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149results about How to "Avoid flushing" patented technology

Preparation method for alpha-acetyl-gamma-butyrolactone

In order to solve the problems of a low safety factor, low yield, high cost, environmental pollution and the like existing in the prior art, the invention provides a preparation method for alpha-acetyl-gamma-butyrolactone. In the method, gamma-butyrolactone and methyl acetate are used as reaction raw materials and metallic sodium is used as a catalyst; the final product is prepared through the phases of reaction, separation, neutralization and extraction. According to the invention, methyl acetate is used as the reaction raw material and a reaction solvent, which on one hand enables production cost to be reduced, the reaction rate to be slowed and dashing out of reacting materials to be avoided, and on the other hand avoids environmental pollution and affection on product quality caused by utilization of benzene solvents; preparation of the catalyst into sodium sand can improve reaction efficiency; high purity alpha-acetyl-gamma-butyrolactone can be obtained through neutralization andextraction of the solid resultants alpha-acetyl-gamma-butyrolactone sodium salt of the reaction which have been subjected to solid-liquid separation without underpressure distillation, thereby effectively improving production efficiency and reducing production cost; the acidic neutral solution used in the invention can be used repeatedly, thereby avoiding environmental pollution by the solution.
Owner:山西三维华邦集团有限公司 +1

Device for continuous preparation of Grignard reagent and method for continuous preparation of Grignard reagent through using device

ActiveCN102603775ANot prone to valve cloggingLess prone to plumbing problemsMagnesium organic compoundsEnvironmental resistanceVapor–liquid separator
The invention discloses a device for the continuous preparation of a Grignard reagent and a method for the continuous preparation of the Grignard reagent through using the device. The device comprises a solvent storage container, a solvent-raw material mixing container, a raw gas storage container, a preheater, a reactor, a magnesium adding bin, a gas-liquid separator, a Grignard reagent reception container and a tail gas recovery apparatus, wherein the reactor adopts a three-phase bubble slurry column reactor. A purpose of the continuous preparation of the Grignard reagent can be realized through using the device of the invention, and initiation and heat radiation problems of a Grignard reaction can be effectively solved through adopting the three-phase bubble slurry column reactor, so potential safety hazards of material rush-out, explosion and the like caused by the severe temperature rise of the Grignard reaction can be effectively avoided, the obstruction of valves and pipelines by magnesium shreds can be prevented, and the high purity Grignard reagent can be obtained; and the tail gas recovery apparatus is arranged in the invention to absorb and recycle tail gases, so the cost is saved, and the environmental pollution is reduced, thereby cleaning and environmental protection requirements of the preparation of the Grignard reagent are realized.
Owner:SHANGHAI HEGNO PHARMA HLDG +1

Amphibole type primary iron ore grading process

The invention relates to an amphibole type primary iron ore grading process. The amphibole type primary iron ore grading process comprises the steps that iron ore with iron mineral disseminated grainsize being P80=17 microns is subject to rough breaking and primary dry in-advance magnetic separation, primary dry in-advance magnetic separation concentrate with the grade being 28.62%, the recoveryrate being 98.51% and the particle size being P80=150 microns serves as raw materials; the process is characterized in that raw ore is subject to semi-automatic-grinding screening closed loop grinding, wet in-advance magnetic separation, two-stage stage grinding stage low intensity magnetic separation, one-roughing one-refined three-scavenging reverse flotation, three-stage closed loop superfine ore grinding and strong magnetic separation process grading, wherein the semi-automatic-grinding screening closed loop grinding product granularity is 0 mm-3 mm, the two-stage closed loop grinding product granularity is P80=30 microns, the three-stage closed loop grinding product granularity is P80=17 microns, and the good indexes with the final iron ore concentrate iron grade being 65.50%, the recovering rate being 76.00%, the comprehensive gangue iron grade being 11.30% and the recovery rate being 24.00% are finally obtained.
Owner:MCC NORTH (DALIAN) ENG TECH CO LTD

