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60results about How to "Control PH value" patented technology

Production method for electrolytic manganese dioxide

The invention relates to a production method for electrolytic manganese dioxide. The method comprises the following steps of: A. preparing a mixed liquid of crude manganese sulfate and slurry; B. neutralizing the mixed liquid to remove iron; C. carrying out three-time deep purification on the crude manganese sulfate solution including first purification to remove heavy metals, second purification to remove trace element molybdenum and third purification to remove calcium sulfate and magnesium sulfate; D. electrolyzing; E. rinsing including six steps of washing acid with hot water, rinsing with a weak base, rinsing with a strong base, washing base with hot water, backwashing with a diluted acid and rinsing with hot water; F. milling; and G. mixing to obtain an electrolytic manganese dioxide product. According to the invention, low-grade manganese oxide ore is used as a main raw material to prepare a manganese sulfate solution, the manganese sulfate solution is subjected to deep purification treatment to obtain a high-purity electrolyte, high-performance electrolytic manganese dioxide special for mercury-free alkaline cells and automobile power cells can be respectively produced under different electrolysis conditions, and the obtained electrolytic manganese dioxide product has low impurity content and high quality.
Owner:GUANGXI GUILIU CHEM CO LTD +1

Preparation method of 1, 3-butylene glycol

The invention provides a preparation method of 1, 3-butylene glycol. The preparation method comprises following steps: A, acetaldehyde is introduced into a fixed bed reactor, under the effect of a supported type solid basic catalyst, aldol condensation reaction is carried out so as to obtain 3-hydroxybutyraldehyde; and B, 3-hydroxybutyraldehyde is subjected to continuous hydrogenation reaction inthe fixed bed reactor so as to obtain 1, 3-butylene glycol. According to the preparation method, the fixed bed reactor is adopted, at the same time, the supported type solid basic catalyst is adoptedto replace a conventional liquid alkali (such as sodium hydroxide) catalysts, and in the step of hydrogenation reduction, a supported nickel hydrogenation catalyst is adopted. The preparation method is capable of solving problems in the prior art product quality is poor, product yield is low, technology process is complex, and a large amount of waste water and waste residue is generated; aldol condensation quenching step is avoided; side reactions are reduced; relatively high reaction conversion rate and yield are achieved; no neutralizing or desalting process is needed in reaction process; and great improvement of traditional 1, 3-butylene glycol preparation technology is realized.
Owner:DONGYING HI TECH SPRING CHEM IND

Fire retardant finish material and method for finishing fabric using the material

The invention discloses a flame-retardant finishing material and a method for using the material to finish fabric. The flame-retardant finishing material is prepared by adding flame retardant, melamine resin, fiber protecting agent, nonionic penetrating agent and phosphoric acid into water used as a solvent. The method finishes the fabric according to the following steps of controlling the pH value of cloth cover not to exceed 8, performing flame-retardant finishing through a dyeing hot-air padding machine, drying, neutralizing through a washing machine, tentering and preshrinking. The fabric finished by the method has good comprehensive effects in formaldehyde content, fiber strength, hand feeling and other index. In particular, the situation of irregular left, middle and right is effectively avoided by adopting the dyeing hot-air padding machine to pad the flame-retardant finishing material. The construction characteristics of the dyeing hot-air padding machine effectively avoid the migration of the cloth cover in a pre-drying process, allow the finishing material to enter the inside of fiber more easily, and allow the hand feeling of the predried-offloaded fabric to be soft. In addition, during washing neutralization, hydrogen peroxide is used to neutralize cloth cover formaldehyde, thereby effectively controlling the formaldehyde content of the fabric.
Owner:ZHEJIANG MIZUDA TEXTILE PRINTING & DYEING TECH CO LTD

Finished product ammonium nitrate aqueous solution pH value controlling method and device thereof

