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34results about How to "Control aspect ratio" patented technology

Metal microparticle, composition containing the same and process for producing metal microparticle

The present invention provides metal fine particles which have selective wavelength absorption characteristics in a wavelength region from visible light to near infrared light, and have sharp absorption characteristics, and influences little the surrounding wavelength, and therefore, they yield tones having high chroma. The present invention provides metal fine particles wherein an aspect ratio is in a range from 1.1 to 8.0, a maximum absorption wavelength in plasmon absorption is in a range from 400 nm to 1,200 nm, and an absorption coefficient at a peak position of the maximum absorption wavelength is in a range from 6,000 to 20,000 L / mol.cm (measurement concentration: 1.6x10-4 mol / L, and solvent:water).
Owner:MITSUBISHI MATERIALS CORP +1

Method for producing rosin

The invention provides a method for producing rosin by turpentine, which comprises the following steps of melting, clarifying and distilling. The melted turpentine liquid is pressed in at least two higher-placed furnaces by vapor pressure in the melting process. The subsequent clarifying process is performed after the melted turpentine liquid is stayed in the higher-placed furnaces. The rosin product obtained by the method of the present invention can reach the grade of national superfine standard.
Owner:景东力奥林产集团林业化工有限公司

Device and method for detecting mechanical parameters of hydrate-containing sediments based on X-CT

The invention provides a device and a method for detecting mechanical parameters of hydrate-containing sediments based on X-CT. The device comprises a reaction kettle, a shear loading unit, a back pressure control unit, an unloading pressure loading unit and a strain measurement unit, wherein the reaction kettle body is a beryllium or carbon fiber pressure-resistant pipe, and the two end are sealed with end covers; the outer side of the lower end cover is connected with an axial pressure loading counter-force mechanism; an upper sample adjusting cushion block, a sediment sample, a lower sampleadjusting cushion block and an axial pressure loading piston are arranged in the reaction kettle from top to bottom. According to the device and the method, high-pressure conditions required for synthesizing the methane hydrate are met, and the axial temperature of the sample can be precisely controlled, so that the sample is uniformly distributed; the sample preparation efficiency can be improved through the rapid temperature control, the sample size can be adjusted, and the purpose of controlling height-diameter ratios of the different samples is achieved; and the synchronous detection of astress-strain curve of the sediments containing the natural gas hydrate and the internal destructive microstructures of the sediments can be achieved, and the constant strain shearing and the constant stress creep tests can be realized.
Owner:QINGDAO INST OF MARINE GEOLOGY

Method for repairing nano stick of zinc oxide in even diameter

The method for preparing zinc oxide nano rod with uniform diameter includes the following steps: (1) dissolving zinc acetate in absolute ethanol or absolute methanol, fully stirring them at zero deg.C to obtain suspended liquor whose concentration is 0.5-30%, dissolving lithium hydroxide in absolute ehtanol or absolute methanol at room temperature to obtain lithium hydroxide solution whose molar concentration is twice that of zinc acetate; (2). under the temperature of zero deg.C drop-by-drop adding isopyknic lithium hydroxide solution to stirring zinc acetate solution to obtain white colloidal mixed solution; (3) placing said colloidal solution into a hydrothermal reactor, sealing said reactor, heat-insulating for 5-24 hr, at 80-200 deg.C, and taking out reaction solution; and (4). centrifugally-separating reaction solution, fully washing separated material by using absolute ethanol, drying at room temp. so as to obtain the invented product.
Owner:ZHEJIANG UNIV

