The invention belongs to the technical field of chemical preparations, and particularly relates to a preparation method for electronic-grade
triglycidyl isocyanurate. The method specifically comprisesthe following steps: uniformly mixing
cyanuric acid,
epoxy chloropropane, organic strong base and water, reacting for 1.5 h at 75-80 DEG C; heat-insulating for 1 h at 100 DEG C; in vacuum, 35-40 DEGC, adding
sodium hydroxide; vacuum-unloading, removing a
solid phase, adding clear water to
mother liquor, stewing and removing superstratum
saline water; in vacuum, 60-70 DEG C, evaporating a part ofepoxy chloropropane from the substratum
mother liquor; placing a distilled material in a
crystallization kettle, stirring, at 8-10 DEG C, and removing a
liquid phase; decompressing the
solid phase, and
microwave-
drying, to obtain a final product. The catalyst is the organic strong base which does not contain
halogen, and the final product has not a
halide ion residue. A cyclization process is alkalified in vacuum, so
epoxy chloropropane
hydrolysis caused by
alkaline water and a by-product produced by TGIC cycle opening are avoided. The technical scheme of the preparation method is used, so the product quality is apparently improved, the product cost and the
energy consumption are greatly reduced, and the environment is friendly.