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126results about How to "Increase unit capacity" patented technology

Continuous production method of epoxy chloropropane by hydrogen peroxide process

The invention provides a preparation method of chloroepoxy propane by chloropropene epoxidation. Chloropropene, a solvent and titanium silicalite molecular sieve catalyst fine particles are put in a reaction kettle for reaction at the temperature of 10-80 DEG C. The method is characterized in that the reaction kettle is a single kettle or multistage slurry bed reaction kettles with same or different volumes which are connected in series; the reaction solution needs not to be homogeneous phase, slurry particles of the chloropropene, the solvent and the titanium silicalite molecular sieve catalyst are added to a first stage reaction kettle by a metering pump, hydrogen peroxide is dropwise added to the first stage reaction kettle or each stage of the reaction kettles, the reaction occurs in a weakly acidic condition, materials are subject to oil-water delamination after the reaction to be divided into oil-phase slurry and water-phase slurry; the catalyst is suspended in the water phase, and the oil phase is sent to a rectification tower to separate the chloropropene, the epichlorohydrin and trace methanol; the water phase slurry is filtered, a catalyst filter cake or concentrated slurry is directly beaten by the solvent, and pumped to a first stage epoxidation reaction kettle, the water phase slurry contains the methanol, trace epichlorohydrin and the water which is generated by the reaction and the water which is taken by the hydrogen peroxide, the trace methanol and the epichlorohydrin are separated out by negative pressure rectification, and the recovered methanol is used for preparation of the catalyst slurry. The method has the advantages of simple process, little solvent consumption and high product separation yield, and is available for industrialized production.
Owner:JIANGSU YANGNONG CHEM GROUP +2

Flexible electrode and preparation method thereof

The invention discloses a preparation method of a flexible electrode and the flexible electrode obtained through the preparation method. The preparation method comprises the steps of a, manufacturing a carbon nano tube and an grapheme oxide into a homodisperse mixed dispersion agent; b, removing a solvent in the mixed dispersion agent, and obtaining a thin film with a three-dimensional conductive network; c, conducting in-situ polymerization on the three-dimensional conductive network with organic polymer conductive materials to obtain a three-element flexible composite film; d, conducting reduction on the grapheme oxide in the three-element flexible composite film to obtain the flexible electrode. According to the preparation method, firstly, the thin film with the three-dimensional conductive network is formed by the carbon nano tube and the grapheme oxide, and then, the in-situ polymerization is carried out on the three-dimensional network with the organic polymer conductive materials; in the three-dimensional conductive network, the carbon nano tube is inserted into the portion between grapheme sheet layers, so that the interval between the grapheme sheets and the specific surface area of the grapheme sheets are increased, the carbon nano tube also overcomes the defect generated in the oxidation process of grapheme, electronic transmission is facilitated, and the specific capacitance of the flexible electrode is improved.
Owner:未名电池科技(深圳)有限公司

Method of manufacturing back contact heterojunction single crystalline silicon solar cell

The invention provides a method of manufacturing a back contact heterojunction single crystalline silicon solar cell, which belongs to the technical field of solar photovoltaics. The method comprises the following steps: (1) cleaning of single crystalline silicon, removal of a damage layer and etching are carried out; (2) a single crystalline silicon front surface passivation layer is formed, and coating of an anti-reflective layer is carried out; (3) coating of a single crystalline silicon back surface passivation layer is carried out; (4) a mask technology is adopted to form a P-type amorphous silicon pattern through coating of the single crystalline silicon back surface; (5) a mask technology is adopted to form an N-type amorphous silicon pattern through coating of the single crystalline silicon back surface; (6) a mask technology is adopted to form a protection film pattern through coating of the back surface; and (7) a chemical plating plus electroplating technology is adopted to form a contact electrode for a transmitting electrode and a base electrode on the back surface. the method of the invention has the advantages of simple process and low manufacturing cost whether for coating and positioning of a P / N junction or for back electrode manufacturing, and can be applied to mass production of the back contact heterojunction single crystalline silicon solar cells.
Owner:深圳市科纳能薄膜科技有限公司

