138 results about "Reactive magnetron" patented technology

The invention relates to an adjustment method of a bimetal gate work function, which mainly comprises the following steps: (1) growing a ultrathin interface oxide layer or a nitrogen oxide layer through rapid thermal oxidation; (2) alternately sputtering and depositing gate dielectrics with a high dielectric constant (K) on the ultrathin interface oxide layer through reactive magnetron sputtering; (3) after the gate dielectrics with the high K are deposited, carrying out rapid thermal annealing; (4) depositing metal nitride gates through reactive magnetron sputtering; (5) injecting metal ions for doping the metal nitride gates; and (6) after metal gate electrodes are formed by etching, carrying out rapid thermal annealing to drive the metal ions onto the interfaces of the metal gates and the gate dielectrics with the high K. The method can be simply and easily realized, has good thermal stability and capacity of adjusting a metal gate work function, is completely compatible with the CMOS process, and is convenient for industrialization of integrated circuits.

The invention relates to a zirconia and alumina gradient composite coat and a production method thereof. The coat comprises composite layers composed of zirconia and alumina according to different mass percentage ratios, and the composite layers composed of zirconia and alumina are laid on a steel substrate. The composite coat can be produced through a metal organic matter chemical vapor deposition technology or a reactive magnetron co-sputtering technology. The zirconia and alumina gradient composite coat combines the hydrogen resistance and penetration characteristics of zirconia and alumina, and the thermal expansion coefficient of the composite coat can be changed by adjusting the proportions of zirconia and alumina in the composite coat to improve the thermal physical matching performance between the composite coat and the substrate, so the thermal cycle use performance of the composite coat is improved.

The invention discloses a Ti/TiN/MaN composite coating on the surface of a cutter. The Ti/TiN/MaN composite coating is divided into three layers, namely a Ti transition layer, a TiN layer and an (Al, Ti, Cr) N layer in sequence outwards from the surface of the cutter, wherein the thicknesses of the Ti transition layer, the TiN layer and the (Al, Ti, Cr) N layer are respectively 50-200nm, or 100-500nm or 2-5Mu m; the tissue structure of the Ti/TiN/MaN composite coating is a nanocrystalline structure; the (111) surface diffraction intensity I of the Ti/TiN/MaN composite coating in X-ray diffraction is lower than 400 and the surface of the Ti/TiN/MaN composite coating is 22-33GPa in hardness and 1-2-level in indentation grade. The invention also discloses a preparation method of the Ti/TiN/MaN composite coating. According to the invention, because a plasma reinforced intermediate-frequency reactive magnetron sputtering technology is used as the preparation method of the composite coating, not only is sputtering evaporation of various reactants facilitated, but also the obtained Ti/TiN/MaN composite coating is dense in tissue, high in purity, flat in surface, high in binding force with a cutter and good in wear resistance, the segregation of film components can be furthest restricted, the ionization rate and the deflection property are greatly improved, and therefore the life of the Ti/TiN/MaN composite coating in cutting machining of stainless steel is prolonged by 50-100 percent; and in addition, the Ti/TiN/MaN composite coating is simple in process, easy to master and control and is convenient for industrial production of a cutter coating.

This invention provides a method for mass production of fog-proof and self-cleaning glass. The method comprises: coating TiO2 and SiO2 onto a cleaned glass substrate by DC reactive magnetron sputtering technology and radiofrequency magnetron sputtering technology using pure titanium target and pure silicon dioxide (quartz) target respectively, thus obtaining TiO2/SiO2 double-layer fog-proof and self-cleaning glass or SiO2/TiO2/SiO2 triple-layer fog-proof and self-cleaning glass. The obtained product has better hydrophilicity, lower initial wetting angle, and longer maintaining time after stopping UV radiation than those of TiO2 single-layer glass, and overcomes the shortcoming of strong dependence on environment of present fog-proof and self-cleaning glasses.

A vanadium oxide thermo-sensitive film material with a high temperature coefficient of resistance (TCR) contains a rare earth element of Yttrium serving as a dopant in a preparation process. The vanadium oxide thermo-sensitive film material includes a substrate and a yttrium-doped vanadium oxide film layer. The yttrium-doped vanadium oxide film layer includes three elements of vanadium, oxygen and yttrium, wherein the atomic concentration of yttrium is at a range of 1%-8%, the atomic concentration of vanadium is at a range of 20-40% and the residue is oxygen. The method for preparing the vanadium oxide thermo-sensitive film material with high TCR includes a reactive magnetron sputtering method using a low-concentration yttrium-vanadium alloy target as a sputtering source or a reactive magnetron co-sputtering method using dual targets including a high-concentration yttrium-vanadium alloy target and a pure vanadium target as a co-sputtering source.

