The invention relates to the technical field of organic
silicon resin preparation, in particular to trapezoidal methyl
silicon resin and a preparation method thereof.The trapezoidal methyl
silicon resin is prepared by taking methyl
trichlorosilane as a main
raw material, introducing a trapezoidal control agent containing amido and alkoxy at the same time to inhibit the reaction activity of the methyl
trichlorosilane and then carrying out
hydrolysis reaction in a small amount of
alcohol solvent and water; the generation of a cross-linked
network structure insoluble substance during
hydrolysis is avoided, and the resin gelation risk is effectively reduced. The
hydrolysis rate is reduced, so that the use amount of the
solvent is reduced, the proportion of
alcohol in the water phase is greatly reduced, and the process and
environmental protection cost is reduced. The trapezoidal
methyl silicone resin prepared by the method is excellent in
viscosity performance, high in yield, excellent in boiling resistance, short in
curing time, high in resin
softening point and short in gelation time.