Method for recovering coin protein sugar dregs and preparing protein nitrogen sources and nitrogen-containing syrup

ActiveCN101787382AIncrease content concentrationEasy to useFermentationProtein nitrogenWastewater
The invention discloses a method for recovering coin protein sugar dregs and preparing protein nitrogen sources and nitrogen-containing syrup in the production of enzymatic corn starch sugar, comprising the steps of size mixing, liquefying, saccharifying, standing separation, centrifugal separation, proteolysis, concentration, drying, compounding, and the like. In the invention, protein is condensed under the heat flash of liquefying, the protein sugar dregs concentrate and float upwards in saccharifying, the sugar dregs are recovered through the steps of standing separation and centrifugal separation, the sugar dregs are dried into protein, or the sugar dregs are hydrolyzed to prepare protein nitrogen sources, and the nitrogen sources can be compounded with syrup to form nitrogen-containing starch syrup for fermenting. Clarified saccharification liquid after centrifugal separation is decolored, filtered, refined and concentrated, and starch syrup products are obtained. The majority of lentous sugar dregs in the saccharification liquid are removed before the treatment of decoloring and filtering, and the decoloring and filtering performance of the material is better. The use level of active carbon, and the like can be properly reduced, the production capability of filtering equipment is improved, and the frequency of the loading and unloading of filters as well as the consumption of washing waste water and various kinds of loss are greatly reduced.
Owner:广州双桥(重庆)有限公司

Thermal field structure of polysilicon ingot casting furnace

The invention relates to a thermal field structure of a polysilicon ingot casting furnace, which comprises a furnace body, a thermal-insulation cage body and a crucible, wherein the thermal-insulation cage body is arranged inside the furnace body, the crucible is arranged inside the thermal-insulation cage body, and the thermal-insulation cage body is a sealed thermal field chamber formed by an upper thermal-insulation body, a lower thermal-insulation body and a thermal-insulation baseplate; the upper thermal-insulation body is fixed on the furnace body; the bottom of the lower thermal-insulation body is placed on the thermal-insulation baseplate, and the lower thermal-insulation body can slide up and down relative to the upper thermal-insulation body through a lifting mechanism; the crucible is placed on a heat exchange platform in a supporting structure; and the thermal-insulation baseplate is placed on supporting columns of the supporting structure for fixation. In the invention, when a silicon material is heated, melted and thermally preserved for a period of time, in a lifted process of the lower thermal-insulation body, a vertical temperature gradient field is formed on a crystallization face of the silicon material due to the vertical temperature difference inside the thermal field chamber, and the crystallographic orientation of the silicon material can be realized by controlling heat dissipating and heating, so that the quality of a polysilicon cast ingot is improved. Meanwhile, the process time is shortened, the energy consumption is decreased and the unit productivity is improved.
Owner:深圳市石金科技股份有限公司

Enclosed type electrolytic tank and electrolytic system

The invention discloses a sealed electrolysis bath and an electrolytic system, the electrolysis bath comprises two end plates, an anode component, a cathode component, sealing components and a compacting device, wherein liquid flowing ports are evenly arranged on the two end plates, liquid flowing through-holes are correspondingly arranged on the anode component and the cathode component, the anode component and the cathode component are separately arranged between the two end plates, a polar chamber is formed between the anode component and the cathode component, the sealing components are evenly arranged on the contact position of the anode component, the cathode component and the end plates, and the anode component, the cathode component and the end plates form a sealed structure after being compacted through the compacting device. The electrolysis bath has simple structure and can increase the circulation speed of electrolyte, the overpotential is effectively lowered, the current density of an anode and a cathode is increased when in electrolysis, the productivity of unit electrolysis bath is increased, and the electrolysis bath can be widely applied in electrowinning various metal and in electrowinning metallic solution with low concentration. The sealed structure avoids the influence of gas which is discharged in the electrolysis process to environment in a workshop.
Owner:BEIJING GENERAL RES INST OF MINING & METALLURGY

