Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

57results about How to "Process control stability" patented technology

Method for producing special rutile type titanium white powder for power coating

The invention discloses a method for producing special rutile type titanium white powder for power coating, which comprises the following steps of: preparing slurry of which titanium dioxide concentration is 300 to 400g / l by using bleached metatitanic acid, and adding a calcining auxiliary agent into the slurry; filtering the obtained metatitanic acid, then calcining solid, and grinding the solidto obtain a primary product; preparing titanium dioxide slurry of which titanium dioxide concentration is 650 to 850g / l by using the obtained primary product, adding a wetting agent into the titaniumdioxide slurry, and performing dispersion and grinding; heating the obtained titanium dioxide slurry to between 40 and 90 DEG C, adding dispersant, zircon salt or titanium salt, silicon salt and aluminum salt into the slurry in turn, adjusting the pH value to between 5 and 9, ageing the mixture, and adjusting the pH value to between 7 and 8; and then filtering, washing and drying the mixture, treating the dried product by an organic surface treatment agent, and vaporizing the product to obtain the rutile type titanium white powder. Compared with the prior art, the rutile type titanium white powder obtained by the method has the properties of stable crystal lattice, good dispersion, heat and yellowing resistance, and good oily whiteness, reducing power, covering power and weather resistance and the like; the appearance and properties of the rutile type titanium white powder are close to that of the rutile type titanium white powder prepared by a chlorination process; and the productionmethod has the advantages of easily obtained process raw materials and stable process control.
Owner:NINGBO XINFU TITANIUM DIOXIDE

Preparation method of fluorine-silicon surfactant

The invention discloses a preparation method of a fluorine-silicon surfactant. The method comprises the following steps of: continually dripping 13 to 18 weight parts of trichlorosilane into 44 to 65 weight parts of perfluor alkyl ethylene or perfluor alkyl ethyl iodide serving as a raw material in the presence of 0.1 to 1.0 weight part of noble metal catalyst so as to obtain an intermediate product; and adding 14.8 to 20 weight parts of high-boiling-point solvent into the intermediate product, continuously dripping 10 to 16.35 weight parts of methanol or ethanol for reacting, decompressing and rectifying so as to obtain a target product. In the method, raw materials are readily available, byproduct is not produced, a reaction in an entire synthesis process is stable, process control is stable, safety, low cost and easy separation are realized, the yield of a final fluorine-silicon surfactant is over 95 percent, and the purity of the surfactant is over 98 percent. Due to the presence of a siloxane active group, the fluorine-silicon surfactant can react with and be tightly combined with substances with a hydroxy functional group, such as glass and the like, so that the surface of the fluorine-silicon surfactant has high waterproofness, oil resistance and soil resistance, surface tension is less than 17.6 dynes per meter, and light transmittance is over 99.9 percent.
Owner:JINZHOU DPF TH CHEM CO LTD

Cleaning and wool making technology for monocrystal silicon chip

The invention relates to a cleaning and wool making technology for a monocrystal silicon chip, and belongs to the technical field of chemical engineering. The technology particularly comprises the following step: (1) adopting a self-made silicon chip cleaning agent to perform precleaning on the silicon chip; (2) putting the pre-cleaned silicon chip into a wool making trough; preparing a wool making liquid in the wool making trough, and adding 0.1 to 5% of sodium hydroxide, 0.1 to 3% of potassium hydroxide, 1 to 5% of isopropyl alcohol and 0.02 to 5% of a self-made wool making additive in percentage by weight into the wool making liquid; rising temperature until the reaction temperature is 70 DEG C to 90 DEG C to make wool; turning on ultrasonic equipment during the wool making process; (3) when the wool is prepared, closing the trough body; before the chip is cast, stirring by adopting a stirring device, wherein the wool making reaction time is 15 to 40 min. According to the invention, through the adoption of the cleaning agent and the wool making additive, the technology is controlled to be simple and stable, the energy consumption is reduced, and the capability of process control is enhanced, so that the control quality of the product in various aspects is greatly improved, the production cost in various aspects is reduced, and the comprehensive economic benefit is increased.
Owner:HENAN INST OF SCI & TECH

Chemical reaction apparatus and chemical reaction method for removing vanadium from crude TiCl4

