86 results about "Perillaldehyde" patented technology

The purpose of the present invention is to provide antiseptic disinfectant, and cosmetics and toiletries, medicine or food containing the same, which enhance the antibacterial activity that 1,2-alkanediol originally have against a broad range of strains by compounding 1,2-alkanediol with 5-10 carbons and a certain fragrance component. The present invention relates to an antiseptic disinfectant, and cosmetics and toiletries, medicine or food containing the same, which include 1,2-alkanediol with 5-10 carbons, and one or more materials selected from a group of citral, geraniol, nerol, perillaldehyde, α-terpineol, dodecanol and L-carvone.

The invention discloses a formula of tobacco flavoring essence containing purple perilla. According to the formula, the tobacco flavoring essence consists of the following components in percentage by mass: 10 to 15 percent of clary sage extractum, 0.3 to 0.8 percent of perillaldehyde, 5 to 10 percent of Yuanyan tobacco extractum, 2 to 8 percent of Guiyan tobacco extractum, 5 to 8 percent of liquorice extractum, 2 to 5 percent of red date extractum, 1.5 to 3 percent of clary sage lactone, 8 to 15 percent of licorice tincture. 6 to 10 percent of carob bean extractum, 1 to 5 percent of vanilla bean extract, 10 to 15 percent of propylene glycol, 10 to 15 percent of purified water and 10 to 15 percent of edible ethanol. According to the formula, purple perilla is added to increase tobacco fragrance and adjust the taste of the tobacco, so that the taste of the tobacco is improved, the natural sweet fragrance of the tobacco is enhanced, dry, astringent and bitter mouthfeel of customers is improved and requirements of the customers are met.

The invention discloses building paint. The building paint is prepared from 3.5-7.5 parts by weight of methyl acetate, 2.3-4.5 parts by weight of hept-2-ene-2-methanol, 6.5-12.7 parts by weight of hydroxymethyl propyl cellulose, 10-15 parts by weight of titanium dioxide, 20-28 parts by weight of white emulsion, 1.2-3.5 parts by weight of perillaldehyde, 2.5-6.4 parts by weight of distyrylphenol polyoxyethylene ether and 3.5-6.8 parts by weight of (R)-(-)-alpha-methoxyphenylacetic acid. Compared with the existing exterior wall paint, the building paint improves an emulsion paint finished product covering capacity through use of a mixture of methyl acetate and white emulsion. Through mixing of hydroxymethyl propyl cellulose and titanium dioxide, latex finished product adhesion and water washing resistance are improved. Through the mixture of perillaldehyde, distyrylphenol polyoxyethylene ether and (R)-(-)-alpha-methoxyphenylacetic acid, the paint film has lasting and beautiful gloss and has lasting pollution resistance.

The invention discloses a preparation method of antibacterial active carbon, which belongs to the technical field of water treatment preparation. Rice husks are subjected to hydrolytic degradation under the action of a compound activator of zinc chloride and copper chloride so as to form a low polymer and be dewatered through reaction, so that an intermediate product can be promoted to be condensed to form a graphite-like microcrystalline structure and produce a porous system; under an acidic condition, a large number of residues of zinc and copper ions in high concentration form a complex in an aromatization organic matter so as to be adsorbed in micropores of the graphite-like microcrystalline structure, and the copper and zinc ions can remarkably inhibit amination of bacteria on nitrite, so that the breeding of the bacteria is reduced, and the aim of an antibacterial effect is achieved. Apurple perilla extract mainly contains perillaldehyde which is a powerful antibacterial substance and has a certain damage effect on formation of a bacterial cell wall, and after activated carbon is soaked in an acetone solution of the purple perilla extract, the purple perilla extract is distributed in activated carbon pores so as to achieve an inhibition effect on surrounding bacteria breeding, so that the aim of the antibacterial effect is achieved.