Citric acid continuous cooling crystallization system and method thereof

The invention relates to a citric acid continuous cooling crystallization system and a method thereof. In an existing method of producing citric acid monohydrate crystal, intermittent processing equipment is used, product size distribution is uneven, a crystal product is agglutinated seriously, and difference between product batches is large. According to the crystallization method, a citric acid solution is heated and concentrated through two-effect heat exchange, then is input into a circulating pipeline composed of an indirect cooler and a cooling crystallizer through a feed pump and is continuously cooled for cooling crystallization in the circulating pipeline under the action of a circulating pump, and citric acid monohydrate slurry is obtained through cooling crystallization; the citric acid monohydrate slurry is discharged through a discharging pump, conveyed to a crystal slurry buffering tank to be buffered and then input into a centrifugal separation device for solid-liquid separation. According to the continuous cooling crystallization method, intermittent crystallization operation of using a crystallization kettle for feeding and discharging and conducting cooling in the kettle in the past is replaced, the feeding, discharging and cooling flow path is stabilized, continuity and stability of product quality can be effectively ensured, and production efficiency and product quality of citric acid monohydrate are greatly improved.
Owner:西安航天华威化工生物工程有限公司

Continuous preparation method of high-purity magnesium hydroxide

InactiveCN101224901ASmall logistics volumeHigh yieldMagnesium hydroxideChemical reactionPollution
The invention provides a method for continuously preparing highly pure magnesium hydroxide which relates to a method for continuously producing highly pure magnesium hydroxide with bischofite as raw material and ammonia as precipitant. The method is characterized in that: a treated bischofite is prepared into a solution with the concentration of 0.5 mol/L-4 mol/L, the bischofite solution and ammonia gas are added continuously after the reaction begins and the chemical reaction for depositing the magnesium hydroxide is carried out continuously. Characteristics of the reaction vessel utilization ratio, the productive capacity of unit volume, technical reliability and stability and so on of the method are greatly improved compared with intermittent reaction technology. The base liquid does not need to be replaced or heated repeatedly, thus energy-saving effect is distinct and labor productivity is high. The method can be used for obtaining magnesium hydroxide with the granularity of 10 microns-100 microns and the purity of 99 percent-99.999 percent. The ammonia nitrogen treatment of the tail solution adopts a commercial method that meets environmental protection requirement. The product produced by the invention has large granule size, high purity, more specifications, low cost, high equipment utilization rate and low one-time investment and has no pollution to the environment.
Owner:DALIAN MARITIME UNIVERSITY +1

Continuous production method of epoxy chloropropane by hydrogen peroxide process

The invention provides a preparation method of chloroepoxy propane by chloropropene epoxidation. Chloropropene, a solvent and titanium silicalite molecular sieve catalyst fine particles are put in a reaction kettle for reaction at the temperature of 10-80 DEG C. The method is characterized in that the reaction kettle is a single kettle or multistage slurry bed reaction kettles with same or different volumes which are connected in series; the reaction solution needs not to be homogeneous phase, slurry particles of the chloropropene, the solvent and the titanium silicalite molecular sieve catalyst are added to a first stage reaction kettle by a metering pump, hydrogen peroxide is dropwise added to the first stage reaction kettle or each stage of the reaction kettles, the reaction occurs in a weakly acidic condition, materials are subject to oil-water delamination after the reaction to be divided into oil-phase slurry and water-phase slurry; the catalyst is suspended in the water phase, and the oil phase is sent to a rectification tower to separate the chloropropene, the epichlorohydrin and trace methanol; the water phase slurry is filtered, a catalyst filter cake or concentrated slurry is directly beaten by the solvent, and pumped to a first stage epoxidation reaction kettle, the water phase slurry contains the methanol, trace epichlorohydrin and the water which is generated by the reaction and the water which is taken by the hydrogen peroxide, the trace methanol and the epichlorohydrin are separated out by negative pressure rectification, and the recovered methanol is used for preparation of the catalyst slurry. The method has the advantages of simple process, little solvent consumption and high product separation yield, and is available for industrialized production.
Owner:JIANGSU YANGNONG CHEM GROUP +2
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