Alloy nanotube and manufacturing method thereof

The invention discloses an alloy nano-tube and a preparation method thereof, which belong to the field of nanometer material. The alloy nano-tube is a solid solution, a metal compound or an amorphous state formed by two transition metal elements, namely A and B, wherein the A accounts for 15.3 to 86.4 percent of the total amount, and the B accounts for 13.6 to 84.7 percent of the total amount. The preparation method comprises the following steps: a formwork with a layer of gold or platinum film introduced into the back side is soaked in an electrolysis bath containing metal ion A and B, and is electrodeposited under certain voltage and current conditions to obtain a binary alloy nano-tube. Binary alloy nano-tubes with different diameters, different lengths and different components can be obtained by adopting formworks with nanochannels with different inner diameters, controlling the electrodeposition time and adjusting cathode current density. The binary alloy nano-tube has simple preparation process, mild reaction conditions, strong controllability and good application prospect.
Owner:BEIJING UNIV OF CHEM TECH

Large height-width ratio photon sieve and preparation method thereof

The invention discloses a large height-width ratio photon sieve and a preparation method thereof. The large height-width ratio photon sieve comprises a substrate and a photon sieve column, wherein the substrate comprises a photon sieve region and an edge region; the edge region is nontransparent for light with a preset wavelength; besides the region in which the photon sieve column is positioned, the photon sieve region is transparent for the light with the preset wavelength; and the photon sieve column is approximately of a cylinder shape, is positioned at the position in the photon sieve region, which corresponds to a fresnel zone plate bright ring, and is nontransparent for the light with the preset wavelength. According to the invention, the height-width ratio can be controlled under high efficiency, so that the phase or amplitude photon sieve can be better manufactured.
Owner:INST OF MICROELECTRONICS CHINESE ACAD OF SCI

Metal fine particle, method for producing metal fine particle, composition containing same, optical absorbing material and application thereof

Disclosed is a method for producing metal fine particles wherein an aqueous solution containing amines having reducing powder and an ammonium salt substantially having no reducing power is used for reducing metal ions by the amines in the presence of the ammonium salt, thereby producing rod-shaped metal fine particles. Also disclosed are metal fine particles which are characterized by being produced by such a method for producing metal fine particles and having a major axis of not more than 400 nm, a minor axis of not more than 15 nm, and an aspect ratio of more than 1.
Owner:MITSUBISHI MATERIALS CORP +1

Method used for preparing flake-like silicon dioxide powder

The invention provides a method used for preparing flake-like silicon dioxide powder, and belongs to the technical field of powder particle size and morphology control. According to the method, bauxitic clay ore powder containing SiO2 is taken as a raw material; an activator, a dispersant, and a crystal grain morphology control agent are added into the raw material for uniform mixing; an obtained mixed powder is subjected to calcining in atmosphere containing halogen, and obtained silicon halide is subjected to hydrolysis so as to obtain silicon dioxide and halogen hydride; after calcining, the valve of a sealed reaction container is unsealed, so that high pressure gas in the sealed reaction container is delivered into a gas-solid separator with a larger volumn via expansion so as to realize gas-solid separation of silicon halide with gas phase and obtain the flake-like silicon dioxide powder, wherein the gas-solid separator is provided with a water cooling jacket. Thickness of the flake-like silicon dioxide powder is less than 0.2 <mu>m, and average diameter-to-thickness ratio is higher than 50. Reaction temperature of the method is relatively low; the method is simple; energy consumption is low; production cost is low; and the diameter-to-thickness ratio of the flake-like silicon dioxide powder can be adjusted.
Owner:贵州天合国润高新材料科技有限公司

Method for manufacturing photon sieve with high height-width ratio

The invention discloses a method for manufacturing a photon sieve with a high height-width ratio. The method comprises the following steps of: manufacturing a photon sieve mask plate and an optical alignment mask plate; performing X-ray copying by utilizing the photon sieve mask plate to obtain a first copied mask plate; performing the X-ray copying again by utilizing the first copied mask plate to obtain a second copied mask plate; and optically aligning a photon sieve pattern of the second copied mask plate by utilizing the optical alignment mask plate as a mask to obtain the photon sieve with the high height-width ratio. Compared with the conventional manufacturing method for the photon sieve, the method has the advantage that: the photon sieve with a higher height-width ratio and a shorter operating wavelength can be manufactured.
Owner:INST OF MICROELECTRONICS CHINESE ACAD OF SCI

