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46results about How to "Uniform surface structure" patented technology

Preparation method of transparent super-hydrophobic zinc oxide coating

The invention relates to a preparation method of a transparent super-hydrophobic zinc oxide coating on a glass substrate. The preparation method comprises the following steps of a, substrate pretreatment; b, zinc oxide solution preparation; c, zinc oxide coating preparation; and d, zinc oxide coating surface modification. Compared with the prior art, the preparation method has the beneficial effects of simple equipment process, low cost and mild reaction condition and is beneficial to large-scale industrial production. The transparent super-hydrophobic zinc oxide coating prepared by using the method has excellent hydrophobicity and transparency; the contact angle is larger than 160 degrees, the rolling angle is smaller than 8 degrees, and water drops can freely roll on the coating, so that the transparent super-hydrophobic zinc oxide coating has relatively good self-cleaning performance; and the light transmittance is approach to 90% which is close to that of blank glass, so that the transparent super-hydrophobic zinc oxide coating has favorable visible light transmittance. A surface modifier used in the preparation method is an alkyl silane coupling agent instead of a fluorinated compound, so that the cost is low, the environment pollution is relatively low, and the modified coating is relatively stable.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

IF isotropic steel with stamping forming improved and manufacturing method thereof

The invention discloses IF isotropic steel with stamping forming improved and a manufacturing method of the IF isotropic steel. The IF isotropic steel is composed of, by weight percent, 0.0012% to 0.0026% of C, not larger than 0.026% of Si, 0.28% to 0.52% of Mn, not larger than 0.015% of P, not larger than 0.010% of S, 0.042% to 0.082% of Al, 0.046% to 0.066% of Ti, not larger than 0.0030% of N and the balance Fe and inevitable impurities. According to the IF isotropic steel, in the subsequent hot rolling, cold rolling, continuous annealing, flattening and bridging production processes, the rolling temperature is controlled to range from 580 DEG C to 620 DEG C, the cold rolling reduction rate is controlled to range from 85% to 95%, the annealing temperature is controlled to range from 708DEG C to 742 DEG C, the flattening ductility is controlled to range from 1.0% to 2.0%, and the bridging ductility is controlled to range from 0.03% to 0.10%; and according to the obtained IF isotropicsteel, the surface roughness Ra ranges from 0.36 micrometer to 0.56 micrometer, the peak concurrent Pc is larger than or equal to 126, the hardness ranges from 95 HV to 110 HV, the plastic strain ratio r90 value is larger than or equal to 1.8, the work-hardening exponent n90 value is larger than or equal to 0.18, and the delta r value is smaller than or equal to 0.20. The beneficial effect that when a round component is deeply stamped, no earing or galling defect is generated is achieved.
Owner:新余钢铁股份有限公司

Method for preparing self-toughening silicon nitride ceramics

The invention provides a method for preparing self-toughening silicon nitride ceramics, and the method comprises the following steps that first a silicon nitride foam ceramic billet is prepared, then sintered to prepare a silicon nitride crystal whisker skeleton body, and finally a silicon nitride organic precursor is dipped, cracked and made into ceramics and the self-toughening silicon nitride ceramics is prepared. According to the method for preparing self-toughening silicon nitride ceramics, the silicon nitride ceramic foam body is obtained by directly foaming; then the silicon nitride ceramic foam body is sintered; a long column-shaped beta-silicon nitride crystal bar is fully grown through the special structure of a large number of pore spaces of the ceramic foam when in sintering; the grown long column-shaped beta-silicon nitride (Si3N4) crystal bar is nearly fully filled in each foam pore in the silicon nitride foam ceramic body; the average slenderness ratio of the beta-Si3N4 crystal bar is 20, and the maximum slenderness ratio can reach about 30; and the silicon nitride crystal whisker skeleton body which is obtained by sintering the silicon nitride foam ceramic billet is dipped and cracked to obtain the self-toughening silicon nitride ceramics, and the toughening effect is good.
Owner:AEROSPACE INST OF ADVANCED MATERIALS & PROCESSING TECH

Method for producing composite panels in a continuously operating press and continuously operating press

The present invention relates to a method for producing composite panels in a continuously operating press (1). In the continuously operating press (1), the pressing blanks (7) are clamped and/or pressed in an area of material feeding segment before a main pressing area along a production direction (22) through steel strips (2,3) which operate around a bending roller (10) and are supported through a rolling rod (4), wherein in the area of material feeding segment, a material feeding segment heating plate (16) and/or hinging plate (12,13) which are used for regulating the geometric dimension of the material feeding segment clearance (E) along the production direction can adjust the clearance of the material feeding segment heating plate (16) and/or the hinging plates (12,13) and/or can be bended. The settlement solution of the utility model is characterized in that: in passing the areas (I,II) of the material feeding segment, the basically linear material feeding segment heating plate (16) which is perpendicular with the production direction (22) and at least two basically linear hinging plates (12,13) that are perpendicular with the production direction (22) are used on a surface side (33) in at least one segment along the production direction (22); and the bended material feeding segment heating plate (16) which is bended perpendicularly with the production direction (22) at least in the area along a longitudinal middle line (LML) along the direction of the pressing blank (7) from the opposite surface side (33). Additionally, the invention also relates to a continuously operating press.
Owner:DIEFFENBACHER GMBH & CO KG

