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141 results about "Ktp laser" patented technology

Integrated laser-induced enhanced plasma spectrum acquisition system

The invention relates to an integrated laser-induced enhanced plasma spectrum acquisition system and belongs to the field of laser plasma spectrum detection. The integrated laser-induced enhanced plasma spectrum acquisition system comprises a pulse laser device, a light beam lifter, a spectrometer, a domain limiting loop, a high voltage discharge electrode, an ICCD (Intensified Charge Coupled Device) camera, a focusing lens, a sample chamber, a reflector, an adjustable optical fiber optical receiving system, a sample to be detected, a three-dimensional electric control translation platform, an imaging CCD (Charge Coupled Device), a gas flow meter and a gas pressure meter. According to the integrated laser-induced enhanced plasma spectrum acquisition system, different LIBS (Laser-induced Breakdown Spectroscopy) signals are collected by utilizing control and synchronous control of internal environments of smaller independent sealed spaces so that integration is realized; a high voltage discharge enhanced and loop limited domain synchronous enhanced LIBS system with the functions of spectrum acquisition, dynamic image analysis and the like is integrated; and more accurate measurement are realized by utilizing environment stress around the sample and control of protection gas; and the system is quick and convenient, and is favorable for industrial production and application.
Owner:刘瑞斌

Method for quantitatively detecting multiple heavy metals in leather at same time based on LIBS (Laser-Induced Breakdown Spectroscopy) technology

PendingCN105572103ARealize in-situ online detectionApplicable to on-site evidence collection tasksAnalysis by thermal excitationGratingCollection system
The invention discloses a method for quantitatively detecting multiple heavy metals in leather at the same time based on an LIBS (Laser-Induced Breakdown Spectroscopy) technology. The method adopts an LIBS detecting system which is formed by a Q-switched pulse Nd:YAG (Yttrium Aluminum Garnet) laser, an echelle grating spectrometer, an ICCD (Intensified Charge-Coupled Device) detector, a rotating platform and the like. The method comprises the following steps: firstly, regulating laser energy by an energy attenuation system consisting of a half-wave plate and a laser Glan prism, gathering the laser energy on the surface of a sample which is fixed to the rotating platform through a focusing lens, and ablating, gasifying and ionizing substances on the surface of the detected sample, thus forming laser plasma; secondly, obtaining a spectral signal of the laser plasma through a spectrum collection system, analyzing and converting element types corresponding to a spectral line, and obtaining content information of characteristic elements through conversion; thirdly, obtaining concentrations of heavy metal elements by combining a CF (Calibration-free)-LIBS method according to the obtained information of the elements.
Owner:TAIZHOU ENTRY EXIT INSPECTION & QUARANTINE BUREAU PEOPLES REPUBLIC OF CHINA +1

Spectroscopy-mass spectrometry combined quantitative analysis device for elements in unknown sample

The invention discloses a spectroscopy-mass spectrometry combined quantitative analysis device for elements in an unknown sample. The device uses a quantitative analysis structure and a method by using a laser-induced breakdown spectroscopy combining with a second level extraction field time-of-flight mass spectrometry (TOF). The quantitative analysis device with high detection sensitivity, real time, quickness, high accuracy, no contact, capability of simultaneously detecting multiple elements, and no need of pretreating the sample is realized. Due to dual-wavelength laser in the device, photofragments and molecular clusters are re-ionized conveniently, the mass spectrometry signal stability is improved, and a laser plasma emission spectroscopy signal is improved; due to a second level extraction field in the device, the TOF resolution ratio is improved conveniently and the signal is optimized conveniently; due to a spectroscopy collection system in the device, the capability of collecting plasma emission light to couple to optical fiber can be improved, an optical path can be folded, the integration and the miniaturization of an instrument are facilitated, and the commercialization of the instrument is realized conveniently.
Owner:DALIAN UNIV OF TECH

Passive electric detection device and method for laser plasma

The invention discloses a passive electric detection device and method for laser plasma. The device consists of two parallel sections and an arc section, wherein the two parallel sections are parallel to each other and connected through the arc section; the whole device is in an M shape; a cross section of the electric detection device is rectangular; a flow channel is formed inside the electric detection device and used for flowing and circulation of water; the two parallel sections are connected with water pipes respectively; and a lead is arranged on the electric detection device and used for performing electric signal detection on the laser plasma. During testing, a laser acting point is located in a concave part of the device, and a ceramic pad is arranged between a to-be-welded object and the M-shaped electric detection device to keep insulation and avoid short circuit; the electric detection lead is connected with a data acquisition card, the data acquisition card is connected with a computer, and data acquisition preparation work is ready; and then water is supplied for cooling. According to the electric detection method for the laser plasma, the stability and the reliability of a real-time electric detection process for the temperature of the laser plasma during laser welding are improved, and the method is easy to implement.
Owner:TIANJIN UNIV