Quick ball joint

Disclosed is a quick ball joint which comprises a ball shell connected with a pipeline and a ball body connected with another pipeline. The ball body is spherical, the inner wall of the ball shell is also a spherical shape for being engaged with the ball body, the inner wall is provided with a sealing ring positioned on the inner side of a vertex of the ball body; the front end of the ball shell is connected with a pressure cover, the inner surface of the pressure cover is an arc-shaped surface, radian of the arc-shaped surface is same with that of the surface of the ball body. As the sealing ring is not positioned at the highest point of a spherical center but at a position deviating 5-7mm from the spherical center, tightness of the ball joint is not very effective when in the absence of an external pull force; the highest point of the ball body extrudes the sealing ring when stretched by an external force, thereby pressing the sealing ring tightly and being capable of bearing relatively high pressure and simultaneously bearing large enough pull force. When in installation, people only need to insert a ball body end into the ball shell, rotate the pressure cover to lead a flange portion of the pressure cover to be screwed at a fastening position of the ball shell, and then plug a pin shaft to prevent the pressure cover from rotating, thereby finishing installation. Accordingly, the ball joint achieves simple and convenient installation.
Owner:WUXI JINYANG PIPING FITTING

Feeder device of dissolving furnace for glass fiber production

The invention discloses a feeder device of a dissolving furnace for glass fiber production. The feeder device comprises a rack and a stock bin arranged on the rack. A discharging pipe is arranged at the lower end of the stock bin. A transmission device driving feeding is arranged at one side of the rack. The transmission device comprises a transmission shaft and a driving mechanism driving rotation of the transmission shaft. A helix tube is arranged at the inner side of the stock bin. The helix tube extends into the discharging pipe. The transmission shaft is connected with the helix tube, and drives rotation of the transmission shaft through the driving mechanism. Materials are rotated and discharged together with the helix tube under the normal thrust of the helix tube. Smooth transportation of materials is ensured, material clashing phenomenon is avoided, dust-free transportation is achieved and safe production is ensured. A detection device for detection of material level is arranged on the inner wall of the stock bin. Through arrangement of the detection device, real-time detection of the change of the material level in the stock bin can be achieved and the feeding amount of materials can be determined. The feeder is advantaged by simple structure, easy maintenance and low usage and maintenance cost.
Owner:TAIJIA GLASS FIBER

Special plasticizer TM8 for automobile interior parts

The invention discloses a special plasticizer TM8 for automobile interior parts. Raw materials and auxiliary materials of the plasticizer TM8 comprise acid anhydride, alcohol, a catalyst, sodium carbonate and a filter aid. A process of the special plasticizer TM8 for the automobile interior parts comprises esterification, purification and filter press purification, and molecular distillation (short-path distillation). In esterification, alcohol is added first, after the temperature of a reactor is less than 80DEG C, 1,2,4-benzeneticarboxylic anhydride is added, then the catalyst is added, whenthe temperature of the material rises to 220DEG C, a negative pressure reaction starts, when an acid value is less than or equal to 0.1mgKOH / g, flash evaporation and dealcoholization start. In purification, steam stripping is performed while temperature rises to 215+ / -10DEG C, and the filter aid diatomite is added so as to purify and stir. In molecular distillation, the vacuum degree reaches lessthan 100pa, and the material inlet temperature is maintained at 215+ / -5DEG C. The raw materials are easy to obtain, the process is advanced, the equipment is simple, the plasticizer is environmentally friendly, has high plasticizing efficiency, resists high and low temperature, has low volatility, has small odor, and is highly stable.
Owner:JIANGSU SENHE CHEM TECH CO LTD

Micro-miniature under-pressure pluggable fluid connector

The invention provides a micro-miniature under-pressure pluggable fluid connector. The micro-miniature under-pressure pluggable fluid connector comprises a plug and a socket. The plug comprises a plugshell and a sealing assembly. The sealing assembly comprises a sleeve and a sealing block. A locating sleeve is arranged at the rear end of the plug shell. The locating sleeve abuts against the sleeve through a first spring. The inner wall of the front end of the plug shell is provided with a first limiting part. A first seal ring is arranged between the sealing block and the plug shell. The socket comprises a socket shell and a sealing rod assembled in the socket shell. The sealing rod is sleeved with a second spring and a sealing ring. The front end of the second spring abuts against the sealing ring, and the rear end of the second spring abuts against the sealing rod. The inner wall of the front end of the socket shell is provided with a second limiting part. The inner side of the sealing ring and the sealing rod form sealing through a second seal ring. The front end of the sealing rod is provided with a plurality of through holes. During operation of the micro-miniature under-pressure pluggable fluid connector, no any seal ring is exposed in fluid, so that the seal rings are prevented from being washed away; and moreover, through the special sealing assembly, the stability ofthe connector is improved, the flow resistance of fluid is reduced, and the fluid flux is increased.
Owner:CHINA AVIATION OPTICAL-ELECTRICAL TECH CO LTD