Preparation method of tellurium nanowire material, tellurium nanowire material and device

The invention discloses a preparation method of a tellurium nanowire material, the tellurium nanowire material and device. The preparation method comprises the following steps: by taking tellurium powder as a raw material, performing deposit growth of tellurium nanowires on the silica surface of a silica-silicon substrate by adopting physical vapor deposition, wherein the gaseous phase of the physical vapor deposition is mixed gas of argon and hydrogen, the total flow of the argon and hydrogen is 70sccm, and the physical vapor deposition temperature is 600-800 DEG C. The tellurium nanowires are directly prepared on the silica-silicon substrate by adopting physical vapor deposition. The preparation method is simple in process, does not involve any chemical reaction, and has the characteristics of environment friendliness and the like, the cost is low, the prepared tellurium nanowire is high in quality, and the draw ratio of the nanowire can be controllably regulated. The tellurium nanowire can serve as a material of a gas sensor, a catalyst, a thermoelectric material, a photoelectric material, a solar cell and a field effect transistor.
Owner:NORTHWEST UNIV

A design method of a cylindrical radial uniform magnetic field coil

The invention discloses a design method of a cylindrical radial uniform magnetic field coil, which comprises the following steps of: firstly, equally dividing the surface of the coil along the axial direction according to the azimuth angle of a cylindrical coordinate system, determining the surface current density expression on one side, and determining that the current density distribution on theother side is completely the same as that on the other side but opposite in current direction; secondly, deducing a magnetic field expression of a target field point, selecting the curvature of the current density as a penalty function of a constraint coil, setting a constraint factor of the penalty function, and solving a value of an undetermined coefficient in the current density expression byutilizing a regularization method to obtain a current density distribution condition of the cylindrical surface; and finally, obtaining an actual current routing shape of the cylindrical radial uniform magnetic field coil by using a flow function. The method serves as an inverse method of coil design, the size of the cylindrical coil is limited in advance, the coordinate position of a target fieldpoint is selected, then actual current distribution of the coil is obtained through calculation, the length-diameter ratio of the cylindrical coil is effectively controlled, and a gap can be reservedin the center of the coil to form a light through hole.
Owner:BEIHANG UNIV

Preparation method for carbon nanotube antistatic material easy to disperse

The invention relates to a preparation method for carbon nanotube antistatic material easy to disperse. First, acid-soluble inorganic powder is selected, an iron or cobalt or nickel catalyst is evenly loaded on the surface of the inorganic powder, and the loading capacity of iron or cobalt or nickel is controlled; then, the load catalyst is placed into reducing atmosphere of 300 DEG C-500 DEG C to be activated, then the activated catalyst is conveyed into a reactor containing alkane, olefin, hydrogen and carbon monoxide, and at 500 DEG C-900 DEG C, carbon nanotubes (CNTs) which have oriented growth and are controllable in length-diameter ratio are prepared; finally, by the adoption of acid dissolution carriers, the carbon nanotube antistatic material easy to disperse is obtained, wherein the content of the carbon nanotubes in the carbon nanotube antistatic material is high. When the addition quantity of CNTs in epoxy resin reaches 10<-4> level, a high-transparency and stable-resistance (106-108 omega) film can be obtained, and the film has excellent antistatic performance characteristics and product economy advantages.
Owner:JUNJIANG SCI & TECH CO LTD SHANGHAI

