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468results about How to "Improve refining effect" patented technology

Al-Si-Cu-Zn-Sn-Ni aluminum-based brazing filler metal and preparation method thereof

The invention relates to an Al-Si-Cu-Zn-Sn-Ni aluminum-based brazing filler metal and a preparation method thereof. The components of the aluminum-based brazing filler metal are 7 to 13 percent by weight of Si, 5 to 11 percent by weight of Cu, 4 to 11 percent by weight of Zn, 1 to 6 percent by weight of Sn, 1 to 3 percent by weight of Ni, 0.02 to 0.3 percent by weight of Ce, 0.01 to 0.1 percent by weight of Sr, 0.01 to 0.2 percent by weight of Zr and the balance of Al. The process flow for preparing the aluminum-based brazing filler metal is that: pure aluminum is added into a graphite crucible and covered by flux for aluminum under the condition of 800 DEG C to 900 DEG C, and slag is removed after melting; the aluminum-based intermediate alloy of high-melting point elements and flux for aluminum are added at the same time, and melting, stirring and slag removal are carried out; the aluminum-based intermediate alloy of low-melting point elements is added under the protection of nitrogen, and melting and stirring are carried out; the mixture of argon and hexachloroethane is added to carry out refining, and standing and slag removal are carried out; the intermediate alloy of trace elements is added, and melting and stirring are carried out; secondary refining and slag removal are carried out; and under the protection of nitrogen, casting formation is carried out. The Al-Si-Cu-Zn-Sn-Ni aluminum-based brazing filler metal has the advantages of low melting point, high strength, high toughness, high corrosion-resistant property and good wetting property and spreadability.
Owner:GUILIN QINGTONG NON FERROUS METAL ARTS & CRAFTS MATERIAL DEV CO LTD

Low-temperature pretreatment process of full-cotton woven fabric

The invention relates to a continuous type low-temperature boiling-off and bleaching pretreatment process of full-cotton woven fabric. At present, the low-temperature boiling-off and bleaching of pre-treatment process exists, but are only the pre-treatment processing process for cotton and blended knitted fabric; research findings or patent documentation of pre-treatment process taking low-temperature boiling-off and bleaching of full-cotton woven fabric are not found at present. In the invention, hot water pre-treatment processing, biological enzyme processing, hot water washing and enzyme blanching and water washing process are firstly preformed on the full-cotton woven fabric, and then the low-temperature scouring and bleaching processing, the low-temperature steam bleaching processingand the water washing process are then performed to finish the pre-treatment of the cotton woven fabric. In the invention, the cotton woven fabric is pre-treated in combination with biological enzymedesizing and the low-temperature scouring and bleaching; the technology in the invention has a good effect without sizing agent residuals and residual cotton seed hulls, and the brightness achieves the effect of the traditional soda boiling and oxygenation bleaching technology.
Owner:HANGZHOU TRANSFAR FINE CHEM CO LTD +2

Industrial refining production method of rice bran oil and equipment thereof

InactiveCN101473873AProblems meeting refining requirementsImprove refining effectEdible oils/fatsSocial benefitsRice Bran Extract
The invention relates to a rice bran oil industrialized refining method and a device for implementing the method. The invention effectively satisfies the rice bran oil refining demands in the rice bran oil industrialized refining. The method is implemented by degumming with water, dewaxing, primary alkali refining, secondary alkali refining, cleaning with water, drying and decolorization, as well as deacidification and deodorization in turn. The device is characterized in that a first crude oil temporary storing tank is connected with a fourth oil pump sequentially through a first oil pump, a hydration kettle, a second oil pump, a pre-cooling tank, a third oil pump and a crystallizing tank, which are connected in series; the fourth oil pump is connected with a first oil refining caldron sequentially through a first frame filtering machine, a second crude oil temporary storing tank and a fifth oil pump; the first oil refining caldron is connected with the water-cleaning caldron sequentially through a sixth oil pump, a second oil refining caldron and a seventh oil pump; the water-cleaning caldron is connected with a decolorization oil pump, a second frame filtering machine, a decolorization oil tank and a deacidification and deodorization kettle through a drying and decolorization kettle; and the deacidification and deodorization kettle is connected with a polishing filter through a shielding pump and a condenser. The invention has the advantages of low production cost, high efficiency, good effect, capability in industrialized mass production and great economic and social benefit.
Owner:PUTIAN JIATENG FOOD IND

