The invention discloses a main device of a cryogenic micro-
differential scanning calorimetry system which comprises a cryostage, a sample support and a reference support; the cryostage is a cylinder, an annular
nitrogen channel is arranged inside the cryostage, and the cyrostage is provided with a cold
nitrogen inlet and a cold
nitrogen outlet; two symmetrical cavities are opened along the central axis line of the cryostage, the upper half part of each cavity is cylindrical, the
lower half part of each is rectangular, the sample support or the reference support is arranged in the rectangular cavities and fixed by a rectangular
brass ring; cold nitrogen carries out the heat exchange with the cryostage after entering the annular channel, the cold energy is transferred to the sample and the reference support, thereby completing the cooling of the sample and a reference substance; the sample and the reference support adopt
quartz glass as substrates, grid-shaped thin-film thermocouples are sputtered on the
quartz substrates; the back surfaces of the
quartz substrates are plated with transparent
tin oxide heating thin films; the outsides of the thin-film thermocouples and the
tin oxide heating thin films are respectively plated with SiO2 protective
layers; the sample and the reference support are geometrically symmetrical and same in weight. The main device of the cryogenic micro-
differential scanning calorimetry system can simultaneously obtain micro-images of the sample and various physical and chemical parameters during the temperature increase and the temperature decrease processes.