Large-area uniform raman detection chip for porous membrane sensitivity enhancing and preparation method for large-area uniform raman detection chip

ActiveCN104406953AImprove Raman detection sensitivityIncrease the number of molecules to be testedRaman scatteringNanoporous membranePorous membrane
The invention provides a large-area uniform raman detection chip for porous membrane sensitivity enhancing and a preparation method for the large-area uniform raman detection chip. The raman detection chip comprises a substrate, a gold-based enhanced structural membrane which is formed on the substrate and is used as an electromagnetic enhancement layer of the raman detection chip, and a nano porous membrane which is formed on the outer surface of the gold-based enhanced structural membrane so as to enrich molecules to be detected. According to the large-area uniform raman detection chip for porous membrane sensitivity enhancing, the nano porous membrane serving as a molecule enriching layer can obviously increase the quantity of the molecules to be detected within a local enhanced electric field working range, so that the raman detection sensitivity of the chip is improved; the large-area uniform raman detection chip is particularly suitable for detection on small-molecular substances with ultralow concentration. The raman detection chip disclosed by the invention has the advantages of low preparation cost, high large-area uniformity and the like, and can suppress interference on a raman fingerprint diagram of the molecules to be detected due to metals.
Owner:INST OF ELECTRONICS CHINESE ACAD OF SCI

Preparation method of novel metal-biochar-based hydrogenation catalyst and application thereof

The invention belongs to the field of preparation of liquid fuel and chemical products through catalytic conversion of biomass, and relates to a preparation method of a novel metal-biochar-based hydrogenation catalyst and an application thereof. The method comprises the following steps: preparing a template agent suspension; then introducing coffee residue slurry, stirring, drying, grinding into powder, and carrying out high-temperature carbonization to obtain biochar; washing with diluted hydrochloric acid and drying to obtain activated carbon; mixing the metal-biochar-based hydrogenation catalyst with nickel nitrate, cerium nitrate and deionized water, then aging, drying and roasting in air, and finally reducing in hydrogen flow to obtain the metal-biochar-based hydrogenation catalyst. The biochar obtained by carbonizing the waste coffee grounds at a high temperature in a CO2 atmosphere has larger specific surface area and specific pore volume and extremely high mesoporous rate, so that the number of active sites of the catalyst is effectively increased, and the problem that the catalyst is easy to block and inactivate pore passages is solved; meanwhile, the yield of aromatic hydrocarbon after deoxidation and hydrogenation of a biomass pyrolysis product is increased, and the method is low in cost, safe, environmentally friendly and suitable for large-scale production.
Owner:JIANGSU UNIV

Ultra-low carbon steel coil plate for ultra-thin shell of oil filter and manufacturing method thereof

The invention discloses an ultra-low carbon steel coil plate for an ultra-thin shell of an oil filter and a manufacturing method thereof. The ultra-low carbon steel coil plate comprises the followingchemical components according to the weight percentage: 0.0028 to 0.0050% of C, less than or equal to 0.030% of Si, 0.45 to 0.55% of Mn, less than or equal to 0.012% of P, less than or equal to 0.008%of S, 0. 045-0.080% of Al, 0.065-0.085% of Ti, and less than or equal to 0.0030% of N. The manufacturing method comprises the following steps of: heating a plate blank, and carrying out rough rollingand finish rolling to obtain a hot rolled plate, wherein the coiling temperature is 590-630 DEG C; and carrying out cold rolling on the hot rolled plate to obtain the ultra-low carbon steel coil plate with the thickness of 0.30 to 0.44 mm, wherein the reduction ratio of cold rolling is 80 to 90%, the annealing temperature is 700 to 760 DEG C, the elongation of temper rolling is 1.0 to 2.0% , andthe elongation of straightening and withdrawal is 0.03 to 0.10%. The ultra-low carbon steel coil plate has the Rel of 220-270MPa, Rm of 330-390MPa, hardness of 54-60HR30T, and elongation A80 of greater than or equal to 40%. The ultra-low carbon steel coil plate has relatively high hardness, relatively good ductility, uniform structure property, good isotropic homogeneity and good deep-drawing property, does not generate earing, can completely replace the traditional 0.50-0.70mm thick material, and meets the requirements on thinning and weight reduction of automotive parts.
Owner:新余钢铁股份有限公司 +1

Super-hydrophilic chitosan quaternary ammonium salt hydrogel composite membrane as well as preparation method and application thereof