Sequential diagnosis system used for nanosecond and picosecond laser beam combined targeting

The invention discloses a sequential diagnosis system used for nanosecond and picosecond laser beam combined targeting, and is used for sequential precision diagnosis in combined targeting by using nanosecond laser beams and picosecond laser beams simultaneously in a laser plasma experiment. The sequential diagnosis system comprises an imaging slit plate, a hard X-ray shielding body, a photocathode slit plate, a photocathode and a streak camera which are arranged in turn along a horizontal direction. In the experiment, soft X-rays generated by nanosecond laser beam targeting are imaged through the slit plate and then irradiated to the partial area of the photocathode; and hard X-rays generated by picosecond laser beam targeting directly penetrate through the slit plate (without imaging) and then irradiate all the area of the photocathode. Two types of X-rays of which the original light source positions are overlapped can be spatially separated on the images recorded by the streak camera so that diagnosis of the sequential relationship between the nanosecond laser beams and the picosecond laser beams can be realized. The sequential diagnosis system has ten picosecond level time discrimination and also has certain soft X-ray spatial discrimination so as to have wide application prospect.
Owner:LASER FUSION RES CENT CHINA ACAD OF ENG PHYSICS

Preparation method of spirofluorene acridine intermediate

The invention relates to a preparation method of a spirofluorene acridine intermediate, relating to the fine organic synthesis field and the photoelectric material application field. The spirofluorene acridine material with the structure shown as below is used as an important organic intermediate in the new fields such as the organic electroluminescence, the photovoltaic cell, the organic electrical storage, the organic nonlinear optics and the organic laser. The invention relates to a novel preparation method of spirofluorene acridine monomer, in particular to a two-step tandem reaction adopting the one pot method. The preparation method comprises the following steps: heating arylamine, arylamine hydrochloride and fluorenone or a derivative of fluorenone to fully react and generate open-loop 9,9'-diaryl intermediate product; and (2) adding polyphosphoric acid and arylamine in the reaction tank to close the loop, alkalifying, stirring, filtering, and washing to obtain the high purity product. The preparation method of the spirofluorene acridine intermediate has the following characteristics: (1) the one pot method is adopted for the tandem preparation process, the middle separation step is not required, the raw materials are cheap and accessible, the yield is high, the product is easy to separate and purify; and (2) the method has mass production value and is environmental friendly.
Owner:NANJING FANGYUAN GLOBAL DISPLAY TECH

3D printing method and device based on pulse current

The invention provides a 3D printing method based on pulse current. The method comprises the following steps of using an amorphous alloy wire or a strip as a raw material, carrying out spot pressing on the amorphous alloy wire or the strip, welding by the pulse current, and stacking layer by layer to form a three-dimensional sample piece. According to the method, the pulse current is used as a heat source for amorphous alloy space additive manufacturing, on one hand, power consumption needed in the manufacturing process is far smaller than that of electron beams, lasers and other traditional heat sources, the energy utilization rate is increased, low-power-consumption additive manufacturing is achieved, on the other hand, the pulse current is used for rapid heating, so that an amorphous alloy is in a non-molten state with low viscosity, the problems that a molten pool is difficult to control under microgravity and heat dissipation and solidification are difficult and the like in a high-vacuum environment in a traditional 3D printing method of metal materials can be solved, and the stability of the space additive manufacturing process can be improved. Besides, point pressure rapid welding and layer-by-layer additive manufacturing are conducted on the amorphous alloy through the pulse current, the thermal action time in the additive manufacturing process is accurate and controllable, the amorphous structure of the raw materials can be kept, and the mechanical property of an additive sample piece is improved.
Owner:CHINA ACADEMY OF SPACE TECHNOLOGY

Metal edge wrapper for aircraft engine fan blade, machining tool and machining method

