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188 results about "Phosphate anion" patented technology

The phosphate anion is actually a polyatomic ion made up of one phosphorus atom and four oxygen atoms. The chemical formula of the anion is "PO"_4^(3-). Now, are always neutral. This means that you must balance the 3- charge on the anion by using three potassium cations.

Preparation method of grapheme/hydroxyapatite composite material

A preparation method of a grapheme/hydroxyapatite composite material comprises the following steps: uniformly mixing oxidized grapheme with the concentration of 0.5-5 mg/ml and a solution or a turbid liquid with the calcium ion concentration of 0.01-3.0 mol/L to obtain a first mixed solution; adding a solution I with the phosphate anion concentration of 0.01-2.0 mol/L to the first mixed solution according to the molar ratio of calcium to phosphorus is (1.5-2.0) to 1, and uniformly mixing the solution I and the first mixed solution under the action of magnetic mixing; adjusting the pH to be 8-14 through a pH adjusting agent to obtain a second mixed solution; transferring the second mixed solution to a reaction kettle; carrying out hydro-thermal treatment for 1-12 hours at the temperature of 160-240 DEG C; cooling the second mixed solution until the temperature of the second mixed solution is the room temperature; cleaning, freezing and drying to obtain the grapheme/hydroxyapatite composite material. The preparation method is environment-friendly, simple and beneficial to large-scale production. The prepared grapheme/hydroxyapatite composite material has the advantages of good mechanical property as well as high electrical conductivity, adsorbability, biocompatibility and osteogenic activity.
Owner:SOUTHWEST JIAOTONG UNIV

Method for preparing antibacterial active titanium oxide nanotube array composite coating material

The invention discloses a method for preparing an antibacterial active titanium oxide nanotube array composite coating material. The method comprises the following steps of: performing electrolytic oxidation to prepare a titanium oxide nanotube array with biological activity by taking titanium and an alloy thereof as an anode, taking an electrolyte solution containing phosphate anion and fluorinion as electrolyte; soaking the titanium oxide nanotube array with biological activity in the solution of silver nitrate and polyethylene glycol which are taken as a soaking solution, taking the titanium oxide nanotube array out, inducing the light in the active titanium oxide nanotube array to deposit silver particles through UV-irradiation, and obtaining the titanium oxide nanotube array composite coating material with the antibacterial property and biological activity. According to the material prepared by the method, the silver particles enter the titanium alloy or a titanium alloy matrix, and the material has long-term antibacterial stability; the thickness of the active titanium oxide nanotube array can be controlled in a range from 100 to 1000nm, and bone cell growth and nutrition transfer are promoted; the active titanium oxide generated through anodic oxidation can prevent release of titanium ion in the matrix, and the corrosion resistance of the matrix is improved; and moreover, the coating material has obvious biological activity and can induce bone apatite formation.
Owner:INNER MONGOLIA METAL MATERIAL RES INST

Chitosan and chitosan quaternary ammonium salt composite magnetic microsphere and preparation method thereof

The invention discloses a chitosan and chitosan quaternary ammonium salt composite magnetic microsphere and a preparation method thereof. The method comprises the steps of preparing a water phase, stirring and dissolving chitosan, chitosan quaternary ammonium salt and a pore-foaming agent PEG or PVP according to a ratio in an acetic acid aqueous solution, and adding magnetic particles for stirring and ultrasonic treatment; preparing an oil phase, and stirring liquid paraffin and Span80 to obtain the oil phase; gradually adding the water phase into the oil phase drop by drop while stirring is carried out to obtain a liquid mixture; adding a sodium polyphosphate aqueous solution into the liquid mixture drop by drop, carrying out stirring, and adding a glutaraldehyde aqueous solution for reaction; carrying out centrifugation and washing to obtain the chitosan and chitosan quaternary ammonium salt composite magnetic microsphere. The composite magnetic microsphere disclosed by the invention is higher in adsorption to electronegative materials such as humic acid, anionic dyes, arsenate ions, phosphate anions and nitrate ions, is higher in pH adaptability, magnetic separation property and regeneration performance, and is high in exchange capacity, high in adsorption speed and easy to separate.
Owner:TIANJIN POLYTECHNIC UNIV

Titanium dioxide/strontium and fluorine-containing hydroxyapatite bioactive nano-composite coating as well as preparation method and application thereof

The invention provides a titanium dioxide / strontium and fluorine-containing hydroxyapatite bioactive nano-composite coating as well as a preparation method and an application thereof. The method comprises the following steps: firstly preparing an electrolyte containing calcium ions, strontium ions, fluorine ions and phosphate anions; and then by taking titanium or a titanium alloy as an anode and stainless steel as a cathode, directly preparing the titanium dioxide / strontium and fluorine-containing hydroxyapatite bioactive nano-composite coating on the surface of a titanium or titanium alloy substrate by virtue of a micro-arc oxidation technology. The coating consists of an inner layer combined on the surface of the substrate and a surface layer combined on the surface of the inner layer, wherein the inner layer is a titanium dioxide layer in a form of a nano crystal and the surface layer is a nano-particle strontium and fluorine-containing hydroxyapatite layer. No non-continuous interfaces are available between the coating and the substrate and the coating has high combining strength and structural stable performance; the coating is relatively small in solubility in a simulated body fluid, so that the coating is effectively implanted and used; and the nano-particle strontium and fluorine-containing hydroxyapatite layer in the surface layer can remarkably promote the osteogenic function of the cells to form new bones and inhibit bacterial adhesion and growth.
Owner:宝鸡卡斯特医疗科技有限公司

