The invention relates to a preparation method of an
antimony pentoxide composite
powder. The preparation method comprises the following steps: firstly,
antimony trioxide is taken for refining; then the refined
antimony trioxide dry powder is added into water, then creatinol-o-
phosphate as a stabilizer and oxydol are added for oxidation
reflux reaction, after the reaction, a reacting liquid is taken for
dialysis for 2 to 3 times, redundant creation o-
phosphate is removed, and an
antimony pentoxide hydrosol is prepared; finally, the prepared
antimony pentoxide hydrosol is added with
zeolite powder, the mixture is stirred and then left to stand, precipitate is obtained through
centrifugation, and the precipitate is filtered and dried so as to obtain the
antimony pentoxide composite
powder. The preparation method provided by the invention uses the creatinol-o-
phosphate as the stabilizer, and the creatinol-o-phosphate contains a plurality of hydroxies and two inflaming retarding elements N and P, so that the stabilizing effect is good, the
flame-retardant effect of the
colloid of antimony
pentoxide is improved, a
zeolite powder is adopted for adsorbing the
colloid of antimony
pentoxide, so as to prepare the antimony pentoxide-
zeolite powder composite powder, during the preparing process, the problem of much loss of antimony pentoxide
dry powder during the
drying process caused by relatively fine antimony pentoxide
dry powder can be solved.