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83results about How to "Effective control of content" patented technology

Preparation method of active graphene/active carbon composite electrode plate

The invention particularly relates to a preparation method of an active graphene/active carbon composite electrode plate, and belongs to the technical field of new energy storage devices. The preparation method comprises the following steps: mixing reduced graphene oxide with a pore-forming agent evenly at the mass ratio of 1 to (5-10); carrying out equivalent-volume impregnation in water for 8-24 hours, carrying out activating treatment at 600-1,000 DEG C in an inert atmosphere for 0.5-4 hours after drying, and cleaning and drying the product to obtain active graphene after activating; carrying out modified treatment on the active graphene; mixing the modified active graphene with the active carbon at the mass ratio of (10%-90%) to (10%-90%), mixing an active graphene/active carbon mixture, a conductive agent and an adhesive at the mass ratio of (75%-93%) to (2%-10%) to (5%-15%) and then laminating the mixture to form a carbon film; and pasting the carbon film and a current collector through a conductive adhesive, and carrying out heating and solidifying to obtain the active graphene/active carbon composite electrode plate. According to the preparation method of the active graphene/active carbon composite electrode plate, the thickness and the density of the final electrode plate are controllable; continuous mass preparation can be carried out; the capacity can also be improved when the prepared electrode plate is applied to a super capacitor; the internal resistance is reduced; the power density is improved; and the voltage endurance capability of the super capacity is improved.
Owner:NINGBO CRRC NEW ENERGY TECH CO LTD

Preparing method for cyclohexane-1,2-dibasic diformate

The invention relates to the field of hydrogenation for preparing cyclohexane-1,2-dibasic diformate, and discloses a preparing method for cyclohexane-1,2-dioctyl phthalate dibasic ester. The method comprises the steps that firstly, hydrogenation raw materials containing phthalic acid dibasic ester and H2 are subjected to first contact in a main hydrogenation reactor in the presence of a first catalyst, and first gas-liquid mixing fluid is obtained; secondly, the first gas-liquid mixing fluid is subjected to gas-liquid separation; thirdly, hydrogen is injected into main hydrogenation reaction liquid through holes with the average hole diameter being the nanometer size, the main hydrogenation reaction liquid is separated out in the second step, and second gas-liquid mixed fluid is obtained; fourthly, the second gas-liquid mixed fluid is subjected to second contact in a rear hydrogenation reactor in the presence of a second catalyst, and third gas-liquid mixed fluid is obtained; and fifthly, the third gas-liquid mixed fluid is subjected to gas-liquid separation. The method has the beneficial effects that the raw material conversion rate, the product selectivity and the cis-structure product content are high.
Owner:HUNAN CHANGLING PETROCHEM SCI & TECH DEV CO LTD

Affinity purification process capable of efficiently improving resolution of polymer separation

The invention provides a novel affinity purification process capable of efficiently improving the resolution of polymer separation. The process specifically includes the following steps that 1, affinity packing is treated, and sampling is performed; 2, drip washing is conducted, wherein a drip washing 2 buffer solution and a drip washing 3 buffer solution are used for drip washing a chromatographic column; 3, elution is conducted, wherein an eluting buffer solution with the pH of 2.8-5.7 or an eluting buffer solution including an additive is used for eluting products, and then the products arecollected; 4, in addition to the elution pH condition and an additive, the development of an elution method is optimized from linear gradient elution to one-step elution. The process breaks through atraditional thinking that an affinity step serves as a coarse purification step. According to the process, polymers can be effectively removed through the affinity step, the effect of fine purifyinga target protein is achieved, the process is amplified by a 15-200 L process and verified by a virus removal process, has a wide application range and can be widely used for antibody proteins, and thus strong technical support is provided for effective control over the content of the polymers in antibody drugs.
Owner:SHANGHAI WUXI BIOLOGIC TECH CO LTD

Method for preparing polyester-nylon composite fibers by melt direct spinning

The invention relates to the field of nylon materials, and discloses a method for preparing polyester-nylon composite fibers by melt direct spinning. The method comprises the following steps of 1) burdening, specifically, heating and mixing caprolactam, an end-capping reagent, water and a catalyst to obtain a mixture; 2) ring opening; 3) pre-polycondensation, specifically, carrying out a pre-polycondensation reaction and devolatilization; 4) final polycondensation, specifically, carrying out a final polycondensation reaction and devolatilization; 5) devolatilizing before spinning; and 6) spinning, specifically, directly conveying nylon melt and polyester melt which are devolatilized before spinning to a composite spinning assembly, performing extruding, cooling, oiling, stretching and winding to obtain the polyester-nylon composite fibers. By means of the method, direct spinning after nylon melt polymerization can be achieved, slices do not need to be prepared in advance, and the content of hot water extractables and cyclic dimers in the nylon melt can be effectively controlled; and composite spinning is carried out on the nylon melt and the polyester melt to obtain the polyester-nylon composite fibers in different composite forms.
Owner:ZHEJIANG HENGYI PETROCHEMICAL RES INST CO LTD

Method for extracting and recycling zinc from beneficiation tailing water of lead silver residues of zinc hydrometallurgy

