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64results about How to "Control precipitation" patented technology

7000 series aluminum alloy material and preparation method thereof

The invention relates to a 7000 series aluminum alloy material and a preparation method thereof. The aluminum alloy material has alloy components of, by weight: 7.6-11.0% of Zn, 1.2-3.0% of Mg, 1.3-2.6% of Cu, 0.04-0.30% of Zr, 0.10-0.60% of Cr, no more than 0.08% of Si, no more than 0.10% of Fe, no more than 0.10% of Ti, no more than 0.15% of total other impurities (wherein the content of single other impurity is no more than 0.05%), and balance of Al. The alloy elements Zr and Cr can be added optionally or simultaneously. The materials are prepared according to the alloy composition; the raw materials are molten; in-furnace refining and standing are carried out; and the material is cast into alloy ingots with required specifications. The alloy ingots are subjected to a preferable graded uniformization process, and is forged or extruded, such that the alloy ingots are molded; the molded materials are subjected to graded solid solution treatment, and are quenched; and artificial forced aging is carried out, such that the material can be processed into parts. The microstructures of the material are uniform, and the property of the material is stable. The ultimate tensile strength of the material can be more than 750MPa. The extensibility of the material is higher than 10%. The T-L direction KIc of the material reaches 28MPam1 / 2.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Biomass three-section type entrained flow bed gasification technology with function of waste heat utilization

The invention discloses a biomass three-section type entrained flow bed gasification technology with the function of waste heat utilization, which relates to the technical field of energy chemical technology. The gasification technology is realized in a way that: carbon powder, pyrolysis gas and oxygen, which are generated after the biomass is pyrolyzed, enter an entrained flow bed to obtain synthetic gas through gasification, and the energy of the gasification waste heat is transferred to water by a heat exchanger of a gasifier, thereby producing superheated steam. The gasifier of the entrained flow bed is divided into a high-temperature entrained flow bed section, a high-temperature heat exchanger section and a low-temperature heat exchanger section, wherein the high-temperature entrained flow bed section adopts a dry ash extraction entrained flow bed gasification technology, and the temperature of the synthetic gas at the outlet is 1280-1320 DEG C; at the high-temperature heat exchanger section, the temperature of the synthetic gas at the inlet is 1280-1320 DEG C, the temperature at the outlet is 580-600 DEG C, a shock chamber and a high-temperature superheater are arranged in the high-temperature heat exchanger section, and the synthetic gas enters the shock chamber at the temperature of 1000-1100 DEG C and leaves at the temperature of 700-800 DEG C; and at the low-temperature heat exchanger section, the temperature of the synthetic gas at the inlet is 580-600 DEG C, the temperature of the synthetic gas at the outlet is 220-230 DEG C, and a low-temperature superheater and a coal economizer are arranged in the low-temperature heat exchanger section. The invention is used for high-efficiency gasification of biomass.
Owner:ZHONGJIEHUAN BEIJING ENERGY TECH

Method for removing phosphorus from high-concentration phosphorus-containing wastewater

The invention discloses a method for removing phosphorus from high-concentration phosphorus-containing wastewater. The method includes regulating a pH (potential of hydrogen) value of the high-concentration phosphorus-containing wastewater with the total phosphorus concentration of 5000-25000 ppm, calcifying the high-concentration phosphorus-containing wastewater, removing the phosphorus from the high-concentration phosphorus-containing wastewater to obtain wastewater and then feeding the wastewater into a wastewater reaction tank; adding flocculating agents into the wastewater reaction tank after reaction is completely carried out and forming solid and liquid mixtures; separating solid from liquid in the solid and liquid mixtures to obtain phosphorus paste and clear liquid; treating the clear liquid and then feeding the clear liquid into biochemical treatment working procedures. The method has the advantages that the phosphorus can be continuously removed at steps of pH regulating, calcification and phosphorus removal, treatment by the aid of the wastewater reaction tank and the like, accordingly, the treated high-concentration phosphorus-containing wastewater with the total phosphorus concentration of 5000-25000 ppm can reach wastewater standards under biochemical treatment conditions, filter residues and the phosphorus paste which are obtained in phosphorus removal procedures can be used as raw materials for producing phosphorus fertilizers, technological procedures are simple, the method is low in investment cost and little in environmental pollution, and the like.
Owner:SICHUAN FOURSTAR BIOTECH RANDD CORP

Control method of coating performance surface quality of double-phase steel cold-rolled high-strength automobile board