Ladle refining slag modifier, preparation method and slag modifying method

The invention belongs to the technical field of steelmaking and refining, and discloses a ladle refining slag modifier, a preparation method and a slag modifying method. The slag modifier comprises the following chemical components in percentage by mass: 30 to 60 percent of CaO, 30 to 60 percent of Al2O3, 2 to 10 percent of MgO2, 2 to 10 percent of B2O3, and less than 8 percent of impurities. The slag modifying method using the slag modifier comprises that: the slag modifier is hoisted to the front of a refining furnace after a steelmaking furnace discharges steels, and then is directly fed into ladles, or the slag modifier can also be fed into the furnace along with other slags at a refining station; the components of modifying slag are determined according to the ladle residue amount and components, desulfuration amount and steel deoxidation product amount; and the modifying slag for controlling the ladle slag comprises the following components according to the adding amount: 48 to 54 percent of CaO, 26 to 32 percent of Al2O3, 6 to 8 percent of MgO, 2 to 4 percent of B2O3, and 0 to 8 percent of SiO2, wherein the modifying slag is better if the content of the SiO2 is lower. The slag modifier has the capabilities of quickly manufacturing the slag, improving desulfuration and deoxidation of the refining slag and accommodating and absorbing deoxidation products, and is simple to prepare and convenient to store, transport and use.
Owner:JIANGSU UNIV

Method for purifying industrial silicon through external refining

The invention relates to a method for purifying industrial silicon through external refining, which comprises the following steps of: continuously introducing refined gas to a ladle before a submerged arc furnace releases a silicon melt to the ladle; then releasing the silicon melt into the ladle, heating in the ladle, controlling the temperature of the melt within a certain scope, adding a refining agent into the ladle for slag refining, adjusting the introducing flow rate, the pressure and the like of the refined gas along with the continuous increase of the quantity of the silicon melt in the ladle for external refining; and after the completion of the external refining, carrying out slag silicon separation and then pouring, i.e. the purification of the industrial silicon through the external refining is finished. Through the external refining process, a majority of metal impurities containing Al, Ca, Ti and Na and a part of B, P, S and C and other non-metallic impurities in the industrial silicon melt can be removed, and meanwhile, the effective components can be controlled for the subsequent purification of the industrial silicon, and high-quality raw materials are provided for solar grade silicon prepared by a metallurgical method. The method has the characteristics of full utilization, energy resource conservation, high production efficiency, less infrastructure investment, no environment pollution and the like.
Owner:KUNMING UNIV OF SCI & TECH

Slag adhesion preventing fluorine-free slag modifier for ladle refining, preparation method and using method

The invention belongs to the field of steelmaking, and particularly discloses a fluorine-free slag modifier for preventing a ladle refining device from adhering slag, a preparation method and a using method. The slag modifier consists of active lime, bauxite and boric anhydride; and the slag modifier comprises the following chemical components in percentage by mass: 75 to 85 percent of CaO, 10 to 20 percent of Al2O3, 5 to 15 percent of B2O3, 0 to 8 percent of MgO, and the balance of impurities, wherein SiO2 is less than 7.0 percent, H2O is less than 0.05 percent, and the total amount of sulfur and phosphor is less than 0.01 percent. During use, in order to prevent a ladle from adhering the slag, the slag modifier is fed into the ladle in the later period of discharging steel from a steelmaking furnace, and in order to prevent an RH dip pipe or a CAS-OB dip cover and the like from dipping into the ladle device to adhere slag, the slag modifier is fed at a refining station. The slag modifier can effectively control the refining device from slag adhesion and improve the service life of a fireproof material, is favorable for reducing the contents of the sulfur, oxygen and impurities in the steel, and is simple to prepare and convenient to store, transport and use.
Owner:JIANGSU UNIV

