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87results about How to "Larger than the area" patented technology

Fluorine-containing metal coating on surface of NdFeB rare-earth permanent magnet and preparation method of fluorine-containing metal coating

The invention discloses a fluorine-containing metal coating on the surface of an NdFeB rare-earth permanent magnet and a preparation method of the fluorine-containing metal coating, and belongs to the technical field of anticorrosion surface treatment. The fluorine-containing metal coating has the thickness of 5-40 microns and is prepared from polytetrafluoroethylene, solid powder and adhesive according to the mass ratio of (1-30):(2-30):(20-40). The preparation method includes the steps of firstly, preprocessing the surface of the NdFeB rare-earth permanent magnet through an oil removal and acid pickling or sand blasting method; secondly, preparing the coating through a centrifugal soaking and throwing or spraying method. Polytetrafluoroethylene contained in paint for preparing the coating has excellent corrosion resistance, and the corrosion resistant capacity of the surface of the NdFeB rare-earth permanent magnet can be improved; in the coating process, no acid bath is used, the fresh surface of the magnet is not damaged after preprocessing, and the surface adhesion force between the coating and the magnet can be effectively improved; no acid waste liquid exists, the environment is not polluted, and the preparation method belongs to the green and environment-friendly coating process.
Owner:NORTHEASTERN UNIV

Method for preparing liquid chromatography monolithic column based on metal-organic frameworks

A method for preparing a liquid chromatography monolithic column based on metal-organic frameworks. The porous MOFs (metal-organic frameworks) and organic polymer monolithic materials are used as separation media, and the stainless steel liquid chromatography monolithic column is prepared by means of in-situ polymerization. Firstly, the MOFs are prepared by means of self-assembly reaction of different metal centers and organic ligands, activated at a certain temperature and ultrasonically dispersed in solvents to obtain suspending liquid of the MOFs. Secondly, the suspending liquid is added into precursor solution, and the doped monolithic column is prepared by means of thermal-initiation polymerization. Thirdly, pore-foaming agents in the MOFs monolithic column are flushed at a high flow rate by a liquid high-pressure pump, and then the liquid chromatography monolithic column can be prepared. The method has the advantages that the superiority of double separation of the MOFs and the monolithic column is integrated, the shortcomings of large backpressure, high consumption of the separation media, complicated filling and the like of a traditional packed column are overcome, the types of the MOFs serving as separation media are expanded, and large-scale popularization and application are facilitated.
Owner:NANKAI UNIV

Preparation method of Ni-based catalyst modified by aid Pt supported by multi-wall carbon nanotube as carrier and application

The invention discloses a preparation method of a Ni-based catalyst modified by an aid Pt supported by multi-wall carbon nanotubes as a carrier and application. The preparation method comprises the following steps: firstly, performing acid modification on multi-wall carbon nanotubes by using nitro-sulfuric acid; by taking the multi-wall carbon nanotubes as a carrier, putting precursor salts of platinum and nickel according to the multi-wall carbon nanotubes to hexachloroplatinic acid hexahydrate and nickel nitrate hexahydrate according to a mass ratio of (5-10):(0.1-0.5):(5-10); further addingdeionized water, performing ultrasonic stirring, drying, and performing roasting and reduction, thereby finally obtaining an expected catalyst Pt-Ni/MWCNT. The catalyst prepared by using the method is low in cost, economic and effective, good in universality, good in environmental-friendliness, free of equipment corrosion and good in circulation property, and is relatively high in activity and relatively high in p-aminophenol selectivity under a relative gentle reaction condition in a process that p-aminophenol is prepared from nitrobenzene through one-step hydrogenation rearrangement, the production conditions can be improved, the production cost is reduced, and the product quality is improved.
Owner:XIANGTAN UNIV

Composite nanofiber air filtration material and preparation method thereof

The invention relates to a composite nanofiber air filtration material and a preparation method thereof. The material comprises a nanometer polyvinyl alcohol fiber layer and an interweaving layer of nanometer polyvinyl alcohol fibers and polyacrylonitrile fibers, the air filtration material in the four layer structure of the nanometer polyvinyl alcohol fiber layer and the interweaving layer of the nanometer polyvinyl alcohol fibers and the polyacrylonitrile fibers in cross distribution is obtained through one-time electrostatic spinning, the diameter of the polyvinyl alcohol fiber layer ranges from 400 nm to 1,000 nm, the diameter of the electrostatic spinning polyacrylonitrile fibers ranges from 150 nm to 500 nm, the porosity ranges from 75% to 90%, the average pore size ranges from 0.4 mu m to 6 mu m, and crosslinking treatment is performed. The performance that the composite nanofiber air filtration material is not prone to layering and better mechanical properties can be obtained, the filtration efficiency to NaCl aerosol with number median diameter of 75 nm ranges from 99.94% to 99.99%, and the pressure is reduced to be 180-600 Pa. The material is particularly suitable for fields such as personal protective products, air quality testing equipment and air purification devices.
Owner:JILIN UNIV