The invention discloses a control method of coating performance surface quality of a double-phase steel cold-rolled high-strength automobile board, which comprises smelting, continuous casting, hot rolling, descaling, acid rolling, continuous annealing and leveling. The descaling process uses a three-stage descaling process, wherein the descaling position comprises descaling after a heating furnace, descaling before rough rolling and descaling before finish rolling, the descaling pressure at each descaling point is greater than or equal to 24MPa, the rough rolling is reciprocating rolling, therolling is carried out for 5 times, and high-pressure water descaling is carried out for every time. By adjusting and optimizing a whole process production process, including controlling the chemicalcomposition of a continuous casting blank, improving the heating and cooling system of the continuous casting, hot rolling, and cold rolling, controlling the hot rolling and descaling processes and cold rolling and acid rolling processes, controlling the roughness of a leveled steel strip, and the like, the surface quality of the double-phase steel cold-rolled automobile board is improved, the element enrichment on the surface of the steel board is inhibited, the quality of a phosphating film is improved, the coating performance of the double-phase steel cold-rolled high-strength automobile board and the anti-corrosion performance of the double-phase steel cold-rolled high-strength automobile board after being coated are improved.
Owner:TANGSHAN IRON & STEEL GROUP +1

Synthesis method of polyvinyl butyral resin

ActiveCN111499780ASteady precipitationImprove uniformityOrganic acidPolyvinyl alcohol
The invention discloses a synthesis method of polyvinyl butyral resin, and belongs to the field of high polymer material preparation. The method comprises the following steps: dissolving polyvinyl alcohol in deionized water, adding an emulsifier, adding n-butyraldehyde to react with an organic acid, then adding an inorganic acid, carrying out a heating reaction, performing neutralizing with an alkaline solution, adjusting the pH value of the reaction solution to 7-9, carrying out solid-liquid separation, treating the solid resin with a stabilizer solution, washing, filtering, and performing drying to obtain the polyvinyl butyral resin. The condensation reaction of polyvinyl alcohol and n-butyraldehyde is catalyzed step by step by adopting organic acid and inorganic acid; the early condensation reaction speed is effectively controlled, resin can be stably separated out from a water phase, the main chain acetal uniformity is improved, inorganic acid is adopted for catalysis in the middleand later periods of the reaction, the condensation reaction speed can be increased, the conversion rate of n-butyraldehyde is increased, and the acetal degree of the resin is improved. The synthesismethod is simple, high in operability and easy for industrial production. The resin can be used in the fields of safety glass, coatings, adhesives and the like.
Owner:HENAN ACADEMY OF SCI CHEM RES INST CO LTD

Mn13 high-manganese steel welding technology

The invention discloses an Mn13 high-manganese steel welding technology, which comprises the following steps that: 1) processing a reasonable welding groove on a butt joint plate material; 2) carryingout transition layer welding, adopting a direct current reverse polarity, immediately carrying out water cooling and hammering after a welding line of which the length is 50-100mm is welded for eachtime, measuring the temperature of a position, which is 10-20mm far away from the groove, of a welded material, cooling to be below 50DEG C, and continuously welding after a surface is cleaned, wherein a welding way is SMAW (Shielded Metal Arc Welding), welding current is 110-130A, electric arc voltage is 35-45V, a welding speed is 150-250mm / min, a cooling way is air cooling, the temperature of alayer channel is less than or equal to 50DEG C, and the thickness of the transition layer is 4-6mm; and 3) welding a filling welding line, adopting argon-rich gas shielded welding for welding, carrying out air cooling to be below 150DEG C after one pass is finished, and carrying out next-pass welding, wherein low-alloy welding wires are adopted as a welding material, welding current is 220-260A, electric arc voltage is 28-31V, a welding speed is 400-450mm / min, a cooling way is air cooling, and the temperature of a layer channel is less than or equal to 150DEG C.
Owner:BAOSHAN IRON & STEEL CO LTD