The invention discloses a perilla leaf extract and an extraction method thereof. The perilla leaf extract comprises 1 part of active ingredient A extracted first and 1.25 parts of active ingredient B extracted for the second time, in parts by weight. After the ingredient A is extracted, polyphenols and anthocyanin in the perilla leaves are removed by use of a microwave method. The ratio of the ingredients of the perilla leaf extract is close to that of oils of the perilla leaves; especially, the ratio of perillaldehyde and the ratio of perillene are relatively high.

The invention discloses a clean production method for extracting natural perfume perillaldehyde, and in particular relates to a clean production method for extracting the natural perfume perillaldehyde from a green plant salted midorinoha. The method is characterized in that: a distillation method is adopted to extract the salted midorinoha, and distillate is adsorbed by an adsorbent resin; and ethanol is used for eluting, an atmospheric distillation method is preformed on eluent to recover the ethanol to obtain yellow concentrated solution, namely a perillaldehyde product.

The invention relates to an extraction method of odorless perillaldehyde with a high stability. The extraction method is characterized by comprising the following steps: (1) squeezing raw materials; (2) performing an ultrasonic treatment; (3) extracting; (4) refluxing and condensing; (5) absorbing and eluting; (6) carrying out a membrane treatment; (7) distilling and condensing. In the conventional extraction method, only one product can be produced; while in the provided extraction method, pigment and perillaldehyde can be produced at the same time, the comprehensive utilization of raw materials is achieved, and the economic benefits are increased. Moreover, the leaf alcohol can be separated from the perillaldehyde through a temperature different grading condensation recovery method, thus the perillaldehyde purity is improved, and the interference of leaf alcohol is eliminated. The liquid perillaldehyde extract after the absorption treatment is subjected to a membrane separation treatment so as to reduce the odor or even eliminate the odor. In the extraction method, a special porous resin is adopted in a multi-stage elution technology, and is co-used with a mixed oxidizing agent so as to produce the perillaldehyde, which has the advantages of high color value, no odor, light resistance, heat resistance, and stability.

The invention relates to a synthetic method of a marine natural product Puupehenol, and belongs to the field of chemical synthesis. The synthetic method comprises the steps: taking (+) aromatic perillaldehyde and hydroxyquinol as starting raw materials, firstly, utilizing (+) aromatic perillaldehyde and p-toluenesulfonhydrazide to form (+) aromatic perillasulfonyl hydrazone, then carrying out palladium-catalyzed cascade Carving migration insertion and intramolecular cyclization reaction of iodine substituted 1,2,4-trimethoxybenzene and (+) aromatic perillasulfonyl hydrazone in an alkali environment to obtain a marine natural product Puupehenol skeleton; and then carrying out hydroxy reduction and double-bond isomerization of a bicyclic sesquiterpanes part of the Puupehenol skeleton, and carrying out oxidation, reduction, cyclization and protection group removal to obtain the final target product Puupehenol. The synthetic method has the advantages of fewer reaction steps, simple operation, and good product selectivity, and is suitable for industrialized production.

The invention discloses a nano-emulsion containing perillaldehyde, citral and nystatin. The nano-emulsion is prepared from the following raw materials by weight percent: 13.60-29.66% of a surfactant, 3.10-7.20% of oil, 0.01-2.00% of perillaldehyde, 0.01-2.00% of citral, 0.01-1.00% of nystatin, and the balance of distilled water, wherein the sum of the percentages by weight of the raw materials is 100%. The nano-emulsion can achieve better skin permeability, improves the solubility of perillaldehyde, citral and nystatin, increases the bioavailability of perillaldehyde, citral and nystatin, and further has the slow release property to prolong the metabolism time of the drum in vivo and give full play of the efficacy.