Preparation method of rear-earth magnesium alloy product

The invention relates to a preparation method of a rear-earth magnesium alloy product. The preparation method comprises the following steps of: placing dehydrated rear-earth chlorate in a melting electrolysis device; adding dehydrated magnesium chloride, potassium chloride and titanium dichloride for dispersing, mixing and carrying out melting electrolysis, so that rear-earth magnesium intermediate alloy is generated by co-electrodeposition of rear-earth ion and magnesium ion at a negative electrode; burdening and mixing the rear-earth magnesium intermediate alloy and the metal magnesium in a smelting device, wherein a molar ratio of the rear-earth metal to the magnesium is (0.1-1.0):100; heating up the rear-earth magnesium alloy mixture for melting, immersing the smelting agent inside the melt and stirring, increasing the temperature to 780 DEG C and stewing for 20 minutes for dividing the melt into an upper layer, a middle layer and a lower layer, wherein the middle melt layer is used as the rear-earth magnesium alloy melt; casting after pre-cooling, cooling and forming, and carrying out surface treatment after carrying out mechanical processing and thermal processing, so that a compact proactive film layer is covered on the surface of the rear-earth magnesium alloy product. The preparation method of the rear-earth magnesium alloy product is high in preparation efficiency, safe and reliable in process, environment-friendly and low in energy consumption.
Owner:YANGZHOU FENG MING METAL PROD

Method and device for casting electromagnetic compound control electroslag remelting fine grains

The invention relates to a method and a device for casting electromagnetic compound control electroslag remelting fine grains, and belongs to the field of preparation of metal materials. According to the method, metallic melt generates forced convection by using the action of exerted pulse magnetic field and periodic electromagnetic force which is generated by compounding of induced current in the melt and electroslag remelting current; a metal material solidification structure is fined; and composition segregation is reduced. Metal droplets can be crushed into fine liquid drops under the action of the electromagnetic force with direction and size in periodic change; the contact area and the contact time of the metal droplets and slag liquid are improved; and a good purification effect is achieved. The device comprises an electroslag remelting work power supply, a pulse power supply and an electromagnetic compound control electroslag remelting crystallizer, wherein the crystallizer is provided with a crystallizer red copper inner sleeve, a side cooling jacket, a bottom cooling jacket and a magnet exciting coil. The method and the device can be applied to electroslag remelting and refining of metal materials such as high-temperature alloy and high alloy steel; the alloy solidification structure can be fined; the segregation is reduced; the refining effect of the electroslag remelting process is improved.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method for determining amount of slagging material and deoxidized alloy added into LF (Low-Frequency) refining furnace by use of reference heat method

ActiveCN103866088AProcessing data is accurateAvoid instabilityProcess efficiency improvementSlagInstability
The invention relates to a method for determining the amount of a slagging material and deoxidized alloy added into an LF refining furnace by use of a reference heat method. The method comprises the following steps: controlling the amount of slags discharged from a rotary furnace during a refining process, wherein the amount of the added synthetic slags is the same during a steel discharging process of the rotary furnace according to the same type of steel heat number; (1) acquiring data and building a database by use of a computer; and (2) using the database for determining the amount of the slagging material and the deoxidized alloy added into this type of steel LF refining furnace when the acquired data of a certain type of steel in the database is accumulated to be not less than 400 heat number. The method disclosed by the invention comprises steps of acquiring operation data, building the database and using the computer to process the data rapidly and accurately; the reference heat method absolutely can be used for replacing the existing slagging method for manually determining the amount of the added slagging material and has the advantages of solving the instability of manual determination, optimizing the refining effect, stabilizing the quality of refined liquid steel and promoting standardized operation.
Owner:LAIWU STEEL YINSHAN SECTION CO LTD

Method for controlling electroslag melting casting by added transient magnetic field and electroslag smelting casting device

The invention discloses a method for controlling electroslag melting casting by an added transient magnetic field. The method includes adding a transient magnetic field to a melting end of an electroslag remelting mother electrode, a liquid slag tank and a metal melting tank so that the transient magnetic field acts on large metal molten drops which are generated by initial melting at the tail end of the electrode and are converging to become big; under joint action of alternating lorentz force and pressure waves generated by the transient magnetic field, dispersing the metal molten drops in a burst manner into small metal molten drop groups, and randomly dispersing the small metal molten drop groups into the liquid slag tank to sufficiently contact with liquid slag after passing the liquid slag tank; after washing, enabling included foreign substances and impurities in the small metal molten drops to enter the liquid slag quickly, slowly settling and converging the foreign substances and impurities into the metal melting tank below the liquid slag tank, and finally crystallizing and solidifying to form solidified cast ingots. The invention further provides an electroslag melting casting device. By adding the transient magnetic field during electroslag melting casting and fining the molten drops by the aid of unique electromagnetic effect of the transient magnetic field, the purposes of improving refining efficiency, fining crystalline grains and reducing segregation of cast ingots are achieved, and industrial application value is realized.
Owner:SHANGHAI UNIV
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