The invention relates to a Fe-Co-S nanosheet material and a preparation method thereof and application. The preparation method comprises steps: S1, soluble cobalt salt, soluble iron salt, urea and ammonium fluoride are dissolved in water, thiourea is added after even stirring, and a hydrothermal reaction is conducted; and S2, after the hydrothermal reaction is finished, cooling, centrifuging, washing and drying are carried out to obtain the Fe-Co-S nanosheet material. Compared with the prior art, the Fe-Co-S nanosheet material is synthesized through one-step hydrothermal synthesis, the material has a porous nano structure with a high effective specific surface area, more electrochemical active sites and a rapid ion transport path can be provided, the preparation method of the material is simple and environmentally friendly, the synthesis time is greatly shortened, and large-scale production of Fe-Co-S nanosheet materials is facilitated.