The invention provides an omega-3 composition with an effect of reducing blood fat. The omega-3 composition comprises oleic acid, linoleic acid, alpha-linolenic acid, vitamin E, sesamin, sesamol, procyanidine and perillaldehyde. The omega-3 composition utilizes the synergistic effect of all the components and can be applied to preparation of health-care food or food. The composition can be obtained by matching of single compounds according to certain proportion and also can comprise multiple materials containing the compounds. To be exact, the composition can be prepared by sunflower seed oil, grape seed oil, black sesame oil, perilla oil, perilla volatile oil and sesame lignan according to certain proportion. The composition provided by the invention has the active components with the effects of reducing cholesterol in blood, adjusting the metabolism, reducing triglyceride and low-density lipoprotein, inhibiting the synthesis of the triglyceride, increasing excretion of various lipids in the body and resisting oxidization and the like, thus achieving the effect of reducing the blood fat and having obvious controlling effect to complications.

The invention relates to a purple perilla new species breeding method. The purple perilla new species breeding method comprises the following steps: step (1) breeding a purple perilla selfing line andstep (2) breeding a hybrid species. Compared with the purple perilla in the prior art, the purple perilla planted by virtue of the breeding method of the invention can apparently improve the yield; the perillaldehyde and purpurin are greatly improved; the antivirus capability can also be greatly improved, the variation can be prevented, the purple perilla can be stably planted, the advantages ofthe purple perilla in the prior art are integrated, the leaf is large and thick, and the performance is stable.

The invention discloses an application of perillaldehyde in preparation of a medicine for preventing and treating vaginitis, and belongs to the technical field of medicines. The invention further discloses a medicine for preventing and treating candida albicans vaginitis, which is a preparation prepared by using perillaldehyde as an active ingredient with pharmaceutically acceptable auxiliaries. The perillaldehyde has a relatively strong effect for inhibiting candida albicans. An in-vivo experiment is carried out by adopting a mouse immunosuppression model to evaluate the effect of perillaldehyde for preventing and treating candida albicans vaginitis; and fungus inspection and tissue histopathologic examination prove that perillaldehyde has relatively strong effects for preventing and treating candida albicans vaginitis, and can be used for preparing the medicine for preventing and treating candida albicans vaginitis.

The invention discloses an antibacterial water treatment material and a preparing method thereof.The antibacterial water treatment material is prepared from, by weight, 50-58 parts of polyvinyl butyral, 6-9 parts of chitosan fibers, 5-7 parts of diisobutyl phthalate, 2-3 parts of phenoxyethanol, 1-2 parts of 1,8-diazabicyclo(5,4,0)7-hendecene, 0.8-1 part of peroxide terephthaloyl, 0.5-1 part of 5,6,7,3',4'-pentamethoxyl flavone, 0.5-0.8 part of zinc borate, 0.2-0.5 part of ammonium oxalate, 0.2-0.3 part of aluminum sulfate and 0.8-0.5 part of perillaldehyde.The invention further provides the preparing method of the antibacterial water treatment material.

The invention provides a preparation method of pomelo peel total flavones. The method comprises the following steps: taking fresh pomelo peel, cleaning, grinding, adding ethanol until the volume percent of ethanol reaches 75%, putting into a 90-DEG C water bath, sufficiently condensing under reflux to obtain a crude extracting solution, carrying out vacuum filtration by using a vacuum filter, collecting the filtrate, concentrating under reduced pressure, drying the concentrated solution and granulating to obtain the pomelo peel total flavone extract. The obtained pomelo peel total flavones have high content, and can be mixed with lauraldehyde and perillaldehyde to prepare the pomelo peel total flavone composition.

The invention relates to a synthesis method for a marine natural product Puupehenone, and belongs to the field of chemical synthesis. According to the synthesis method, (First) fragrant perillaldehyde and cyclohexanedione serve as initial raw materials; the synthesis method comprises the following steps: reacting the cyclohexanedione which is subjected to alkyl protection and the aldol of the (First) fragrant perillaldehyde to prepare beta-hydroxycyclohexanone of bicyclic sesquiterpanes; performing nucleophilic cyclization-elimination reaction of attacking a carbonyl by a hydroxyl under the catalysis of an acid to obtain a skeleton of the marine natural product Puupehenone; oxidizing the carbonyl at the ortho-position of an unsaturated ketene six-member ring carbonyl of the Puupehenone skeleton, and performing keto enol interconversion to obtain the final natural product Puupehenone. The synthesis method has the characteristics of few reaction steps, simple operation, high product selectivity, and application to industrial production and the like.