InactiveCN103497078APH value quickly reaches the standardControl PH valueExplosivesAir compressorAqueous solution
The invention provides a finished product ammonium nitrate aqueous solution pH value controlling method comprising the steps that: temperature and pressure of ammonium nitrate aqueous solution in a storage tank are adjusted; compressed air stirring is carried out; self circulation mixing is carried out by using a circulation conveyor pump; and acid liquid or alkali liquid is added according to the calculation of pH value, such that pH value is adjusted. The invention also provides a controlling device comprising the storage tank. An air distributor is horizontally arranged in the middle in the storage tank. The air distributor is connected with an air compressor arranged outside the storage tank through a first pipe. An acid/alkali tank used for adjusting the pH value is connected in the first pipe. The circulation conveyor pump is connected at an outlet end on the bottom of the storage tank. The outlet end of the circulation conveyor pump communicates with the upper end of the storage tank through a second pipe. The outlet end of the second pipe is positioned at the middle-upper part of the storage tank. With the method and the device provided by the invention, ammonium nitrate aqueous solution pH value can be precisely and rapidly controlled, such that application requirement can be satisfied, and safety during the application process can be ensured.
Owner:ANHUI WANBEI COAL REFCO GRP LTD HANSHAN HENGTAI NONMETALLIC MATERIALS BRANCH

Factory-like recirculating aquaculture system for Hucho taimen

Provided is a factory-like recirculating aquaculture system for Hucho taimen, pertaining to the technical field of aquaculture. The key points of the system are described in that outlet ends of aquaculture ponds communicate with a sedimentation pond through pipelines; the sedimentation pond is located on the side of the aquaculture ponds; a microfiltration machine pond is arranged on the side of the aquaculture pond; additionally, an outlet end of the sedimentation pond communicates with an inlet end of the microfiltration machine pond; the side of the microfiltration machine pond is equippedwith a water return pond; aquaculture water at an outlet end of the microfiltration machine pond and an inlet end of the water return pond as well as in the water return pond enter a floating ball-type biological filter through a pipeline and a water pump; an outlet of the floating ball-type biological filter communicates with a trickling filter through a pipeline and a water pump; the trickling filter is located above an oxygenating tank; the oxygenating tank is disposed on the side of the water return pond; the interior of the oxygenating tank is equipped with an ultraviolet radiation disinfection device; the ultraviolet radiation disinfection device communicates with the oxygenating tank; water in the oxygenating tank communicates with the aquaculture ponds through pipelines. The factory-like recirculating aquaculture system for Hucho taimen is used for factory-like aquaculture of Hucho taimen.
Owner:HEILONGJIANG RIVER FISHERY RES INST CHINESE ACADEMY OF FISHERIES SCI

Factory-like circulating water breeding method for hucho taimen

The invention relates to a factory-like circulating water breeding method for hucho taimen, and belongs to the technical field of aquaculture. The method is characterized in that a hucho taimen circulating water breeding system is connected with a hucho taimen juvenile fish breeding system, juvenile fishes are subjected to tameness and cultivation and parallel screening in sequence, fish fry of different sizes are put into multiple breeding ponds respectively, water drained from the breeding ponds passes through a settling pond and a micro filter tank, and then residual feed and fecal suspensions are filtered and removed; detection is conducted by means of a PH online monitoring system, and the PH value of breeding water is adjusted; the breeding water enters a floating type biofilter through a water pump to remove organic matter such as ammonia nitrogen, nitrate and nitrite; harmful gas such as CO2 is removed in a trickling filter; pure oxygen is increased in an oxygen increasing groove; water obtained after oxygen increasing is subjected to ultraviolet ray disinfection; finally, the breeding water automatically flows into the breeding ponds through an oxygen increasing high-levelwater tank, and the whole hucho taimen circulating water breeding process is completed. The method is used for factory-like hucho taimen breeding.
Owner:HEILONGJIANG RIVER FISHERY RES INST CHINESE ACADEMY OF FISHERIES SCI