The invention relates to a self-lubricating antifriction composite thin film based on MoS2-TiC-C and a preparation method thereof, belonging to the technical field of nano-surface treatment, and the MoS2-TiC-C composite thin film is prepared by sputtering pure titanium or pure nickel on a stainless steel substrate and further carrying out reactive magnetron sputtering. The preparation process is simple, the deposition process is easy to control, and the composite thin film after deposition does not need to carry out heat treatment and can be directly used as the antifriction protective thin film on the surface of a mechanical part. The composite thin film prepared by the process has high hardness, the nano-hardness can achieve 7.6GPa, the anti-wear and antifriction performance is excellent, the friction coefficient can achieve 0.04, and the surface of the thin film can avoid the phenomena of wearing through and shedding after the friction and wear test.

The invention discloses a preparation method of a composite coating used for a gas bearing, which adopts a mid-frequency reactive magnetron sputtering system to deposit a Ti/AlTiN/Ti: DLC high- hardness and high-abrasion-resistance composite membrane. The smaller the friction coefficient between a rotor and a stator of the dynamic gas bearing is, the better to the starting of a motor, and in the high-speed rotation process, the stator and the rotor can possibly collide with each other or even have instant melting lock faults. The dynamic gas bearing made of single material can not satisfy the current requirements, and the surface modification technique of the bearing material is the key technology that limits the application of the dynamic gas bearing. The coating prepared through the method reduces the friction coefficient, improves the abrasion resistance and at the same time solves the problems of corrosion resistance and abrasive resistance of the coating. The preparation method is easy to realize and all the materials are common, so the preparation method can realize industrial production.

A powder material moved and mixed by the application of a mechanical force. The moving of the bed of powder in a container while the container is in a vacuum under a vapor source produced by magnetron sputtering, thermal evaporation, or other means of producing a coating vapor such as plasma enhanced chemical vapor deposition (PECVD), provides a means of coating the particles of powder with a material which will impart certain other desirable characteristics to the base material of which the powder is composed. The range of and combinations of coatings include a pure metal, co-deposited metals, and non-metals formed by reactive magnetron sputtering, evaporation or PECVD, or a sequentially deposited coating of both metals and non-metals. The mechanical means may be by striking, stirring or a piezoelectric transducer may be used. The mechanical force may be imposed on an open moving container of the bulk material in a vacuum or an open stationary container of the bulk material in a vacuum.

The invention provides a preparation method for a TiO2/SiO2-Ag-SiO2 nanocomposite film. The method comprises the steps of: injecting Ag ions and then forming Ag nanoparticles in a quartz glass substrate; and then depositing a TiO2 film on the surface of a silica substrate by virtue of direct-current reactive magnetron sputtering so as to obtain the TiO2/SiO2-Ag-SiO2 composite film. The Ag nanoparticles prepared by the method provided by the invention are inlaid in quartz glass, thus greatly overcoming the problem that the Ag nanoparticles are oxidized. Via the nanocomposite structure prepared by the method provided by the invention, the absorption of titanium dioxide to an ultraviolet ray part is greatly improved, so that the photocatalytic efficiency is improved. The preparation method can be widely applied to the field of optoelectronics.

The invention discloses a technology for preparing multilayer film thermoelectric materials through a physical vapor deposition method. The technology is applied to the field of preparing of multilayer film thermoelectric materials. A proper base is selected, and the multilayer film thermoelectric materials are prepared through reactive magnetron sputtering. In the preparing process, different bases can be selected for deposition, and meanwhile material kinds, film layer thicknesses, film layer numbers and the like can be selected. Compared with other methods for preparing multilayer film thermoelectric materials, the physical vapor deposition method is obvious in layered structure, high in precision, capable of reaching the nanometer level and improving the thermoelectric performance, easy to operate, capable achieving batched production, good in controllability and capable of preparing diverse multilayer film thermoelectric materials.

The invention discloses a soft and hard composite coated cutting tool and a preparation method thereof. The cutting tool comprises a substrate and a soft and hard composite coating coated on the outer surface of the substrate, wherein the substrate is made from hard alloy; the soft and hard composite coating sequentially comprises a ZrN transition layer, a CNx hard coating and a WS2 soft coating from inside to outside; the ZrN transition layer is prepared through a direct current reactive magnetron sputtering method; and both the CNx hard coating and the WS2 soft coating are prepared through a radio frequency magnetron sputtering method. The soft and hard composite coating in the invention combines the advantages of the WS2 soft coating and the CNx hard coating; the high hardness and the high wear resistance of the hard coating and the antifriction property of the soft coating are combined; and the therefore, the cutting tool can simultaneously have high wear resistance and very low friction coefficient.

The invention discloses a preparation method for a transition metal nitride super-capacitor coating material, and relates to a super-capacitor. The transition metal nitride super-capacitor coating material is obtained by performing reactive magnetron sputtering at different deposition pressures. The different deposition pressures are between 1.0 and 5.0 Pa; the transition metal nitride is ZrN, HfN and NbN. By regulating and controlling the deposition pressure during a thin film depositing process, the maximum specific capacitance values of the transition metal nitrides can be respectively 12.0, 13.5, and 10.2 mF/cm<2>; after 20,000 times of recycling, the capacity retention rates are all up to 90 percent.