Packaging bag forming machine

The invention discloses a packaging bag forming machine. The packaging bag forming machine includes a rack, a feeding mechanism, a bag forming machine, a film pulling mechanism, a back sealing mechanism, a horizontal sealing mechanism and a buffer mechanism, wherein the feeding mechanism is arranged on the rack for precise releasing and conveying of packaging films, the bag forming machine folds the packaging films into a cylinder shape and fills goods, the film pulling mechanism is located at one side of the bag forming machine for pulling the packaging films folded into the cylinder shape forward, the back sealing mechanism is located at one side of the bag forming machine to seal the side edge of the cylindrical packaging films, the horizontal sealing mechanism is located on the lower part of the bag forming machine to seal the upper and lower ends of the cylindrical packaging films and cut the cylindrical packaging films into separate packaging bags, and the buffer mechanism is located between the bag forming machine and the horizontal sealing mechanism and can be clamped on the packaging films for packing buffer after horizontal sealing. According to the packaging bag formingmachine, the to-be-packaged goods can be automatically packaged into the package bags, the degree of automation is high, the manpower is saved, the goods after packaging is neat and attractive, the amount of the filled goods is accurate, and the filled goods is not prone to being spilled.
Owner:昆山迈格金相机械设备有限公司

Evaporator with heat exchange assembly convenient to clean

The invention discloses an evaporator with a heat exchange assembly convenient to clean. The evaporator comprises straight pipes, elbow pipes, cleaning circular rings, horizontal rods and short brushes. The straight pipes and the elbow pipes can be disassembled. The two end faces of each elbow pipe are fixedly provided with rubber protrusions clamped to annular clamping grooves formed in the endsof the corresponding straight pipes. One elbow pipe and two straight pipes are integrally assembled to form a U-shaped structure. The horizontal rods penetrate through the straight pipes. The horizontal rods are sleeved with the cleaning circular rings. The outer edges of the cleaning circular rings are uniformly provided with the short brushes. In the evaporator provided by the invention, the straight pipes and the elbow pipes are detachably connected. When the elbow pipes are dismantled from the straight pipes, the inner walls of the elbow pipes are made to slide over the surfaces of long brushes, and the inner walls of the elbow pipes can be cleaned; the horizontal rods are made to move back and forth by pulling a flexible steel wire back and forth, so that the cleaning circular rings fixedly connected to the horizontal rods move back and forth on the inner walls of the straight pipes, and at the moment, the short brushes located on the edges of the cleaning circular rings can cleanthe inner walls of the straight pipes. The evaporator is convenient to use.
Owner:江苏世林博尔制冷设备有限公司

Industrial production method of o-nitrobenzenesulfonyl chloride

The invention discloses an industrial production method of o-nitrobenzenesulfonyl chloride. The method comprises the following steps that o-nitrochlorobenzene and sodium methyl mercaptide are subjected to an etherification reaction, filtering is conducted, an obtained filter cake is subjected to recrystallization, and through centrifugation separation and drying, a dry product of o-nitrobenzene dimethyl sulfide is obtained; the dry product of o-nitrobenzene dimethyl sulfide is subjected to a chlorination reaction in batches to obtain a wet crude product, an appropriate amount of hydrochloric acid is added in a chlorination reaction system, the chlorination reaction is carried out in a hydrophilic organic acid solvent, and the mole ratio of the o-nitrobenzene dimethyl sulfide to water during the chlorination reaction is 1:(5-15); a finished product of o-nitrobenzenesulfonyl chloride is obtained through refining and drying. Through HPLC detection, the content of the o-nitrobenzenesulfonyl chloride synthesized by means of the method is 98-98.5%; the yield is 0.72-0.75, the acquisition rate is 0.97 or above, the turbidity (ppm) is 1.5-2, and the melting point is 66-67 DEG C. By adopting the hydrophilic organic acid solvent, the problems about large-scale production discharging, yield and quality are solved, and meanwhile the purposes of mixed application and post-treatment separation of large-scale production water-soluble solvents are achieved.
Owner:苏州市泽宸贸易有限公司