High-linearity gradient coil design method

The invention discloses a high-linearity gradient coil design method, and the method comprises the steps: proposing two new Fourier series expansion current density functions, and introducing a stream function; selecting discrete target points in the N target areas, deducing a magnetic field expression of the target field points according to the Biot-Savart law, and constructing a relation matrix between the magnetic field expression and the current density function; setting a value of a target field point, selecting a minimum curvature of a flow function as a penalty function of a constraint coil, setting a constraint factor of the penalty function, solving an undetermined coefficient in a current density expression through a regularization method, and obtaining a current density distribution condition of the cylindrical surface; the current density is discretized using a stream function to generate a winding diagram of the coil. The gradient coil is designed by improving the target field method, so that the linearity of the gradient field is greatly improved; the size of the cylindrical coil is preset before calculation, so that the limitation on the size is overcome; curvature constraint and regularization methods are introduced to solve the ill-conditioned problem of solutions, so that the gradient coil is convenient to process and manufacture.
Owner:BEIHANG UNIV

A device and method for detecting mechanical parameters of hydrate-containing sediments based on x-ct

The present invention proposes a device and method for detecting mechanical parameters of hydrate-containing sediments based on X-CT. The device includes a reactor, the body of the reactor is a beryllium or carbon fiber pressure-resistant tube, the end covers at both ends are sealed, and the outer side of the lower end cover is connected to the The axial pressure loading reaction mechanism is connected, and the interior of the reactor is from top to bottom: the upper sample adjustment pad, the sediment sample, the lower sample adjustment pad and the axial pressure loading piston, and also includes a shear loading unit, a back pressure control unit, Unload the pressure loading unit and the strain measurement unit. The invention satisfies the high-pressure conditions required for the synthesis of methane hydrate, and can accurately control the axial temperature of the sample to make it evenly distributed; it can also quickly control the temperature to improve the efficiency of sample preparation, and can adjust the size of the sample to achieve control of different The purpose of the aspect ratio of the sample is that the invention can realize the simultaneous detection of the stress-strain curve of the gas hydrate-containing sediment and the internal damage microstructure of the sediment, and can realize the constant-strain shear and constant-stress creep test.
Owner:QINGDAO INST OF MARINE GEOLOGY

Solar cell front conductive silver paste and preparation method thereof

The invention provides solar cell front conductive silver paste and a preparation method thereof, and the conductive silver paste is prepared from the following materials in parts by weight: 40-50 parts of bisphenol A epoxy resin; 20 to 40 parts of nano silver particles; 30 to 50 parts of nano glass powder; 50-60 parts of an organic carrier mixed solution; 8 to 10 parts of tetraethyl titanate; 6-9 parts of alkaline amine; 5 to 10 parts of anhydride; 8 to 15 parts of a boron trifluoride monoethylamine complex; the organic carrier mixed solution comprises organic acid doped conductive organic polymer / epoxidized soybean oil with the mass fraction concentration of 15%-20% and a high-boiling-point solvent with the mass fraction concentration of 80%-85%. According to the invention, the contact between the inorganic powder and the screen cloth material can be effectively wetted, the more excellent fine line ink penetration capability is provided, the method is suitable for the high-speed printing of the ultra-fine grid of the current large-area silicon wafer, the fine grid line width control capability is excellent, and the better electrode height-width ratio can be formed.
Owner:DK ELECTRONICS MATERIALS INC

Dispersing method capable of accurately regulating and controlling slenderness ratios of alumina whiskers

The invention provides a dispersing method capable of accurately regulating and controlling slenderness ratios of alumina whiskers. The dispersing method comprises the following step: dispersing the alumina whiskers in a dispersing agent by adopting a cooperative dispersing method implemented by ultrasonic waves, blade agitation and big ball low-speed ball milling, wherein the dispersing agent comprises a first dispersing agent and a second dispersing agent; the first dispersing agent is polyethylene glycol; the second dispersing agent is 2-amino-2-methyl-1-propanol or polyacrylic acid; the mass ratio of the first dispersing agent to the second dispersing agent is (1 to 3) to (0.1 to 3). Compared with the prior art, the dispersing method has the advantages that a steric-hindrance effect and an electric double layer theory are brought into full consideration, a non-ionic dispersing agent and an anionic dispersing agent prepared from specific components are used in a combination way, and the cooperative dispersing method implemented by the ultrasonic waves, the blade agitation and the big ball low-speed ball milling is adopted on the basis of reasonably controlling the proportion of the two dispersing agents, so that a good dispersing effect of the alumina whiskers of different slenderness ratios is achieved.
Owner:GUANGDONG UNIV OF TECH

