The invention relates to a three-dimensional graded carbon-clad NaTi<2>(PO<4>)<3> / C
micrometer flower
electrode material and a preparation method and application thereof. The
diameter of the three-dimensional graded carbon-clad NaTi<2>(PO<4>)<3> / C
micrometer flower
electrode material is 5-10 micrometers, the thickness of a carbon-clad NaTi<2>(PO<4>)<3> / C
nanosheet subunit is only 1-5 nanometers, mesopores with pore diameters of 2-30 nanometers are formed in the carbon-clad NaTi<2>(PO<4>)<3> / C
nanosheet subunit, the thickness of a surface
carbon layer is 2-5 nanometers, and the
nanosheet subunits are in over joint to form a three-dimensional conductive network. The three-dimensional graded carbon-clad NaTi<2>(PO<4>)<3> / C
micrometer flower
electrode material has the advantages that the three-dimensional graded carbon-clad NaTi<2>(PO<4>)<3> / C micrometer flower is prepared by a simple and practical solovothermal method combined with a high-temperature
calcination method, and is endowed with excellent
high rate performance and stable long-circulation capability when taken as a positive electrode active material of a
sodium ion battery. The process is simple, the three-dimensional graded carbon-clad NaTi<2>(PO<4>)<3> / C micrometer flower
electrode material is high in practicable and is high in
safety coefficient, the requirement on a device is low due to the adoption of the solovothermal method and the
calcination processing, production can be expanded, and market promotion is promoted.