Wear-resistant steel and production method thereof

The invention discloses wear-resistant steel and a production method thereof, and relates to the technical field of steel production, and the wear-resistant steel comprises the following chemical components in percentage by mass: 0.10 to 0.45 percent of C, 0.20 to 0.55 percent of Si, 0.50 to 1.50 percent of Mn, less than or equal to 0.015 percent of P, less than or equal to 0.003 percent of S, less than or equal to 0.060 percent of Nb, less than or equal to 0.030 percent of V, 0.008 to 0.025 percent of Ti, 0.20 to 1.00 percent of Cr, less than or equal to 1.80 percent of Ni, less than or equal to 0.50 percent of Mo, 0.025 to 0.055 percent of Al, 0.0010 to 0.0030 percent of B, 0.0010 to 0.0018 percent of Mg, less than or equal to 0.0045 percent of N and the balance of Fe and inevitable impurities. On the premise that the high-strength martensite structure of the wear-resistant steel plate is guaranteed, through quantitative treatment of microalloying elements, the number and the size of carbonitride are reduced, the cooling speed and the austenite temperature of a casting blank are regulated and controlled, a secondary quenching optimization process is adopted, structure grains are refined, structure stress is eliminated, and the wear resistance of the wear-resistant steel plate is improved. The problem of delayed cracks of wear-resistant steel in the cutting and grinding process of casting blanks and steel plates is solved.
Owner:NANJING IRON & STEEL CO LTD

Paste for light receiving surface electrode of solar cell, manufacturing method and solar cell unit

The invention provides a paste for a light receiving surface electrode of a solar cell, wherein the paste can form an electrode that has high binding strength with a substrate and low contact resistance and furthermore high output can be obtained on condition that an LDE substrate is used, and a manufacturing method of the paste, and a solar cell unit with high output. The conductive paste for forming the light receiving surface electrode comprises leadless tellurite glass with various compositions. Various lead-containing additives and an additive with high-melting-point metal are mixed in the paste. Preferably the lead is carried in appropriate methods of false firing, chemical method, mechanical method, etc. Therefore if the electrode of the light receiving surface is formed through a fire-through manner, an erosion surface which appropriately has recesses and projections can be obtained. Therefore a requirement for a high electric characteristic and high binding strength can be satisfied. Furthermore, because the light receiving surface electrode (28) contains high-melting-point metals and lead, recombination is suppressed. Therefore high output can be obtained even the LDE substrate is equipped.
Owner:NORITAKE CO LTD

Method for eliminating white structure of high-purity pig iron for hydrogen-based smelting reduction casting and pig iron

The invention discloses a method for eliminating a white structure of high-purity pig iron for hydrogen-based smelting reduction casting. The method comprises the characteristics of the high-purity pig iron for casting produced by a hydrogen-based smelting reduction non-blast furnace ironmaking process, and comprises primary inoculation of pig iron liquid, desulfurization, secondary inoculation and external refining degassing (O, N, H) treatment. The high-purity pig iron for casting produced by the hydrogen-based smelting reduction process is low in silicon, phosphorus and titanium, the primary inoculation treatment comprises the step of adding a silicon-barium-calcium inoculant and an auxiliary agent into molten iron, and the secondary inoculation treatment comprises the step of adding a strontium-silicon inoculant into the molten iron to strengthen elements promoted to be graphitized in the molten iron, so that the graphitization capacity of the molten pig iron is enhanced, carbon atoms are separated out, and a white structure generated by carbon and iron compounds formed in the solidification and crystallization process is avoided. By means of the technical scheme, the problem of the high-purity pig iron white structure for casting produced through an existing hydrogen-based smelting reduction process is solved.
Owner:内蒙古赛思普科技有限公司

Device and process for producing 1-octylene by ethylene selective oligomerization

The invention provides a device and a process for producing 1-octylene by ethylene selective oligomerization, and relates to the field of chemical industry. The device comprises an oligomerization reactor, the circulation pipeline is led out from the top of the oligomerization reactor and returns to the oligomerization reactor, a gas compression device, a heat exchanger and a gas-liquid separator are sequentially arranged on the circulation pipeline, the gas compression device is connected with the top of the oligomerization reactor, and a gas phase outlet and a liquid phase outlet of the gas-liquid separator are respectively communicated with the inside of the oligomerization reactor. A solvent used in the process can comprise a low-boiling-point component and a high-boiling-point component, the low-boiling-point component is selected from C3-C5 hydrocarbons, and the high-boiling-point component is selected from C6-C10 hydrocarbons. According to the device and the process, reaction heat can be effectively and stably removed, precipitation of polyethylene and oligomer generated in the reaction on a heat exchange wall surface is reduced, the cost of a cooling medium is reduced, meanwhile, the reaction temperature is stably controlled, and the reaction efficiency and selectivity are improved.
Owner:浙江智英石化技术有限公司
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