The invention relates to a making method of pickled radish with low nitrite content, and belongs to the technical field of food processing. The method comprises a making method of pickled radish, or amaking method of radish pickles or a making method of pickled sauce radish. The required main material is radish strips, and auxiliary materials comprise purple perilla and soybean sprout juice, edible salt, white vinegar, soybean oligosaccharide, white sugar, capsicum frutescens, ginger, garlic and water. The making method comprises the operation steps as follows: the radish strips are dehydrated by a hot air drying technology; pickling mother liquor is made from the purple perilla and soybean sprout juice and the auxiliary materials; dried radish and the pickling mother liquor are mixed, ajar is sealed for fermentation, and the pickled radish or radish pickles or pickled sauce radish with low nitrite content is made. The nitrite content of the pickled radish is 1.0-2.8 mg/kg, and is lower than the commercial content of 9.6 mg/k. Perillaldehyde and other substances in purple perilla leaves can inhibit reproduction and growth of harmful bacteria. Polypeptides, amino acids and monosaccharides in soybean sprouts provide nutrients for lactic acid bacteria and promote fermentation of the lactic acid bacteria.

The invention relates to the technical field of beauty products and provides sea buckthorn beauty mud with lasting whitening and moisturizing effects and a preparation method thereof. The preparationmethod comprises the following steps: loading sea buckthorn juice with jellyfish dry powder and coating with perillaldehyde to prepare a sea buckthorn compound A; loading sea buckthorn juice and hyaluronic acid with composite shell powder of shrimp and crab shells to prepare a sea buckthorn compound B; and then mixing the sea buckthorn compound A, the sea buckthorn compound B, a ginkgo biloba extract, a bamboo leaf extract, bamboo charcoal powder, lecithin, talcum powder, glycerin, seaweed glue, hydroxyethyl celluloses and deionized water into mud to prepare the sea buckthorn beauty mud with the lasting whitening and moisturizing effects. Compared with a traditional method, the preparation method provided by the invention has the benefits that the isolation of active ingredients of sea buckthorns can be effectively prevented, and the defect that the effects of the active ingredients of the sea buckthorns are not deep and lasting is also overcome.

The invention discloses a clay desulfurizer as well as a preparation method and an application thereof. The desulfurizer is prepared from raw materials in parts by weight as follows: 28-36 parts of clay, 1-5 parts of pectin, 3-7 parts of perillaldehyde and 11-19 parts of acetic acid. The clay is taken as a raw material and mixed with the pectin, the mixture is ground and then treated with acetic acid and perillaldehyde, and the desulfurizer is prepared. Gasoline with ultralow sulfur content being 6 mu g/g or below can be obtained under the condition that RON (research octane number) loss is lower than 2.0. The desulfurizer has good sulfur selectivity and high desulfurization degree, and the octane number loss caused by olefin hydrogenation saturation can be avoided while a sulfur-containing compound in gasoline is deeply removed. The desulfurizer is long in service life and environment-friendly, causes no secondary pollution and is good in regeneration performance. A preparation process is simple, easy to operate and control, stable in performance, low in production cost and suitable for industrial production.

The invention belongs to the technical field of deodorants and in particular relates to a deodorant. The deodorant is prepared from the following raw materials in parts by weight: 3 to 5 parts of vanillin, 6 to 8 parts of carvone, 0.5 to 2 parts of perillaldehyde, 1 to 2 parts of citral, 3 to 5 parts of eucalyptol, 1 to 3 parts of cinnamaldehyde, 20 to 25 parts of ethanol and 150 to 300 parts of de-ionized water. The deodorant provided by the invention does not contain chemical harmful substances and chemical objectionable odor, is efficient and stable and is simple in preparation and low in price.