Combined fertilizer synergist containing polyglutamic acid, phosphate solubilizing bacteria and potassium bacteria and preparation method and application of combined fertilizer synergist

ActiveCN104276882AStrong ability to decompose inorganic phosphorusImprove bioavailabilityFertilizer mixturesPhosphate ionPhosphate solubilizing bacteria
The invention discloses a combined fertilizer synergist containing polyglutamic acid, phosphate solubilizing bacteria and potassium bacteria. The combined fertilizer synergist comprises the following components in proportion: phosphate solubilizing bacteria, potassium bacteria and polyglutamic acid at the mass ratio of (0.1-1) to (0.1-1) to (0.001-0.1). The invention also discloses a preparation method and application of the fertilizer synergist. The phosphate solubilizing bacteria disclosed by the invention are capable of effectively releasing phosphate anions (PO4<3+>) in soil or fertilizer; the potassium bacteria are capable of effectively releasing potassium ions (K<+>) in the soil or fertilizer; after being compounded with the phosphate solubilizing bacteria and the potassium bacteria, the polyglutamic acid not only can provide a good growth environment for survival of the phosphate solubilizing bacteria and the potassium bacteria, but also can fully chelate nutrient elements released by the phosphate solubilizing bacteria and the potassium bacteria; and due to the synergistic effect, the effect of solubilizing phosphate and potassium is relatively outstanding, therefore the combined fertilizer synergist can be cooperatively used together with fertilizers, the utilization rate of the fertilizer is increased, and the combined fertilizer synergist can also be directly fertilized as a bacterial manure.
Owner:轩凯生物科技(滁州)有限公司

Process for preparing graphite according to electrochemical method

The invention discloses a process for preparing graphite according to an electrochemical method. The process comprises the following steps: firstly, mixing lewis acid with protonic acid to obtain electrolyte; secondly, taking graphite paper as an anode, and completely immersing the graphite paper into the electrolyte for intercalating to obtain intercalated graphite paper with expanded volume; thirdly, using the intercalated graphite paper as an anode, immersing the intercalated graphite paper into a solution containing sulfate ions or phosphate anions, and applying voltage to enable the intercalated graphite paper to continuously expand, wherein the intercalated graphite paper gradually falls off to form expanded graphite paste; fourthly, repeatedly washing the graphite paste by using pure water, filtering, then uniformly mixing the graphite paste with the pure water to obtain dilute paste, and sequentially carrying out ultrasonic exfoliation, filtering and drying on the dilute paste to obtain graphene powder. According to the process disclosed by the invention, the problem that a strong acid, a strong oxidant or an expensive poisonous organic solvent is adopted for preparing graphene according to an existing electrochemical method is solved, a preparation process of the graphene is also simplified, and the preparation cost is reduced.
Owner:DEYANG CARBONENE TECH

Synthesis of cathode active materials

The present invention relates to a method for preparing a lithium vanadium phosphate material comprising forming a aqueous slurry (in which some of the components are at least partially dissolved) comprising a polymeric material, an acidic phosphate anion source, a lithium compound, V2O5 and a source of carbon; wet blending said slurry, spray drying said slurry to form a precursor composition; and heating said precursor composition to produce a lithium vanadium phosphate. In one embodiment the present invention relates to a method for preparing a lithium vanadium phosphate which comprises reacting vanadium pentoxide (V2O5) with phosphoric acid (H3PO4) to form a partially dissolved slurry; then mixing with an aqueous solution containing lithium hydroxide; adding a polymeric material and a source of carbon to form a slurry; wet blending said slurry; spray drying said slurry to form a precursor composition; and heating said precursor composition for a time and at a temperature sufficient to produce a lithium vanadium phosphate compound. In an alternative embodiment the present invention relates to a method for preparing a lithium vanadium phosphate which comprises preparing an aqueous solution of lithium hydroxide; partially dissolving vanadium pentoxide in said aqueous solution; adding phosphoric acid to the aqueous solution; adding a polymeric material and a source of carbon to the solution containing vanadium pentoxide to form a slurry; spray drying said slurry to form a precursor composition; and heating said precursor composition for a time and at a temperature sufficient to form a lithium vanadium phosphate. The electrochemically active lithium vanadium phosphate so produced is useful in making electrodes and batteries.
Owner:VALENCE TECH INC