InactiveCN106946286AHigh vanadium removal efficiencyProcess control stabilityTitanium tetrachlorideChemical reactionDouble tube
The invention discloses a chemical reaction apparatus for removing vanadium from crude TiCl4. The chemical reaction apparatus comprises, in a successively connected manner, a mixing reactor (6), a flash tank (7), a float valve column (11), a cooler (12), and a reflux tank (13), and also includes a crude TiCl4 storage tank (2), a secondary reactor (8), a double tube-sheet heat exchanger (9), a white oil storage tank (1), a metering pump (3), a flow meter (5), and a vanadium-removed TiCl4 storage tank (17). The invention is direct at a conventional technology of using mineral oil to remove the vanadium from crude TiCl4, wherein the crude TiCl4 heated by the double tube-sheet heat exchanger and precisely metered white oil are uniformly mixed according to ratio in the mixer, so that the two components are rapidly reacted in the mixer to remove the vanadium; the mixture then is fed into the flash tank to perform flash; and the TiCl4, with a VOCl3 impurity being removed, is fed into the high-boiling-point impurity removing float valve column in the form of vapor to further remove high-boiling-point impurities in the TiCl4; and the TiCl4 is cooled to produce a TiCl4 inter-product. The method solves the problems of poor quality stability and high energy consumption in a conventional TiCl4 vanadium removal process, has simple device arrangement and stable process control, and is high in vanadium removal efficiency.
Owner:JINCHUAN GROUP LIMITED

Recycled-ABS toughened foam material and preparation method thereof

ActiveCN103509313ALow densityIncrease heat deflection temperaturePlasticizerPolyvinyl chloride
The invention discloses a recycled-ABS (acrylonitrile-butadiene-styrene) toughened foam material. The recycled-ABS toughened foam material is prepared from the following components in parts by weight: 100 parts of recycled ABS, 5-50 parts of polyvinyl chloride, 0.5-15 parts of hollow glass microsphere, 0.5-20 parts of plasticizer, 0.5-20 parts of lubricant, 0.1-20 parts of fire retardant, 0.1-10 parts of smoke suppression agent, and 0.1-5 parts of antioxidant. The invention further discloses a preparation method of the recycled-ABS toughened foam material. The method fully utilizes the recycled ABS, toughens with polyvinyl chloride and improves the flame retardant property, and uses the hollow glass microsphere to fill and foam, so as to avoid the disadvantages that the product is heavy in smell, and the injection molding process is strictly controlled while performing the chemical foaming method; during the production process, the water gap leftover material can be repeatedly processed and utilized for many times. The recycled-ABS toughened foam material prepared from the preparation method is particularly suitable for production of injection products with requirements for high recycled-ABS utilization rate, low production price, good material toughness, light product dead load and flame retardant property.
Owner:HUBEI SUPERE ELECTRIC

Method for preparing high-temperature resistant zinc stearate

InactiveCN101914007AImprove long-term high temperature performanceNo pollution in the processCarboxylic acid salt preparationProcedure AgentsAntioxidant
The invention relates to the technical field of plastic processing aids, in particular to a method for preparing high-temperature resistant zinc stearate. An obtained product is mainly taken as a lubricating mold release agent in the plastic industry for processing at the high temperature. The method comprises the following steps of: putting stearic acid into a reaction kettle under normal pressure to heat the stearic acid to 130 to 180 DEG C; adding zinc oxide and a catalyst in two steps; reacting, adding an antioxidant, stirring and discharging the reaction product, wherein temperature is kept between 130 and 180 DEG C in an entire reaction process; and smashing to obtain a zinc stearate product. The acid value of free stearic acid in the high-temperature resistant zinc stearate prepared by the method is less than 0.5 percent and the whiteness of the product is enhanced greatly after heat is preserved at the temperature of 220 DEG C for 2 hours. Moreover, the zinc stearate has the advantages of stable process control, stable product quality, small fluctuation, no pollution of the used catalyst and the antioxidant on the environment and capability of meeting the environmental protection requirements of energy conservation and emission reduction; and the process has the advantages of simpleness, easy implementation, contribution to expanding the application field of the zinc stearate and very high economic benefit and social benefit.
Owner:DONGGUAN CHNV TECH CO LTD

High-strength normalized container steel with yield strength at 415 MPa level and thermal treatment method thereof

The invention provides high-strength normalized container steel with the yield strength at the 415 MPa level and a thermal treatment method of the high-strength normalized container steel with the yield strength at the 415 MPa level and belongs to the technical field of steel for pressure containers. When the thickness of the high-strength normalized container steel with the yield strength at the 415 MPa level is 6-29 mm, the high-strength normalized container steel with the yield strength at the 415 MPa level comprises, by weight, not larger than 0.2% of C, 0.1%-0.5% of Si, 1.0%-1.3% of Mn, not larger than 0.035% of P, not larger than 0.035% of S, 0.1%-0.18% of V, 0.4%-0.7% of Ni and the balance Fe and inevitable impurities; when the thickness of the high-strength normalized container steel with the yield strength at the 415 MPa level is 30-55 mm, the high-strength normalized container steel with the yield strength at the 415 MPa level comprises, by weight, not larger than 0.2% of C, 0.1%-0.5% of Si, 1.31%-1.6% of Mn, not larger than 0.035% of P, not larger than 0.035% of S, 0.1%-0.18% of V, 0.4%-0.7% of Ni and the balance Fe and inevitable impurities; and when the thickness of the high-strength normalized container steel with the yield strength at the 415 MPa level is 56-75 mm, the high-strength normalized container steel with the yield strength at the 415 MPa level comprises, by weight, not larger than 0.2% of C, 0.1%-0.5% of Si, 1.61%-1.7% of Mn, not larger than 0.035% of P, not larger than 0.035% of S, 0.1%-0.18% of V, 0.4%-0.7% of Ni and the balance Fe and inevitable impurities. The high-strength normalized container steel with the yield strength at the 415 MPa level and the thermal treatment method of the high-strength normalized container steel with the yield strength at the 415 MPa level have the advantages that the mechanical properties of a steel plate can all meet standard requirements, it can be guaranteed that the steel plate has good tenacity, the technology cost is low, and the technology is easy to implement.
Owner:SHOUGANG CORPORATION