Decontaminable water-permeable concrete and preparation method thereof

The invention discloses decontaminable water-permeable concrete with strong decontamination ability and high mechanical strength and a preparation method thereof. The decontaminable water-permeable concrete is composed of the following components in percentages by mass: 75% to 80% of aggregate, 13% to 17% of cement, 3% to 6% of water, 1% to 2% of fly ash, 0.34% to 0.73% of a reinforcing agent and0.05% to 0.09% of a water reducing agent, wherein 10% to 20% of the aggregate is replaced by ceramsite as an improvement. The preparation method for the decontaminable water-permeable concrete comprises the following steps: (10) aggregate moisturizing: a step of adding all aggregate including the ceramsite and 50% of the water into a stirrer, and carrying out stirring for 30 s so as to moisturizethe surface of the aggregate; (20) material mixing: a step of adding the cement, the fly ash, the reinforcing agent and the water reducing agent into surface-moisturized aggregate, and carrying out stirring for 60 s; and (30) material discharging: a step of adding remained water into the stirrer, carrying out uniform mixing under stirring, filling a material by layers, carrying out intercalation tamping for molding, and carrying out curing so as to obtain the decontaminable water-permeable concrete.
Owner:YANGZHOU UNIV

Method and device for reinforcing cane juice neutralization reaction by hydraulic micro-oscillation

The invention relates to a method for reinforcing cane juice neutralization reaction by hydraulic micro-oscillation, which is applicable to a clarification technique of cane juice or liquid glucose by a sulfurous process. The method comprises the steps of preliming, primary heating, stoving neutralization, hydraulic micro-oscillation reinforced cane juice neutralization reaction, secondary heating and settling. The hydraulic micro-oscillation reinforced cane juice neutralization reaction is implemented in a way that: the cane juice or neutralized juice subjected to stoving neutralization reaction is pumped into a hydraulic micro-oscillation reinforced cane juice neutralization reaction device to subjected to hydraulic micro-oscillation reinforced cane juice neutralization reaction, and enters the steps of secondary heating and settling. The hydraulic micro-oscillation reinforced cane juice neutralization reaction device for implementing the method can change the size of the flow section of the cane juice or liquid glucose in the flowing process: the device is a cylindrical container or tubular container with inconsistent cross-sectional area. The method and device provided by the invention can reinforce the cane juice neutralization reaction, and enhance the purity of the clear juice by more than 1%; and the consumption of lime and sulfur is reduced by more than 20%.
Owner:GUANGXI UNIVERSITY OF TECHNOLOGY +1

Modified biochar and method for repairing heavy metal pollution of soil by using modified biochar

The invention relates to biochar, in particular to modified biochar and a method for repairing heavy metal pollution of soil by using the modified biochar. The modified biochar is prepared by the following method: S1, air-drying corn straws; s2, crushing the corn straws to obtain straw powder; s3, adding water into the straw powder, and stirring until the water content of the straw powder is 20-30%; s4, feeding the straw powder into a carbonization furnace, and closing the carbonization furnace; s5, introducing carbon dioxide gas, and emptying air in the carbonization furnace; s6, increasing the temperature to 100 DEG C, and performing heat preservation for 15-30 min; s7, increasing the temperature to the carbonization temperature, wherein the carbonization temperature ranges from 680 DEG C to 750 DEG C, the carbonization time ranges from 1 h to 2 h, and obtaining the modified biochar; s8, cooling to room temperature after carbonization is finished; and S9, heating the modified biochar into a ball mill, and grinding to obtain the modified biochar powder with the particle size of 10-20nm. The modified biochar has larger specific area and pore volume, richer oxygen-containing functional groups and stronger pollutant adsorption capacity.
Owner:江苏苏环生态科技有限公司

Method for synthesizing porous oxide microspheres with vanillin alloy complex as precursor

ActiveCN110054211AImprove the shortcomings of photocatalysis such as insufficient specific surface areaImprove shortcomings such as insufficient specific surface areaHybrid capacitor electrodesCopper oxides/halidesMicrosphereCopper oxide
The invention discloses a method for synthesizing porous oxide microspheres with a vanillin alloy complex as a precursor. The method includes the steps of firstly, synthesizing a vanillin alloy complex (Zn-MOF material or Cu-MOF material) by solvothermal reaction, and roasting the vanillin alloy complex which serves as the precursor in the presence of air so as to obtain a porous oxide (zinc oxideor copper oxide material). The obtained porous zinc oxide material, with the average particle diameter of 2-4 micrometers, has a hexagonal wurtzite structure, is high in specific surface area, and can effectively improve the defects that a traditional zinc oxide material is easy to agglomerate and is limited in photocatalytic performance due to insufficient exposed active sites and specific surface area. The obtained porous copper oxide microspheres with the average particle size of 1-5 micrometers are monoclinic, has a large specific surface area, and can effectively improve the defects thata traditional copper oxide material on a super capacitor is insufficient in specific surface area and low in energy density. The method is simple, low in cost and suitable for popularization and application.
Owner:WUHAN INSTITUTE OF TECHNOLOGY
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