A method of manufacturing a fin field effect transistor

The invention relates to a fin field effect transistor preparation method. The preparation method comprises the following steps: a base is provided, wherein the base comprises a semiconductor substrate and an insulating layer located on the semiconductor substrate, the base has a stepped shape and has a high region and a low region; a hard mask layer is formed on the insulating layer and planarization is performed; the hard mask layer and the insulating layer are etched, and at least one groove is formed in the high region and the low region of the base separately so as to expose the semiconductor substrate; the groove is filled with a semiconductor material and planarization is performed to form a fin pattern; and the hard mask layer is removed through etching to form fins having different heights. According to the invention, the heights of the fins, the height difference of the fins having different heights and the fin depth-width ratio can be controller easier, the problem that the fin height is not easy to control in the prior art can be solved skillfully, and the yield of semiconductor devices can be improved.
Owner:SEMICON MFG INT (SHANGHAI) CORP +1

Preparation method of alloy semiconductor composite nano material based on aqueous phase synthesis and alloy semiconductor composite nano material

The invention discloses a preparation method of alloy semiconductor composite nano-material based on aqueous phase synthesis and the alloy semiconductor composite nano-material. The preparation methodcomprises the steps of nanogold preparation, nano-alloy preparation and composite nano-material preparation. According to the preparation method provided by the invention, two or more composite nanomaterials with ideal photoelectric application properties and controllable particle size and thickness can be prepared by combining a seed growth method and a chemical replacement method, and comparedwith other single-component or composite materials compounded through other manners, local surface plasma coupling is more ideal; and the photothermal conversion efficiency is higher.
Owner:JIHUA LAB

A method for preparing flaky silicon dioxide powder

The invention provides a method used for preparing flake-like silicon dioxide powder, and belongs to the technical field of powder particle size and morphology control. According to the method, bauxitic clay ore powder containing SiO2 is taken as a raw material; an activator, a dispersant, and a crystal grain morphology control agent are added into the raw material for uniform mixing; an obtained mixed powder is subjected to calcining in atmosphere containing halogen, and obtained silicon halide is subjected to hydrolysis so as to obtain silicon dioxide and halogen hydride; after calcining, the valve of a sealed reaction container is unsealed, so that high pressure gas in the sealed reaction container is delivered into a gas-solid separator with a larger volumn via expansion so as to realize gas-solid separation of silicon halide with gas phase and obtain the flake-like silicon dioxide powder, wherein the gas-solid separator is provided with a water cooling jacket. Thickness of the flake-like silicon dioxide powder is less than 0.2 <mu>m, and average diameter-to-thickness ratio is higher than 50. Reaction temperature of the method is relatively low; the method is simple; energy consumption is low; production cost is low; and the diameter-to-thickness ratio of the flake-like silicon dioxide powder can be adjusted.
Owner:贵州天合国润高新材料科技有限公司

Array substrate, preparation method thereof and display panel

The invention provides an array substrate and a preparation method thereof and a display panel, the array substrate comprises an electrode layer, a gate insulation layer and an active layer, the electrode layer comprises a first metal layer, a second metal layer and a third metal layer which are stacked, a first end of the active layer is electrically connected with the first metal layer, and a second end of the active layer is electrically connected with the third metal layer. The second end of the active layer is electrically connected with the third metal layer, the second metal layer comprises at least two stacked metal sub-layers in the direction from the first metal layer to the third metal layer, and every two adjacent metal sub-layers are arranged in an insulated mode; according to the invention, the first metal layer, the second metal layer and the third metal layer which form the electrode layer are stacked, the channel of the active layer is arranged on the side wall of the electrode layer, the second metal layer is divided into a plurality of metal sub-layers which are stacked, and the thickness and the number of the metal sub-layers can be regulated and controlled, so that the thickness and the number of the metal sub-layers can be regulated and controlled. Therefore, the width-to-length ratio of the channel of the active layer can be regulated and controlled, and the purpose of flexibly regulating the characteristics of the thin film transistor is achieved.
Owner:WUHAN CHINA STAR OPTOELECTRONICS SEMICON DISPLAY TECH CO LTD