Efficient reaction equipment for rectification

The invention discloses efficient reaction equipment for rectification. The equipment mainly comprises an outer frame, a motor, a steam pipe, a condensation shell, a water passing head, a middle shell, a liquid outlet pipe, a layering shell, a densimeter, an electromagnetic liquid level meter, a metering pump, a middle rod, a pneumatic frame and a condensation pipe,the middle part of the outer frame is fixedly provided with a sealing sleeve, the inner wall of the sealing sleeve is fixedly provided with a wear-resisting sleeve, a middle rod is rotationally installed on the inner side of the wear-resisting sleeve, an air supply cavity is formed in the middle of the middle rod, a speed reducer is fixedly installed in the middle of the top end of the outer frame and fixedly connected with thetop end of the middle rod, and a motor is fixedly installed at the top end of the speed reducer. The equipment is reasonable in structural design, the Luneng efficiency is improved through a built-inefficient Luneng structure, the discharging purity and downstream stability are improved through detachable filtering equipment and an equipartition structure, and material flushing caused by floodingis prevented; and with simple electronic equipment, controllable liquid level control can be achieved, the purity of discharged liquid is guaranteed, and the reaction equipment is provided with a flexibly-changed stirring and scraping structure and is high in practicability.
Owner:苏州市浒墅关化工添加剂有限公司

Dyeing and finishing method of full-color modal polyester peach skin yarn-dyed fabric and fabric

ActiveCN110592970AChicken paw prints noChafing problem noShrinkingDry-cleaning apparatus for textilesFiberYarn
The invention provides a dyeing and finishing method of a full-color modal polyester peach skin yarn-dyed fabric and the fabric. The method includes the steps of unwinding, preprocessing, dyeing, postprocessing, rewinding, warping, slashing, weaving and after-finishing; the after-finishing process includes the steps of zero-shrinkage-rate pre-shrinkage, singeing, desizing, water sanding, air washing+enzyme washing, sizing and pre-shrinkage. The method has the advantages that the green cutting problem between modal fiber under the low cohesive force is avoided; treatment is conducted through ascouring agent in the preprocessing step, grease on the modal fiber surface is sufficiently removed, and the dyeing uniformity is improved; dyes excellent in compatibility and high in color light reproducibility are selected in the dyeing step, the dyes, anhydrous sodium sulphate and sodium carbonate are added at a low temperature, and the problem is solved that modal is quite to color and prone to dyeing defects; the shrinkage rate is 0% in the zero-shrinkage-rate pre-shrinkage step, the fabric is ironed, and dead creases are avoided; by means of the fabric sanding process of water sanding and air washing+enzyme washing, the fabric is endowed with the polyester peach skin effect.
Owner:张家港市金陵纺织有限公司

Pressure swing adsorption oxygen production device for producing high-purity oxygen by using two-stage PSA (Pressure Swing Adsorption)

The invention discloses a pressure swing adsorption oxygen production device for producing high-purity oxygen by using two-stage PSA (Pressure Swing Adsorption). Comprising an air compressor, an air buffer tank connected to the air outlet end of the air compressor through a connecting pipe, a freeze dryer communicated with the air buffer tank through a connecting pipe, a filter set connected to the inner wall of one side of the freeze dryer in a sleeving mode, an oxygen generation main machine connected to one end of the filter set in a sleeving mode and an oxygen buffer tank connected to the air outlet end of the oxygen generation main machine in a sleeving mode. Sliding grooves are formed in the inner walls of the two sides of the air buffer tank, sliding blocks are slidably mounted in the sliding grooves, mounting pipes are welded to the outer walls of the opposite sides of the two sliding blocks, the inner walls of the bottom ends of the mounting pipes are sleeved with filter elements, and partition plates are welded to the outer walls of the top ends of the mounting pipes. The spring buffers impact force borne by the filter element, the filter element can be prevented from being burst open or damaged, the service life of the filter element is prolonged, compressed air can smoothly enter the air outlet pipe while buffering is conducted, and the working efficiency is improved.
Owner:苏州希特高纯气体设备有限公司
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