Method of reducing staining of stannous in dentifrice compositions

Disclosed are methods for reducing the staining of dentifrice composition containing stannous comprising administering to a subject the dentifrice composition. The dentifrice composition is a dual phase dentifrice and is contained in physically separated compartments of a dentifrice dispenser. The first dentifrice composition comprises an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and has a total water content of up to about 20%. The second dentifrice composition comprises an effective amount of stannous ions. The molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1 and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate. The dentifrice composition may alternatively be a single phase dentifrice. The single phase dentifrice will comprise an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and an effective amount of a stannous ion. The single phase dentifrice has a total water content of up to about 20%, the stannous ion is not delivered from stannous fluoride, a molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1, and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate.
Owner:THE PROCTER & GAMBLE COMPANY

Preparation method for directly generating hydroxyapatite-containing biological ceramic membrane on surface of titanium

The invention discloses a preparation method for directly generating a hydroxyapatite-containing biological ceramic membrane on the surface of titanium, and aims to solve the practical problems that the prior art is complex in process, time-consuming, low in electrolyte utilization ratio, poor in membrane forming efficiency and the like. The preparation method adopts a basic method of micro-arc oxidation, and is characterized in that during the preparation of electrolyte, low-solubility calcium dihydrogen phosphate is used for providing phosphate anions and citric acid is used as a complexing agent. Compared with the prior art, although the solubility of the calcium dihydrogen phosphate used in the preparation method is low, the solubility of the calcium dihydrogen phosphate is improved after the calcium dihydrogen phosphate is complexed with the citric acid, calcium ions and phosphate anions are provided at the same time, the utilization ratio of the electrolyte is high, the reaction speed is high, the membrane forming efficiency is high, the preparation method is simple and easy to operate and low in cost, the hydroxyapatite-containing biological ceramic membrane prepared by the preparation method is stable in structure, uniform in distribution and high in effective matter content, and has a wide prospect in the fields of hard tissue implants, tooth planting and the like.
Owner:JILIN UNIV

Method of quickly preparing calcium phosphate coating containing third-party beneficial ions

The invention provides a method of preparing a calcium phosphate coating containing third-party beneficial ions in a microwave-assisted manner within a short time. The method comprises the following steps: microwave heating a reaction solution containing phosphate anions and calcium ions to form the calcium phosphate coating; and adding the third-party beneficial ions into the reaction solution to prepare the calcium phosphate coating containing the third-party beneficial ions. The method provided by the invention has the advantages of efficiency, low energy consumption, low investment and easiness in control and can fully coat orthopaedical or dental implantation apparatuses and stents with complex structures and the like. The obtained calcium phosphate coating containing the third-party beneficial ions can be applied to the biomedical engineering field of hard tissue repair.
Owner:CHANGZHOU UNIV

Synthesis of Cathode Active Materials

The present invention relates to a method for preparing a lithium vanadium phosphate material comprising forming a aqueous slurry (in which some of the components are at least partially dissolved) comprising a polymeric material, an acidic phosphate anion source, a lithium compound, V2O5 and a source of carbon; wet blending said slurry, spray drying said slurry to form a precursor composition; and heating said precursor composition to produce a lithium vanadium phosphate. In one embodiment the present invention relates to a method for preparing a lithium vanadium phosphate which comprises reacting vanadium pentoxide (V2O5) with phosphoric acid (H3PO4) to form a partially dissolved slurry; then mixing with an aqueous solution containing lithium hydroxide; adding a polymeric material and a source of carbon to form a slurry; wet blending said slurry; spray drying said slurry to form a precursor composition; and heating said precursor composition for a time and at a temperature sufficient to produce a lithium vanadium phosphate compound. In an alternative embodiment the present invention relates to a method for preparing a lithium vanadium phosphate which comprises preparing an aqueous solution of lithium hydroxide; partially dissolving vanadium pentoxide in said aqueous solution; adding phosphoric acid to the aqueous solution; adding a polymeric material and a source of carbon to the solution containing vanadium pentoxide to form a slurry; spray drying said slurry to form a precursor composition; and heating said precursor composition for a time and at a temperature sufficient to form a lithium vanadium phosphate. The electrochemically active lithium vanadium phosphate so produced is useful in making electrodes and batteries.
Owner:SWOYER JEFFREY +2

Method of reducing staining of stannous in dentifrice compositions

Disclosed are methods for reducing the staining of dentifrice composition containing stannous comprising administering to a subject the dentifrice composition. The dentifrice composition is a dual phase dentifrice and is contained in physically separated compartments of a dentifrice dispenser. The first dentifrice composition comprises an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and has a total water content of up to about 20%. The second dentifrice composition comprises an effective amount of stannous ions. The molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1 and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate. The dentifrice composition may alternatively be a single phase dentifrice. The single phase dentifrice will comprise an effective amount of one or more linear polyphosphates having an average chain length of about 4 or more and an effective amount of a stannous anion. The single phase dentifrice has a total water content of up to about 20%, the stannous ion is not delivered from stannous fluoride, a molar ratio of polyphosphate anion to stannous ion is from about 0.2:1 to about 5:1, and the efficacy of the stannous ion in the dentifrice is not reduced by the polyphosphate.
Owner:THE PROCTER & GAMBLE COMPANY
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