Fermentation method capable of reducing content of heavy metal cadmium in rice

The invention discloses a fermentation method capable of reducing the content of heavy metal cadmium in rice. According to the invention, stable fermentation broth is prepared through necessary soaking or fermentation procedure of deep processing of milled early long-grain non-glutinous rice, and the simple and low-cost method using the stable fermentation broth for reducing the content of heavy metal cadmium in rice is provided. A bacterial strain in traditional fermentation broth, e.g., lactobacillus plantarum, lactobacillus fermenti, lactobacillus salivarius and yeast, is employed to improve the nutrient structure in an impregnation solution used in the process of fermentation, so nutrient supply in the process of microbial fermentation can be increased, the growth rate of microbes is promoted, and the number of live bacteria of the microbes in the impregnation solution is increased in a certain period of time. Through improvement of the vitality of lactic acid bacteria, increase of the acidity of the impregnation solution can be accelerated, and impregnation of the acid solution is capable of reducing the content of heavy metal cadmium in rice. In virtue of acid production of the lactic acid bacteria, a complexing bond between the heavy metal cadmium and protein is broken, so cadmium is dissociated; a part of cadmium is adsorbed in virtue of membrane absorption of the microbes at the same time; thus, the content of heavy metal cadmium in rice is substantially reduced after washing.
Owner:GAEA GEM RICE

Wastewater treatment apparatus and control method thereof

The invention relates to the technical field of desulfurization wastewater pretreatment, and discloses a wastewater treatment device, which comprises a configuration system, a storage system, a firstconveying system, a neutralization system, a second conveying system and a control system, and is characterized in that the control system is electrically connected with a first liquid level meter, aconveying pump, a dosing pump and a PH detector; the invention also discloses a control method for the wastewater treatment system, which comprises the following steps: acquiring the pH value in the neutralization tank, comparing the pH value with a preset pH value, and controlling the frequency of the dosing pump according to the pH value comparison result, thereby controlling the amount of limeemulsion added into the neutralization tank by the chemical storage tank; and obtaining liquid level information of the medicine storage box, and controlling the opening and closing of the conveying pump according to the liquid level information. According to the device and the control method, the structure is simple, the operation is easy, the lime emulsion preparation precision and the neutralization tank pH value regulation precision are improved, the labor intensity of personnel is reduced, and meanwhile, the safe and stable operation of a desulfurization wastewater pretreatment system isimproved.
Owner:广州中电荔新热电有限公司

Production method of EDTA

The invention discloses a production method of EDTA (ethylenediaminetetreacetic acid). The production method is characterized by preparing EDTA by taking sodium cyanide, ethanediamine, formaldehyde and liquid caustic soda as raw materials and comprises the following steps: (1) condensation reaction: adding part of a sodium cyanide solution, a liquid caustic soda solution and ethanediamine into a condensation reaction kettle, then starting stirring, then switching on a steam regulating valve, then increasing the temperature to 88-95 DEG C, dropwise adding formaldehyde and the remaining sodium cyanide solution, condensing the tail gas generated in the reaction process and absorbing the tail gas under negative pressure, adding hydrogen peroxide after the reaction is ended, and decolorizing to obtain a condensed material; (2) acidification reaction: adding the condensed material into an acidification reaction kettle, starting stirring, opening an acidification condenser, adding return water into the acidification condenser, adding hydrochloric acid into a reaction kettle till the pH of the reaction kettle is 2.1-4, carrying out centrifugal separation on the precipitated crystal to obtain an EDTA wet material, then carrying out airflow drying to obtain EDTA. Through the production method, the occurrence of side reactions is reduced; the purity of EDTA is improved; the conditions are provided for directly preparing sodium salt; the process steps are simplified.
Owner:潍坊滨海石油化工有限公司

Intelligent management system of domestic wastewater

The invention relates to an intelligent management system of domestic wastewater. The intelligent management system comprises a wastewater settling tank, a wastewater purification tank, a clean water tank and a control system, wherein the wastewater settling tank is used for collecting the domestic wastewater and is connected with the wastewater purification tank through an immersible pump; aluminum polychlorid and a liquid level sensor are placed in the wastewater settling tank; the wastewater purification tank is used for treating harmful substances in the wastewater and is connected with the clean water tank through the immersible pump; microorganisms, zeolite and a liquid level sensor are fed into the wastewater purification tank; the clean water tank is used for storing a water source and conveying the water source to a water utilization place; a water conveying pump, a backflow pump, a liquid level sensor and a PH detector are arranged in the clean water tank; the backflow pump is connected with the clean water tank and the wastewater purification tank; the water conveying pump is connected with a pipeline of the water utilization place; the control system is connected with the liquid level sensors, the PH detector, the immersible pump, the backflow pump, the water conveying pump and an electromagnetic valve; the electromagnetic valve is arranged on the pipeline of the water utilization place. The intelligent management system is mainly used for simple treatment of the wastewater, thus realizing recycling.
Owner:黄科钧