ActiveCN105838886ASmall and uniform filter poresPrevent breakthroughProcess efficiency improvementMagnesiumFilter paper
The invention discloses a method for extracting and recycling zinc from beneficiation tailing water of lead silver residues of zinc hydrometallurgy. The method comprises the steps of (1) removing impurities from beneficiation tailing water of lead silver residues of zinc hydrometallurgy, adding a beneficiation reagent, and filtering; (2) adding industrial magnesium hydroxide, and stirring; (3) carrying out two-stage counter-current extraction on the slurry through adopting organic phases; (4) carrying out two-stage counter-current washing on loaded organic phases through adopting a diluted acid solution; (5) carrying out reverse extraction on water washing organic phases through adopting a waste electrolyte; and (6) deoiling a stripping solution. According to the method, the washing efficiency is effectively improved, inclusion transmission of cadmium impurities is reduced, and the loss of the organic phases in a water phase outlet is reduced; and filtration is carried out through a filter press adopting silicone oil filter paper as a medium, the stripping solution of which the oil content is 0.5 ppm or below is stably produced, and the method has important meaning for stable electrolytic production.
Owner:CHIFENG ZHONGSE ZINC IND CO LTD

Xylose-mother-liquid continuous full-filling impunity-removing device and method

The invention relates to a xylose-mother-liquid continuous-full-filling impunity-removing device and method. The device comprises an alkali adding unit, a continuous full-filling unit, a discharging control unit, a CO2 feeding station, a steam station and a tank after full filling, wherein the alkali adding unit is used for adding Ca(OH)2 alkali liquor into xylose mother liquid; the continuous full-filling unit is used for introducing CO2 fed by the CO2 feeding station into the xylose mother liquid added with alkali for full filling mixing to remove colloid and colloid impurities in the xylosemother liquid; the discharging control unit is used for introducing the CO2 fed by the CO2 feeding station and steam delivered from the steam station into the xylose mother liquid after full filling,and the pH value of the xylose mother liquid after full filling is controlled and stabilized; the tank after full filling is used for collecting and temporarily storing the xylose mother liquid afterfull filling and impunity-removing to be ready to enter the next process. The invention also discloses a method with the device. According to the xylose-mother-liquid continuous-full-filling impunity-removing device and method, the pH of the xylose mother liquid is continuously adjusted and stabilized, feeding and discharging are continuous, the automatic degree of the device is high, continuousuninterrupted production is achieved, and the production efficiency can be improved.
Owner:ZHEJIANG HUAKANG PHARMA +1

Highland barley oatmeal as well as preparation method thereof

InactiveCN103330140AIncreased beta-glucan contentEffective control of contentFood preparationBiotechnologyBARLEY BRAN
The invention discloses highland barley oatmeal as well as a preparation method thereof. The highland barley oatmeal comprises highland barley oatmeal raw pieces; the highland barley oatmeal raw pieces are dried up after being sprayed by a highland barley bran water extraction liquid, the process is repeated until the beta-glucan content in the highland barley oatmeal is greater than 45wt%; the highland barley bran water extraction liquid is obtained in a manner that obtaining a from highland barley bran is subjected to a water extraction method to obtain a filter liquid, and the filter liquid is subjected to concentration, wherein the beta-glucan content is 17-60wt%. The method for preparing the highland barley oatmeal comprises the following steps of: 1, preparing a highland barley oatmeal concentration liquid by adopting the water extraction method, crushing the highland barley oatmeal, adding water into the crushed highland barley oatmeal, decocting to obtain the filter liquid, and concentrating the filter liquid for future use; 2, spraying the highland barley oatmeal concentration liquid on the highland barley oatmeal raw pieces, and drying; 3, repeating the step 2 until the beta-glucan content in the highland barley oatmeal is greater than 45wt% and less than 60wt%, thereby obtaining a finished product.
Owner:TIBET MODERN AGRI

One-dimensional iron-based wave-absorbing material derived from a metal organic framework, and preparation method thereof

ActiveCN113620349AFacilitate augmentation and optimizationHigh complex permeabilityMagnetic/electric field screeningFerrous oxidesFrequency bandBroadband
The invention discloses a one-dimensional iron-based wave-absorbing material derived from a metal organic framework, and a preparation method thereof, and belongs to the technical field of microwave absorbing materials. A one-dimensional metal organic framework (Fe-bdc) is used as a precursor, and a process of air oxidation and hydrogen reduction is adopted, so that the content and morphology of magnetic components in the derived one-dimensional iron-based wave-absorbing material are regulated and controlled, optimization of electromagnetic parameters is promoted, and effective absorption of broadband electromagnetic waves is realized under the condition of low thickness. From the aspect of components, non-magnetic components are effectively removed in the oxidation process, and the content of each magnetic component can be effectively adjusted in the reduction process. From the aspect of the structure, the one-dimensional bead-shaped structure has relatively strong shape anisotropy, can promote the formation of a magnetic conductive path and a conductive path, and is beneficial to enhancing the electromagnetic attenuation capability. The effective absorption frequency band of the one-dimensional iron-based wave-absorbing material can reach 3.52 GHz under the condition that the thickness is only 1.2 mm, and the one-dimensional iron-based wave-absorbing material shows excellent low-thickness and broadband wave-absorbing characteristics. The method does not need complex equipment, the cost is low, and the product consistency is high.
Owner:HEFEI UNIV OF TECH
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