The invention discloses a super-hydrophilic chitosan quaternary ammonium salt hydrogel composite membrane and a preparation method and application thereof. The preparation method comprises the following steps of: adding chitosan quaternary ammonium salt powder into an acetic acid aqueous solution, and heating and stirring to obtain a transparent solution A; adding and dissolving a reinforcing agent acrylamide and a cross-linking agent into an acetic acid aqueous solution, then adding an initiator, and stirring until the initiator is completely dissolved to obtain a solution B; mixing the solution A and the solution B, and stirring well to obtain pre-gelled liquid with a room-temperature self-crosslinking function; and by taking an ultrafiltration membrane as a base membrane, transferring the pre-gelled liquid to the surface of the base membrane by adopting a surface multi-time coating method, and after cross-linking and curing at room temperature, putting the pre-gelled liquid into a blast oven for heat treatment to obtain the super-hydrophilic chitosan quaternary ammonium salt hydrogel composite membrane. The preparation method disclosed by the invention is simple. The surface of the obtained composite membrane is super-hydrophilic, the flux of the composite membrane is higher than that of a membrane prepared by a traditional single loading method, the anti-pollution performance is remarkably enhanced, and the composite membrane has a relatively high rejection rate on divalent cations.
Owner:OCEAN UNIV OF CHINA

A kind of preparation method of transparent superhydrophobic zinc oxide coating

The invention relates to a preparation method of a transparent super-hydrophobic zinc oxide coating on a glass substrate. The preparation method comprises the following steps of a, substrate pretreatment; b, zinc oxide solution preparation; c, zinc oxide coating preparation; and d, zinc oxide coating surface modification. Compared with the prior art, the preparation method has the beneficial effects of simple equipment process, low cost and mild reaction condition and is beneficial to large-scale industrial production. The transparent super-hydrophobic zinc oxide coating prepared by using the method has excellent hydrophobicity and transparency; the contact angle is larger than 160 degrees, the rolling angle is smaller than 8 degrees, and water drops can freely roll on the coating, so that the transparent super-hydrophobic zinc oxide coating has relatively good self-cleaning performance; and the light transmittance is approach to 90% which is close to that of blank glass, so that the transparent super-hydrophobic zinc oxide coating has favorable visible light transmittance. A surface modifier used in the preparation method is an alkyl silane coupling agent instead of a fluorinated compound, so that the cost is low, the environment pollution is relatively low, and the modified coating is relatively stable.
Owner:WUHAN INSTITUTE OF TECHNOLOGY

Preparation method of a double-layer composite self-assembled lubricating film

The invention provides a preparation method of a double-layer self-assembly lubricating film and relates to a preparation method of a novel double-layer self-assembly film formed by 1,2-Bis(triethoxysilyl)ethane and a low-surface-energy silane coupling agent. The method comprises the steps that single crystal silicon wafers are cut and cleaned and then are subjected to oxidation treatment; and the processed silicon wafers are immersed into 1,2-Bis(triethoxysilyl)ethane hydrolysate, and a first-layer film is prepared; and the obtained film is immersed into a low-surface-energy silane coupling agent solution again after being cleaned and dried, and deposition of a second-layer film is carried out through active groups on the surface of the first-layer film. Instruments and equipment involved in the preparation method are simple, operation is easy during the process, and the obtained double-layer films are of a stable and ordered structure. Compared with a single-layer film of the low-surface-energy silane coupling agent, the double-layer films can maintain a low friction coefficient, and the adhesion resistance and abrasion resistance of the double-layer self-assembly lubricating film can be effectively improved. The double-layer film is expected to become an effective means of solving the problems of lubrication and protection of the surfaces of devices in micro electro-mechanical systems.
Owner:CHINA UNIV OF MINING & TECH

A color-coated cold-rolled substrate for home appliance panels and its manufacturing method

ActiveCN104946978BHigh hardnessImprove dent resistanceMicrometerAging resistance
The invention discloses a color-coated cold-rolled baseplate used for a household appliance panel and a manufacturing method of the color-coated cold-rolled baseplate. The cold-rolled baseplate is manufactured by a plate blank consisting of the following ingredients by weight percentage: 0.0035-0.0065% of C, less than or equal to 0.009% of Si, 0.38-0.48% of Mn, 0.040-0.056% of P, less than or equal to 0.009% of S, 0.035-0.055% of Al, 0.045-0.055% of Ti, less than or equal to 0.0036% of N, and the balance being Fe. The method is characterized in that the plate blank is heated, and subjected to rough rolling and precision rolling to form a hot-rolled plate; a coiling temperature is 670-720 degrees; a hot-rolled coil is subjected to cold rolling; the temperature of a soaking zone of a continuous annealing furnace is 765-780 degrees; the elongation of temper rolling is 0.45-0.58%; the withdrawal and straightening elongation is 0.05-0.15%; the roughness of a working roll for the temper rolling is 1.3-1.7 micrometers; and a peak count (Pc) of the working roll for the temper rolling is greater than or equal to 120. With the adoption of the design ingredients and the manufacturing method, the color-coated cold-rolled baseplate with good deep drawability, low cost, ageing resistance and excellent dent resistance is obtained, and higher requirements of the household appliance panel are met.
Owner:XINYU IRON & STEEL CO LTD
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