The invention discloses a metal edge wrapper for an aircraft engine fan blade, a machining tool and a machining method and belongs to the aircraft component manufacturing technology. The metal edge wrapper comprises side plates and a nose wing. The machining tool comprises a pressure part, an inner strutting piece, side pressing plates, end clamping plates, a built-in fixing part and an external pull fixed base. The pressure part and the side pressing plates are in pivot connection through four-link pressing and locating assemblies. The machining method comprises the steps of preparing the tool, clamping the metal edge wrapper, welding the metal edge wrapper, conducting distressing heat treatment and removing the tool to complete machining. The machining method is adopted for conducting welding on the metal edge wrapper clamped and located by the tool and can adapt to multi-curvature complicated 3D-shape metal edge wrappers. The clamped metal edge wrapper is leveled first. Implementation of the machining method is not limited to the welding manners such as electron beams, CMT or laser. The welded metal edge wrapper can be subjected to heat treatment along with the machining tool. The shaping effect is ensured. Through the machining method, the machining cost of the metal edge wrapper can be remarkably reduced, and the efficiency can be improved.
Owner:上海两擎机电科技合伙企业(有限合伙)

Perovskite single crystal nanoring and preparation method and application thereof

The invention discloses a perovskite single crystal nanoring and a preparation method and application thereof. The perovskite single crystal nanoring has an annular morphology and a single crystal structure, is an independent and continuous nanoring, is regular in morphology, has no visible surface defect structures such as grain boundaries and pores, and has good crystal quality. A two-dimensional confinement space is formed by a substrate, a metastable solution formed by the perovskite precursor solution and a polar organic solvent grows in the two-dimensional confinement space to form a single-crystal nanoring structure, the perovskite single-crystal nanoring is prepared through the two-dimensional confinement space of the substrate and solvent regulation and control engineering, and compared with other methods, the invention is small in energy consumption, low in cost and suitable for industrial production. The invention is low in cost, simple in process, clear in product, single in product configuration and suitable for large-scale production; the perovskite single crystal nanoring disclosed by the invention is of a single crystal structure, has the advantages of higher crystal quality, no crystal boundary and small defect density, and has huge potential application value in the fields of laser and the like.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Laser plasma extreme ultraviolet light source and extreme ultraviolet light generating method

The invention relates to a laser plasma extreme ultraviolet light source and an extreme ultraviolet light generation method. The laser plasma extreme ultraviolet light source comprises a vacuum targetchamber, an optical lens module, a droplet target generator and a collecting mirror for collecting extreme ultraviolet light, wherein an optical focus formed by the laser through the optical lens module is located in the vacuum target chamber; the droplet target generator is used for providing droplets for the vacuum target chamber; the moving line of the liquid drop in the vacuum target chamberpasses through the optical focus, and the liquid drop generated by the liquid drop target generator and the laser generate extreme ultraviolet light at the optical focus; the collecting direction of the collecting mirror is perpendicular to the laser incident direction and is not parallel to the moving direction of the liquid drops. The focus of the optical lens module is in a vacuum environment,and therefore damage to other equipment is prevented. Meanwhile, the collection direction of the collector is perpendicular to the laser incident direction, and no hole needs to be formed in the middle of the collection mirror, so that more light can be collected, the collection efficiency is improved, and the conversion efficiency of the light source is further improved.
Owner:GUANGDONG INTELLIGENT ROBOTICS INST

Preparation device and preparation method for titanium alloy composite material

The invention discloses a preparation device and preparation method for a titanium alloy composite material. The preparation device comprises a gun body. A laser beam channel, a first plasma generating electrode, a second plasma generating electrode, a first wire guide nozzle and a second wire guide nozzle are arranged on a nozzle of the gun body. A laser beam transmitted by the laser beam channelis located on the central axis of the laser beam channel. The first plasma generating electrode, the second plasma generating electrode, the first wire guide nozzle and the second wire guide nozzle are sequentially and evenly distributed on the periphery of the laser beam channel, and an included angle is formed between the central axis of the laser beam channel and each of the first plasma generating electrode, the second plasma generating electrode, the first wire guide nozzle and the second wire guide nozzle. A laser-plasma composite heat source is used for fusing and depositing a wire, the energy of the composite heat source is concentrated, the heat input in the deposition process is small, composite material grains are refined, few defects exist, the forming precision is high, and the preparation device is simple in structure, easy to implement, high in deposition efficiency and suitable for preparation of large-size composite materials with various properties.
Owner:SOUTH CHINA UNIV OF TECH +1
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