45 results about "Anhydrous Zinc Acetate" patented technology

The invention discloses a preparation method of a three-dimensional flower-like zinc oxide nanometer material and an obtained product. The method comprises the following steps: mixing anhydrous zinc acetate and ethylene glycol to obtain a transparent solution, adding a mixture of lauryl amine and oleic acid into the transparent solution, and uniformly mixing so as to obtain a precursor solution; raising the temperature of the precursor solution to be 130-140 DEG C under inert gas shielding so as to carry out a reflux reaction, performing centrifugal separation and washing after reaction completion, thereby obtaining the zinc oxide nanometer material, wherein the zinc oxide nanometer material is in the shape of a three-dimensional flower. The process disclosed by the invention is simple and convenient in process flow and short in reaction time, and the obtained product has the flower shape, looks like half a calliandra flower, is controllable in morphology and adjustable in size, has excellent application prospects in the fields of new energy materials and sensing and can serve as an additive of a high-end sun and skin care product.

The invention discloses a di-pyrene modified perylene bisimide derivative fluorescent probe and a synthesis method and application thereof, and belongs to the technical field of protein detection. The preparation of the fluorescent probe comprises the following steps that in a protective atmosphere, 1-methyl-2-pyrrolidinone solution of a pyrene sulfonyl derivative is added into a 1-methyl-2-pyrrolidinone solution of perylene; then, anhydrous zinc acetate is added to obtain a mixed solution; next, the mixed solution is stirred; heating reflux is performed for 10 to 15h at 150 to 200 DEG C; after the reaction liquid obtained after the reflux is cooled to the room temperature, filtering is performed to obtain filter liquid; the filter liquid is subjected to acid washing; precipitates occur; suction filtration is performed; filter cake is obtained; the filter cake is washed and dried to obtain the di-pyrene modified perylene bisimide derivative fluorescent probe. The fluorescent probe provided by the invention has the advantages that the chemical stability is high; the response speed is high; the sensitivity is high; the discrimination performance is good; the sample consumption quantity is small; the data collection is simple, and the like. The instant and on-line detection of the protein can be realized. The fluorescent probe provided by the invention can be used for respectively realizing the distinguished detection of various proteins.