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The bismuth-phosphate process was used to extract plutonium from irradiated uranium taken from nuclear reactors. It was developed during World War II by Stanley G. Thompson, a chemist working for the Manhattan Project at the University of California, Berkeley.
Method for cooperatively removing copper, arsenic, tellurium and lead from crude bismuth
The present application belongs to the technical field of non-ferrous metallurgy, and particularly relates to a method for cooperatively removing copper, arsenic, tellurium and lead in crude bismuth, which comprises the following steps: S1, obtaining molten bismuth liquid by melting, adding an oxidizing agent to the molten bismuth liquid, and performing a pre-oxidation reaction under stirring; S2, adding a composite removing agent and a fluxing agent to perform a reaction, and then removing surface dross; the composite removing agent comprises iron powder, bismuth phosphate and sodium sulfide; S3, adding the crude bismuth after step S2 to a vacuum rectification furnace, vacuum heat-insulating, and outputting refined bismuth. Through the cooperative design of pre-oxidation activation, in-situ sulfidation and phosphate slagging, the present application realizes the simultaneous and efficient removal of impurities such as Cu, As, Te and Pb, and the effective recovery of Ag. Subsequent vacuum distillation further removes residual lead in depth, and ensures that the refined bismuth product reaches a high standard.
Owner:SHANDONG HUMON SMELTING