, and after drying, active calcium carbonate powder isobtained. The operation process of the wet surface treatment method disclosed by invention is simple, and in the process of treatment, an activator can more uniformly wrap the surface of calcium carbonate.
Owner:XUANCHENG XINTAO CALCIUM CARBONATE

Method for preparing copper cladded iron composite powder

A preparation method of copper-clad iron composite powder which includes procedures as follow: the alcaline etching waste liquor containing copper is added into the acid etching waste liquor, thus feed solution with pH between 2 and 4.5 is obtained and the concentration of copper between 50 and 100g / L. The reduced iron powder is washed by acid, delivered to a reaction kettle with turbine type stirring, added with water with stirring, added orderly with dispersant agent and inhibitor and evenly with feed solution containing copper with continuous stirring, making the copper completely claddingthe surface of the iron powder grain, thus copper-clad iron composite powder is obtained. Then the copper-clad iron composite powder is subject to pumping filtration, washing, centrifugal dehydration,antioxidation treatment, vacuum drying and screen separation, thus termination production is obtained. The method of the invention can make the copper evenly, tightly, firmly and completely claddingthe iron powder grain, and not be oxidized for six months of storage, thus increasing the oxidation resistance. The prepared copper-clad iron powder by the invention has bright surface colour and lustre, high cladding rate, even and compact surface cladding, futhermore, the cost is lower compared with prior preparation methods because of avoiding using copper sulfate.
Owner:SHENZHEN SHENTOU ENVIRONMENT TECH CO LTD

Liquid friction-increasing rubber for shoe plate of rear-drum brake and preparation method thereof

The invention relates to liquid friction-increasing rubber for a shoe plate of a rear-drum brake and a preparation method thereof. The preparation method comprises the following steps: 1, dissolving silicon carbide, antimony sulfide, benzoyl peroxide, sulphur, quartz powder and Buna-N rubber in ethyl acetate and fully stirring; 2, smearing the above mixture onto the surface of a processed shoe plate by a brushing method or an infiltration method; 3, standing and air-drying; 4, placing the shoe plate in a constant-temperature vulcanization box to fully vulcanize rubber; and 5, cooling the vulcanized shoe plate and directly applying the shoe plate in assembling of the brake. The invention has the following beneficial effects: as the friction-increasing formula is blended into a liquid state, the liquid friction-increasing rubber is convenient to smear, can produce productivity and is suitable for mass production; the surface coating is uniform so as to effectively cancel influence of processing precision and raise conjoint ratio; as NRB (Buna-N rubber) is used as a base material, elasticity and buffer performance are enhanced and noise is reduced effectively; and as quartz powder is used to replace emery, the friction-increasing material is easier to distribute uniformly, hard lumps and hard spots are eliminated, and comfortability of drivers is improved.
Owner:ZHEJIANG WANXIANG SYST +1

Graphene shoulder and neck pain patch and preparation method thereof

The invention discloses a graphene shoulder and neck pain patch comprising a backing layer, a graphene film layer, a raw material medicine layer and an anti-sticking release paper layer. The raw material medicine layer is placed between the anti-sticking release paper and the backing layer; a raw material medicine is in the middle position of the raw material medicine layer and comprises the following substances: radix angelica sinensis, rhizoma gastrodiae, pilose antler, radix saposhnikoviae, notopterygium root, radix angelicae tuhuo, baked ginger, asarum sieboldii, fructus evodiae, safflower, radix dipsaci and garden balsam stem; the raw material medicine is also mixed with sodium hydroxymethylcellulose, sodium alginate and glycerol, so the raw material medicine is uniform in coating, has good adhesion and does not produce greater fluidity; the outer side of the raw material medicine is laid with the graphene film layer which can effectively activate the vitality of damaged cells andrestore normal function. The graphene shoulder and neck pain patch has the advantages of low price and convenient and quick use, and has the functions of relaxing tendons and dredging collaterals, activating blood circulation and promoting qi. The graphene film layer at the bottom layer can effectively promote the transmission of drugs, accelerates the absorption of the raw material medicine, andhas a good healing effect on shoulder and neck pain and other symptoms.
Owner:GUANGXI UNIV OF CHINESE MEDICINE

Preparation method for improving interfacial properties of carbon fiber composite material

The invention provides a preparation method for improving interfacial properties of a carbon fiber composite material. The method is characterized by comprising the steps of firstly, preparing plasma activated carbon fiber; secondly, preparing a maleic anhydride dimethylbenzene solution; thirdly, subjecting the activated carbon fiber to ultrasonic infiltration; fourthly, performing grafting of maleic anhydride; and fifthly, purifying a crude product of the plasma activated carbon fiber which the maleic anhydride is grafted to. The method has the advantages that the free radicals formed on the surface of carbon fiber are processed through plasmas of argon-oxygen mixed gas, so that the polymerization reaction speed of the free radicals and the maleic anhydride is accelerated and the degree us improved; the reaction speed is accelerated through a high temperature, and the grafting reaction time is only 3 min to 7 min, so that grafting carbon fiber which is uniform in surface coating and high in grafting rate and has certain quantities of anhydride groups is obtained, the grafting carbon fiber and epoxy resin are subjected to reaction well, and the interfacial properties of the composite material is improved; and the method is energy-saving, environment-friendly and convenient to process.
Owner:DONGHUA UNIV

Composite coating method for the surface of heat-dissipating tooth parts

The invention discloses a compound painting method for surfaces of heat radiating teeth class parts. By utilizing the method, the root regions of heat radiating teeth can be reached, and the coating quality of deep regions is enhanced. The compound painting method is realized through the technical scheme: dividing the surfaces of the heat radiating teeth class parts into A, B, C and D painting regions according to the teeth width and teeth depth parameters of the heat radiating teeth, and carrying out three-stage stepped spraying treatment on the roots, side surfaces and tops of the heat radiating teeth class parts; first, using a thin-pipe long-neck spraying gun to carry out stepped spraying treatment on the bottom and side wall deep-cavity coating regions of the heat radiating teeth; avoiding other regions, carrying out skip spaced spraying on the bottom regions of the heat radiating teeth at a perpendicular angle, and then, spraying the side wall regions of the heat radiating teeth from bottom to top at an angle of 70-80 degrees; and after standing for 5-10 minutes, changing a common spraying gun after coated films are leveled, and carrying out large-area spraying on the top and other outer coating regions of the heat radiating teeth by using the common spraying gun.
Owner:10TH RES INST OF CETC
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