Filter material for self-antibacterial and self-disinfecting mask and manufacturing method thereof

The invention belongs to the technical field of daily protection products, in particular to a filter cloth material for a mask with self-antibacterial and self-disinfecting functions and a manufacturing method thereof. The specific implementation process comprises the steps of discharging, degreasing, washing, acid pickling, sensitizing, washing, activating, pre-silvering, silvering, washing, surface modifying, drying, collecting and the like, and proper nano-silver particles can be deposited on the fiber surface after a conventional mask filter material is treated by the method, so that the killing effect on microorganisms such as bacteria or viruses is realized. According to the technology, the defect that an existing mask filter material can only filter particulate matter or droplets but cannot exterminate bacteria or viruses can be overcome; meanwhile, the nano-silver particles and the filter material fibers are firmly combined and are only distributed on the surfaces of the filtermaterial fibers, and compared with other silver-containing filter materials, the nano-silver filter material has the advantages of continuous industrial production, high effective utilization rate ofsilver, strong binding force of the silver particles and the filter material fibers, low manufacturing cost and the like.
Owner:常州微度化工新材料科技有限公司

Complex electron donor for drag reducer polymerization

ActiveCN101735366ASignificantly increased activityUniform heat releasePipeline systemsChemical industryElectron donor
The invention relates to an organic polymer synthesis technique, in particular to a complex electron donor for drag reducer polymerization, belonging to the technical field of chemical industry. The complex electron donor is characterized in that polymerization monomers are added into an anhydrous oxygen-free reaction system, wherein the mixture ratio of laurylene to styrene is 10:1-1:10, or the mixture ratio of laurylene to octylene is 10:1-1:10; the cocatalyst is 0.1%-3% and is obtained by diluting triisobutylaluminum with a refined solvent, wherein the triisobutylaluminum is 20%, the normal heptane is 20%-50%, the rubber solvent oil is 20%-50%, the main catalyst is 0.005%-0.1%, and the complex electron donor is 0.01%-0.5%; and the reaction temperature of the system is -40-10 DEG C, the stirring process is carried out continuously, the reaction time is 24-188 hours, thus a sticky super high molecular weight polymer is obtained. The invention has the advantages of obviously improving the activity of the catalyst system, reducing the consumption of the main catalyst, reducing the consumption of other additives, and the like. In the process of production, the heat release of the catalysis system is uniform, and the process control is stable. By applying the complex electron donor of the invention to long-distance oil transmission pipelines, the pipeline transmission capacity is improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for producing special rutile type titanium white powder for power coating

The invention discloses a method for producing special rutile type titanium white powder for power coating, which comprises the following steps of: preparing slurry of which titanium dioxide concentration is 300 to 400g / l by using bleached metatitanic acid, and adding a calcining auxiliary agent into the slurry; filtering the obtained metatitanic acid, then calcining solid, and grinding the solidto obtain a primary product; preparing titanium dioxide slurry of which titanium dioxide concentration is 650 to 850g / l by using the obtained primary product, adding a wetting agent into the titaniumdioxide slurry, and performing dispersion and grinding; heating the obtained titanium dioxide slurry to between 40 and 90 DEG C, adding dispersant, zircon salt or titanium salt, silicon salt and aluminum salt into the slurry in turn, adjusting the pH value to between 5 and 9, ageing the mixture, and adjusting the pH value to between 7 and 8; and then filtering, washing and drying the mixture, treating the dried product by an organic surface treatment agent, and vaporizing the product to obtain the rutile type titanium white powder. Compared with the prior art, the rutile type titanium white powder obtained by the method has the properties of stable crystal lattice, good dispersion, heat and yellowing resistance, and good oily whiteness, reducing power, covering power and weather resistance and the like; the appearance and properties of the rutile type titanium white powder are close to that of the rutile type titanium white powder prepared by a chlorination process; and the productionmethod has the advantages of easily obtained process raw materials and stable process control.
Owner:NINGBO XINFU TITANIUM DIOXIDE
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products