Alloy nanotube and manufacturing method thereof

The invention discloses an alloy nano-tube and a preparation method thereof, which belong to the field of nanometer material. The alloy nano-tube is a solid solution, a metal compound or an amorphous state formed by two transition metal elements, namely A and B, wherein the A accounts for 15.3 to 86.4 percent of the total amount, and the B accounts for 13.6 to 84.7 percent of the total amount. The preparation method comprises the following steps: a formwork with a layer of gold or platinum film introduced into the back side is soaked in an electrolysis bath containing metal ion A and B, and is electrodeposited under certain voltage and current conditions to obtain a binary alloy nano-tube. Binary alloy nano-tubes with different diameters, different lengths and different components can be obtained by adopting formworks with nanochannels with different inner diameters, controlling the electrodeposition time and adjusting cathode current density. The binary alloy nano-tube has simple preparation process, mild reaction conditions, strong controllability and good application prospect.
Owner:BEIJING UNIV OF CHEM TECH

Method for manufacturing photon sieve with high height-width ratio

The invention discloses a method for manufacturing a photon sieve with a high height-width ratio. The method comprises the following steps of: manufacturing a photon sieve mask plate and an optical alignment mask plate; performing X-ray copying by utilizing the photon sieve mask plate to obtain a first copied mask plate; performing the X-ray copying again by utilizing the first copied mask plate to obtain a second copied mask plate; and optically aligning a photon sieve pattern of the second copied mask plate by utilizing the optical alignment mask plate as a mask to obtain the photon sieve with the high height-width ratio. Compared with the conventional manufacturing method for the photon sieve, the method has the advantage that: the photon sieve with a higher height-width ratio and a shorter operating wavelength can be manufactured.
Owner:INST OF MICROELECTRONICS CHINESE ACAD OF SCI

Passenger ship main body structure resistant to stormy waves and unlikely to turn over

The invention discloses a passenger ship main body structure resistant to stormy waves and unlikely to turn over and belongs to the technical field of shipping design and construction of traffic navigation passenger ships. The passenger ship main body structure can meet the demands for civil water transportation of passengers and solve the problems that the gravity centers of most passenger ship main body structures of different countries all around the world at present are too high, there are too many ship passenger cabin layers above ship full-load water lines in order to contain more passengers, and correspondingly the ships are likely to turn over. According to the structure, by reducing the height of a hull, reducing the passenger cabin layers, widening the hull, increasing underwaterpressure loading buoyancy chambers, lowering the gravity center of the hull, vertically designing the hull in an A shape with a narrow upper part and a wide lower part from the prow to the stern, designing two layers of passenger cabins, making a conical cockpit positioned above the passenger cabins, forming a catamaran and adopting other design schemes, the passenger ship main body structure isachieved.
Owner:李乃斌

A kind of preparation method of anisotropic silicon quantum dot film

The invention relates to a preparation method of a silicon quantum dot film having anisotropy, and discloses a technical method for regulating elemental composition variation to form different strain energy induced anisotropic polymorphous silicon quantum dots, further regulating the absorption spectrum range and obviously improving the photoelectric conversion efficiency of a used material. The preparation method comprises the following main steps: performing pretreatment prior to coating, performing magnetron co-sputtering on a silicon-germanium alloy target and a carbon target having different composition ratios with Ar ions, regulating the sputtering power of the silicon-germanium target and the carbon target, and depositing a composition-controllable amorphous silicon carbide-germanium film on a silicon and glass base; and then, performing multi-stage annealing treatment in a nitrogen gas atmosphere, thus forming the silicon quantum dot film having anisotropy, which is inlaid in amorphous SiC. The film has multi-exciton effect, and simultaneously has multi-wavelength light absorption characteristics in a wavelength range of 1800nm (infrared) to 300nm (ultraviolet), thus hopefully improving the light absorption and photoelectric conversion efficiency of a silicon-based photovoltaic device greatly.
Owner:汉中艾斯达特新材料科技有限公司

