The application discloses a kind of
methylamine synthesis rectification purification systems, including deaminating unit, extraction unit,
dehydration unit, separation unit and
environmental protection processing unit, the deaminating unit includes deaminating
tower, first overhead condenser, first
reflux tank and first kettle liquid cooler;The extraction unit includes extraction
tower, second overhead condenser, second
reflux tank, second kettle liquid cooler;The separation unit includes first packed rectification column, third overhead condenser and third
reflux tank, second packed rectification column, fourth overhead condenser, fourth reflux tank.In the application, excess
liquid ammonia in material after synthesis reaction can be effectively removed by cooperation of deaminating
tower, first overhead condenser and other equipment, and the influence of
ammonia on subsequent product quality is reduced.Two-way design at the outlet of first reflux tank can flexibly control reflux and production, and improve
deamination efficiency and material utilization.