The invention discloses a cuprous oxide-zinc oxide heterojunction solar cell and a preparation method thereof. Corning glass is used as a substrate, metal titanium is grown by a magnetron sputtering method, and then a silver electrode is sputtered on a titanium thin film; a nitrogen-doped Cu2O thin film is grown by using a reactive magnetron sputtering method; a microcrystalline silicon oxide thinfilm is grown on the surface of the nitrogen-doped Cu2O thin films by using an isotopic chemical vapor deposition method; a Al-doped ZnO thin film is grown by using the magnetron sputtering method; and a layer of Ag electrode is deposited on the ZnO thin film by using the magnetron sputtering method through a mask plate. The amorphous silicon oxide in microcrystalline silicon oxide is applied topassivate CuO deep level defect on the Cu2O surface, the doped silicon nanocrystals transport photogenerated carriers, and the hydrogen introduced in the growth process is diffused into Cu2O at subsequent annealing temperatures so as to reduce the defect density and improve the efficiency of the Cu2O solar cell.

The invention relates to an industrial preparation method of smart glass capable of automatically regulating infrared transmittance. The industrial preparation method comprises the following steps: (1) conventionally cleaning glass, and then performing sputtering deposition of a Ti or Si elemental element film with the thickness of 5-20nm on the surface of the glass by an ion beam sputtering method as a crystallization inducing layer; (2) performing reactive sputtering deposition of a vanadium oxide film on the crystallization inducing layer by a direct current reactive magnetron sputtering method, wherein a reactive sputtering target is prepared by fusion of high-purity vanadium with the purity of 99.96% and doping elements with different atomic ratios; reactive sputtering source gas is Ar/O2 mixed gas, and the flow proportion of Ar/O2 is 5%-10%; and (3) performing heat treatment by adopting a fast heat treatment technology for heating by light of a halogen lamp after deposition of the vanadium oxide film, wherein the temperature in the whole heat treatment process is 450-550 DEG C, and the time is 10-20min; an annealing atmosphere adopts N2/O2 mixed gas, N2 and O2 are formed by gasification of liquid nitrogen and liquid oxygen, and the flow proportion of N2 to O2 is (98%-99%): (2%-1%).

The invention discloses a vacuum reaction magnetron sputtering coating device for the inner cavity of an engine cylinder liner, comprising: a vacuum sputtering chamber, a cylinder liner support, a magnetron cathode structure and a motion control mechanism; the cylinder liner support is fixed on the The bottom of the vacuum sputtering chamber; the motion control mechanism is installed on the top of the vacuum sputtering chamber, and connected to the magnetron cathode structure to drive it; The inner surface is coated, so that the inner surface of the cylinder liner has better high temperature resistance and wear resistance; not only can the inner surface of the cylinder liner be fully covered with coating, but also can achieve uniform coating.

The invention relates to a preparation method of an epitaxial lanthanum strontium cobalt oxide film based on radio-frequency reactive sputtering. A radio-frequency reactive magnetron sputtering technology is adopted, and factors such as sputtering power, sputtering air pressure, the flow ratio of argon to oxygen and the temperature of a substrate are taken into comprehensive consideration in the sputtering process. According to the method, the importance of post-annealing is specially emphasized, sufficient oxygen is needed in the preparation process of La(1-x)SrxCoO3 film to avoid influence on the related physical characteristics of the film caused by forming of an oxygen vacancy, the defects such as the oxygen vacancy can be overcome by the post-annealing, and the surface of the film can be smoother. The preparation method of the epitaxial La(1-x)SrxCoO3 film has the advantages of compatibility with conventional industrial production, convenience in doping, simplicity in regulation of the concentration of a doped Sr element, simplicity in selection of a target material, higher utilization rate of the target material and the like, and is widely applicable to the preparation of related spintronics devices.

The invention belongs to the technical field of magnetron sputtering coating, and particularly relates to a method for improving the magnetron sputtering deposition rate of SiO2 thin film. A plasma emission and detection system is employed for real-time monitoring an intermediate frequency reactive magnetron sputtering plasma emission spectrum, and stabilizing the reactive magnetron sputtering at any operating point in a transition state according to the set value of the detection system; wherein gas atmosphere comprises argon as a process gas and oxygen as a reactive gas; and the process gas is fed below twin targets, and the reactive gas is fed above the twin targets. The in situ monitoring of the plasma emission spectrum in the present invention does not affect the thin film growth process, and is conducive to the development of the process of thin film preparation in an intelligentization direction and the combination of spectral analysis with a computer, effectively improving production efficiency and reducing production costs.