River sewage high-efficiency treatment and purification device for irrigation

The invention discloses a river sewage high-efficiency treatment and purification device for irrigation. The device comprises a water collecting tank, the lower portion of the water collecting tank isprovided with a baffle plate, the upper portion of the baffle plate is in clamping connection with a polypropylene filter bag, the water collecting tank is connected with a water pump through a waterinlet pipe, the water pump is connected to a sterilization chamber through a water outlet pipe, the inner wall of the sterilization chamber is provided with an ultraviolet lamp, the lower portion ofthe sterilization chamber is provided with an activated carbon filter screen, a reaction chamber is formed in the lower portion of the activated carbon filter screen, one side of the reaction chamberis provided with a medicine feeding tube, the side of the medicine feeding tube is provided with blades, the blades are rotatably connected with a motor through a rotating shaft, a reverse osmosis membrane is mounted on one side of the reaction chamber, and a water purification tank is disposed on one side of the reverse osmosis membrane. The device achieves the treatment of river sewage simply and efficiently, prevents waste of water resources, fully and effectively achieves purification treatment of the river sewage, and provides convenience for irrigation of the river sewage.
Owner:FARMLAND IRRIGATION RES INST CHINESE ACAD OF AGRI SCI

Flue gas desulfurization and denitrification optimization control method based on hysteresis model

The invention relates to a hysteresis model-based flue gas desulfurization and denitrification optimization control method, which comprises the following steps of: establishing a power plant desulfurization and denitrification system simulation model through dynamic simulation software according to modular modeling and a control strategy; establishing a first delay time prediction model for the time delay existing in the determination of the pH value of an absorption tower in the desulfurization system, and establishing a second delay time prediction model for the time delay existing in the determination of the concentration of flue gas nitrogen oxide at the inlet of the denitration system through a flue gas online monitoring device CEMS; predicting the concentration of sulfur dioxide at a desulfurization outlet and the concentration of nitrogen oxide at a denitration inlet by adopting a support vector machine model; controlling the slurry spraying amount according to the predicted value of the sulfur dioxide concentration in combination with a first lag time prediction model, and controlling the ammonia spraying amount according to the predicted value of the nitrogen oxide concentration in combination with a second lag time prediction model; and the control parameters are issued to the desulfurization and denitrification system simulation model for intelligent diagnosis.
Owner:STATE GRID HEBEI ENERGY TECH SERVICE CO LTD +2

Production method for electrolytic manganese dioxide

The invention relates to a production method for electrolytic manganese dioxide. The method comprises the following steps of: A. preparing a mixed liquid of crude manganese sulfate and slurry; B. neutralizing the mixed liquid to remove iron; C. carrying out three-time deep purification on the crude manganese sulfate solution including first purification to remove heavy metals, second purification to remove trace element molybdenum and third purification to remove calcium sulfate and magnesium sulfate; D. electrolyzing; E. rinsing including six steps of washing acid with hot water, rinsing with a weak base, rinsing with a strong base, washing base with hot water, backwashing with a diluted acid and rinsing with hot water; F. milling; and G. mixing to obtain an electrolytic manganese dioxide product. According to the invention, low-grade manganese oxide ore is used as a main raw material to prepare a manganese sulfate solution, the manganese sulfate solution is subjected to deep purification treatment to obtain a high-purity electrolyte, high-performance electrolytic manganese dioxide special for mercury-free alkaline cells and automobile power cells can be respectively produced under different electrolysis conditions, and the obtained electrolytic manganese dioxide product has low impurity content and high quality.
Owner:GUANGXI GUILIU CHEM CO LTD +1
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