A Dispersion Method for Precisely Controlling the Aspect Ratio of Alumina Whiskers

The invention provides a dispersing method capable of accurately regulating and controlling slenderness ratios of alumina whiskers. The dispersing method comprises the following step: dispersing the alumina whiskers in a dispersing agent by adopting a cooperative dispersing method implemented by ultrasonic waves, blade agitation and big ball low-speed ball milling, wherein the dispersing agent comprises a first dispersing agent and a second dispersing agent; the first dispersing agent is polyethylene glycol; the second dispersing agent is 2-amino-2-methyl-1-propanol or polyacrylic acid; the mass ratio of the first dispersing agent to the second dispersing agent is (1 to 3) to (0.1 to 3). Compared with the prior art, the dispersing method has the advantages that a steric-hindrance effect and an electric double layer theory are brought into full consideration, a non-ionic dispersing agent and an anionic dispersing agent prepared from specific components are used in a combination way, and the cooperative dispersing method implemented by the ultrasonic waves, the blade agitation and the big ball low-speed ball milling is adopted on the basis of reasonably controlling the proportion of the two dispersing agents, so that a good dispersing effect of the alumina whiskers of different slenderness ratios is achieved.
Owner:GUANGDONG UNIV OF TECH

Controllable double-layer prismatic-disc-shaped micron zinc oxide and preparation method thereof

The invention discloses controllable double-layer prismatic-disc-shaped micron zinc oxide and a preparation method thereof, and belongs to the technical field of preparation of micro-nano materials. The preparation method comprises the steps of uniformly dispersing a zinc source in a solvent, dropwise adding an alkali solution, and carrying out double decomposition reaction to obtain a reactant solution; carrying out hydrothermal reaction on the reactant solution, and naturally cooling after the hydrothermal reaction is finished to obtain a product solution; and after the obtained product solution is subjected to centrifugal treatment, reserving a solid product, washing the obtained solid product, and then drying to obtain the controllable double-layer prismatic-disc-shaped micron zinc oxide. The solvent is a mixed solvent of an alcohol solvent and water, and by adjusting the mixing ratio of the alcohol solvent and the water, the controllable adjustment of the size of the side length of the double-layer prismatic disc-shaped micron zinc oxide prismatic disc and the height of the double-layer prismatic disc is realized. The controllable double-layer prismatic-disc-shaped micron zinc oxide with high purity and good crystallinity is prepared through the preparation method with a simple process and has excellent ultraviolet light absorption performance.
Owner:XI AN JIAOTONG UNIV

Preparation and application of a magnetic hydrogel loaded with one-dimensional Fe3O4 nanocrystals

Preparation and application of a magnetic polymer hydrogel loaded with one-dimensional iron ferric oxide nanocrystals, preparing anionic hydrogel or anionic hydrogel precursor solution, and preparing FeSO4 and Fe2(SO4)3 mixed water to form iron Ionic solution; then mix the two, soak at room temperature, so that the anionic hydrogel completely absorbs iron ions; soak the hydrogel that has absorbed iron ions in NaOH solution, and heat it in a water bath to obtain a magnetic material loaded with one-dimensional Fe3O4 nanocrystals. The polymer hydrogel can be used to treat sewage containing organic dyes. The present invention does not use any toxic or organic reagents, and obtains a loaded one-dimensional structure (rod-shaped ) Magnetic polymer hydrogel of Fe3O4 nanocrystals, and overcomes the problem of uneven distribution of magnetic particles.
Owner:扬州爱科新材料科技有限公司
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